EN ISO 8780-4-1995 en Pigments and Extenders - Methods of Dispersion for Assessment of Dispersion Characteristics - Part 4 Dispersion Using a Bead Mill《颜料和稀释剂 色散特性评定用色散方法 第4部分 色散用压.pdf
《EN ISO 8780-4-1995 en Pigments and Extenders - Methods of Dispersion for Assessment of Dispersion Characteristics - Part 4 Dispersion Using a Bead Mill《颜料和稀释剂 色散特性评定用色散方法 第4部分 色散用压.pdf》由会员分享,可在线阅读,更多相关《EN ISO 8780-4-1995 en Pigments and Extenders - Methods of Dispersion for Assessment of Dispersion Characteristics - Part 4 Dispersion Using a Bead Mill《颜料和稀释剂 色散特性评定用色散方法 第4部分 色散用压.pdf(17页珍藏版)》请在麦多课文档分享上搜索。
1、- CEN EN*IS0*8780- 4 95 3404589 0308529 886 _._ A . BRITISH STANDARD Pigments and extenders - Methods of dispersion for assessment of dispersion characteristics Part 4. Dispersion using a bead mill The European Standard EN Is0 8780-4 : 1995 has the status of a British Standard 5s EN IS0 1780-4 : 199
2、5 d BS 3483 : Part D4 : 1991 National foreword This Part of BS 3483 has been prepared under the direction of the Pigments, Paints and Varnishes Standards Policy Committee. It is identical with IS0 8780-4 : 1990 Pigments and extenders - Methods of dispersion for assessment of dispersion characteristi
3、cs - Part 4 : Dispersion using a bead mill, published by the International Organization for Standardization (ISO). in 1994 the Eurpoean Committee for standardization (0 accepted Is0 8780-4 : 1990 as European standard EN Is0 878-4 : 1995. As a consequence of implementing the European standard this Br
4、itish standard is renumbered Bs EN ISO878O-4 and any refemce to BS 3483: part D4 should be read as a reference to Bs EN IS0 8780-4: Cross-references international standard Is0 842 : 1984 ISO 2431 : 1984 IS0 8780-1 : 1990 IS0 8781-1 : 1990 ISO8781-2 : 1990 ISO8781-3 : 1990 Cornsponding British Standa
5、d BS 4726 : 1986 Methods for samping raw mate is the rotational frequency, in revolutions per minute, of the shaft; n 1 *-u- Figure 2 - Effedive diameter of discs The type, number and diameter of the discs, the ge- ometry of the vessel and the effective peripheral speed of the revolving discs shall
6、be agreed on and shall be recorded in the test report NOTE 1 A vessel with a double wall to allow circulation of a liquid to control the temperature is recommended, and a lid with a central aperlure may also be provided. NOTE 2 The nominal capacity of the vessel will depend on the volume of the mill
7、 base. Examples are given in table 1. 2 CEN EN*IS0*8780- Y 95 m 3404589 0108537 952 m IS0 8780-4:1990(E) Nominal capacity of vessel Mill base Diameter Height of of vessel vessel ml mm mm rnl 50 50 70 125 1 O0 65 a5 250 volume i Table 1 - Mill base volume and dimensions of bead mill vessel 200 I 1 1
8、85 110 500 4.2 Grinding spheres, of a suitable type. Spheres of the same size and type shall be used for all the mill bases under simultaneous test. The type, mean diameter and density shall be agreed on and shall be recorded in the test report. IC the spheres have never been used, they shall be con
9、ditioned by stirring them in a mill base (see clause 7). for example Cor 60 min, and cleaned. NOTE 3 The diaineter, density and total mass of the grinding spheres have a significant effect on the disper- sion obtained Glass spheres of a mean diameter of 1 mm to 2 mm and a density of 2.6 gkm3 f 0.2 g
10、lcrn3 have been found lo be suitable Steel balls with a diameter of 2 mrn lo 3 mm. a density of about 7.8 gkm3 and a hard- ness on Mohs scale of 7 to 8 may also be used. 5 Binder system The binder system shall be agreed on between the interested parties. The lest report shall state the binder, the s
11、olvent and the concenlration of the binder in the solvent. as well as giving information on the rheological properties (for example viscosity or flow time) of the binder system. The same balch of binder system shall be used for all tests in the same series. 6 Sampling Take a representative sample of
