BS EN ISO 16017-1-2001 Indoor ambient and workplace air - Sampling and analysis of volatile organic compounds by sorbent tube thermal desorption capillary gas chromatography - Pump.pdf
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1、BRITISH STANDARD BS EN ISO 16017-1:2001 Indoor, ambient and workplace air Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography Part 1: Pumped sampling The European Standard EN ISO 16017-1:2000 has the status of a British Standard ICS 13.
2、040.20; 13.040.30 NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAWBS EN ISO 16017-1:2001 This British Standard, having been prepared under the direction of the Health and Environment Sector and policy Committee, was published under the authority of the Standards Policy and Stra
3、tegy Committee on 21 September 2001 BSI 21 September 2001 ISBN 0 580 38491 8 National foreword This British Standard is the official English language version of EN ISO 16017-1:2000. It is identical with ISO 16017-1:2000. The UK participation in its preparation was entrusted by Technical Committee EH
4、/2, Air Quality, to Subcommittee EH /2/3, Ambient Atmospheres, which has the responsibility to: A list of organizations represented on this committee can be obtained on request to its secretary. Cross-references The British Standards which implement international or European publications referred to
5、 in this document may be found in the BSI Standards Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Find” facility of the BSI Standards Electronic Catalogue. A British Standard does not purport to include all the necessary provisions of a contrac
6、t. Users of British Standards are responsible for their correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. aid enquirers to understand the text; present to the responsible international/European committee any enquiries on the interpreta
7、tion, or proposals for change, and keep the UK interests informed; monitor related international and European developments and promulgate them in the UK. Summary of pages This document comprises a front cover, an inside front cover, the EN ISO title page, the EN ISO foreword page, the ISO title page
8、, pages ii to iv, pages 1 to 28, an inside back cover and a back cover. The BSI copyright date displayed in this document indicates when the document was last issued. Amendments issued since publication Amd. No. Date CommentsEUROPEANSTANDARD NORMEEUROPENNE EUROPISCHENORM ENISO160171 November2000 ICS
9、 Englishversion Indoor,ambientandworkplaceairSamplingandanalysisof volatileorganiccompoundsbysorbenttube/thermal desorption/capillarygaschromatographyPart1:Pumped sampling(ISO160171:2000) Airintrieur,airambiantetairdeslieuxdetravail Echantillonnageetanalysedescompossorganiques volatilspartubeadsorpt
10、ion/dsorption thermique/chromatographieenphasegazeusesur capillairePartie1:Echantillonnageparpompage(ISO 160171:2000) Innenraumluft,AuenluftundLuftamArbeitsplatz ProbenahmeundAnalyseflchtigerorganischer VerbindungendurchSorptionsrhrchen/thermische Desorption/KapillarGaschromatographieTeil1: Probenah
11、memiteinerPumpe(ISO160171:2000) ThisEuropeanStandardwasapprovedbyCENon30September2000. CENmembersareboundtocomplywiththeCEN/CENELECInternalRegulationswhichstipulatetheconditionsforgivingthisEurope an Standardthestatusofanationalstandardwithoutanyalteration.Uptodatelistsandbibliographicalreferencesco
12、ncernings uchnational standardsmaybeobtainedonapplicationtotheManagementCentreortoanyCENmember. ThisEuropeanStandardexistsinthreeofficialversions(English,French,German).Aversioninanyotherlanguagemadebytra nslation undertheresponsibilityofaCENmemberintoitsownlanguageandnotifiedtotheManagementCentreha
13、sthesamestatusasthe official versions. CENmembersarethenationalstandardsbodiesofAustria,Belgium,CzechRepublic,Denmark,Finland,France,Germany,Greece, Iceland,Ireland,Italy,Luxembourg,Netherlands,Norway,Portugal,Spain,Sweden,SwitzerlandandUnitedKingdom. EUROPEANCOMMITTEEFORSTANDARDIZATION COMITEUROPEN
14、DENORMALISATION EUROPISCHESKOMITEEFRNORMUNG ManagementCentre:ruedeStassart,36B1050Brussels 2000CEN Allrightsofexploitationinanyformandbyanymeansreserved worldwideforCENnationalMembers. Ref.No.ENISO160171:2000EForeword ThetextoftheInternationalStandardISO160171:2000hasbeenpreparedbyTechnical Committe
15、eISO/TC146“Airquality“incollaborationwithTechnicalCommitteeCEN/TC264 “Airquality“,thesecretariatofwhichisheldbyDIN. ThisEuropeanStandardshallbegiventhestatusofanationalstandard,eitherbypublication ofanidenticaltextorbyendorsement,atthelatestbyMay2001,andconflictingnational standardsshallbewithdrawna
16、tthelatestbyMay2001. AccordingtotheCEN/CENELECInternalRegulations,thenationalstandardsorganizationsof thefollowingcountriesareboundtoimplementthisEuropeanStandard:Austria,Belgium, CzechRepublic,Denmark,Finland,France,Germany,Greece,Iceland,Ireland,Italy, Luxembourg,Netherlands,Norway,Portugal,Spain,
17、Sweden,SwitzerlandandtheUnited Kingdom. NOTEFROMCMC: TheforewordissusceptibletobeamendedonreceptionoftheGerman languageversion.Theconfirmedoramendedforeword,andwhenappropriate,thenormative annexZAforthereferencestointernationalpublicationswiththeirrelevantEuropean publicationswillbecirculatedwiththe
18、Germanversion. Endorsementnotice ThetextoftheInternationalStandardISO160171:2000wasapprovedbyCENasa EuropeanStandardwithoutanymodification. ENISO160171:2000Reference number ISO 16017-1:2000(E) INTERNATIONAL STANDARD ISO 16017-1 First edition 2000-11-15 Indoor, ambient and workplace air Sampling and
19、analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography Part 1: Pumped sampling Air intrieur, air ambiant et air des lieux de travail chantillonnage et analyse des composs organiques volatils par tube adsorption/dsorption thermique/chromatographie en ph
20、ase gazeuse sur capillaire Partie 1: chantillonnage par pompage ENISO160171:2000ii ENISO160171:2000 iii Contents Page Foreword.iv 1 Scope 1 2 Normative references 2 3 Terms and definitions .2 4 Principle3 5 Reagents and materials 3 6 Apparatus .5 7 Sample tube conditioning.6 8 Calibration of pump.7
21、9 Sampling.7 10 Procedure .8 10.1 Safety precautions.8 10.2 Desorption and analysis .8 10.3 Calibration 9 10.4 Determination of sample concentration10 10.5 Determination of desorption efficiency.10 11 Calculations10 11.1 Mass concentration of analyte .10 11.2 Volume concentration of analyte .11 12 I
22、nterferences 11 13 Performance characteristics 11 14 Test report 12 15 Quality control12 Annex A (normative) Determination of breakthrough volumes from gas standards.21 Annex B (normative) Determination of breakthrough volume from the extrapolated retention volume.22 Annex C (informative) Descriptio
23、n of sorbent types .23 Annex D (informative) Guidance on sorbent selection .24 Annex E (informative) Guidance on sorbent use .25 Annex F (informative) Summary of data on overall uncertainty, precision, bias and storage26 Bibliography28 ENISO160171:2000iv Foreword ISO (the International Organization
24、for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has t
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