12、 lhe product to he tested. as described in IS0 842 7 Mill base composition The viscosity o a mill base depends on !he binder demand of the pigment and its concentration in a given binder system. Preliminary experirrients shall therefore be carried oiit to ascertain a suitable mil! base composition T
13、he viscosity of the mill base during dispersion shall be such that the grinding spheres can move freely (see ctaiice i) while the bead mill is runciing This can be checked by obser- vation. For binder systems wiih flow times of 20 s to 40 s. determined with flow cup IS0 2431 No.6. the follow- ing pi
14、gment concentrations have been found to be suitable as starting points- pigments of low binder demand - pigment con- centration 25 Oh (ni;ni) lo 60 ?4 (rn/m); pigments of medium binder demand - pigmenl concentration 10 O b) a reference lo this part o IS0 8780; c) the items of supplementary informati
15、on referred to in annex A; d) any deviation from lhe procedure specified: e) the date(s) of the test. 4 CEN EN*ISO*780- 4 95 3404589 0308539 725 W . IS0 8780-4:1990(E) Annex A (normative) Required supplementary information The items of supplementary information listed in this annex shall be supplied
16、 as appropriate to enable lhe method to be carried out. its temperature (see 9.2). The information required should preferably be agreed between the interested parties and may be e) Pre-mixing lime (see 9 1) derived, in part or totally. from an international or national standard or other document rel
17、ated to the 9 Stirring times (see 9.2). product under lest g) Stabilization procediire (see 9 3) a) Type and complete details of the bead mill (see 4.1). h) De-aeration procedtire (see 9.4) b) Type. mean diameter. density and total mass of the grinding spheres (see 4.2). c) Binder system (see clause
18、 5). d) Composition of the mili base (see clame 7) and Annex ZA (normative) Normative references to international publications with their relevant European publications This European Standad mcoqxxates by dated or undateci reference, provisions from other publications. These normative references are
19、 cited at the appropriate piaces in the text and the publications are listed hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply to this European standard oniy when in- in it by amendment or revision. For unated references the latest edition of t
20、he publication referred to applies (including amendments). hblication Year IS0 8781-1 1990 IS0 8781-2 1990 IS0 87813 1990 Is0 87W1 1990 1Itk EN Year pigmatSandt?xecteristics part 3: Assessmatfnnn the &unge an gloss PigmenLSand-Melhodsofd.ispersiOnfn- ENIS878-1 1995 aswsmm of d.lspersion chamceristic
21、s W 1: htraluction pigmats and QtenderS- Mewds of assessment of EN IS0 8781-2 1995 EN IS0 8781-3 1995 Publication($) referred to See national foreword. CEN EN*ISO*8780- 4 95 = 3Y04589 0108540 447 Amd. No. BS 3483 : Part D4 : 1991 IS0 8780-4 : 1990 Date lkxt affected This British Standard, having bee
22、n prepared under the direction of the Pigments, Paints and Varnishes Standards Policy Committee, was published undei the authority of the Standards Board and comes into effect on 30 April I991 o BSI I991 The following ES1 references relate to the work on this standard: Coniiiiittee reference PVC/I D
23、raft for comment 86152356 M: ISBN O 5sO 19.537 6 9104-4-0.7k- U Committees responsible for this British Standard The preparation of this British Standard was entrusted by the Pigments, Paints and Varnishes Standards Policy Committee (PVC/-) to khnical Committee PVC/i, upon which the following bodies
24、 were represented: Aluminium Powder and Paste Association British Cement Association British Railways Board Chemical Industries Assaation oil and Colour Chemists Association Mntmakers Association of Great Britain Ltd. Titanium Pigment Manufacturers khnical Committee Zinc Development Association BSI,
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