ANSI ASTM C611-1998 Standard Test Method for Electrical Resistivity of Manufactured Carbon and Graphite Articles at Room Temperature.pdf

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1、Designation: C611 98 (Reapproved 2016) An American National StandardStandard Test Method forElectrical Resistivity of Manufactured Carbon and GraphiteArticles at Room Temperature1This standard is issued under the fixed designation C611; the number immediately following the designation indicates the

2、year oforiginal adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method covers the determination of the ele

3、c-trical resistivity of manufactured carbon and graphite articles atroom temperature.1.2 The values stated in SI units are to be regarded asstandard. No other units of measurement are included in thisstandard.1.3 This standard does not purport to address all of thesafety concerns, if any, associated

4、 with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Terminology2.1 Definitions:2.1.1 resistivitythe property of a material that determinesits resistance to

5、 the flow of an electrical current. It is defined asthe value of , in milliohm metres, as follows: 5 RA!/Lwhere:R = resistance of a specimen of the material of uniform crosssection, ohms,A = uniform cross section, mm2, andL = distance between potential contacts, mm.3. Significance and Use3.1 This te

6、st method provides a means of determining theelectrical resistivity of carbon or graphite specimens. The useof specimens that do not conform to the specimen sizelimitations described in the test method may result in analteration of test method accuracy.4. Apparatus4.1 The means for applying current

7、and potential terminalsto the specimen is specified in 5.2.3.1. A typical specimenholder is shown in Fig. 1.4.2 Bridge, Potentiometer, or Suitable Digital Voltmeter,with necessary accessories for making resistance measure-ments with a limit of error of less than 0.5 %. Fig. 2schematically depicts tw

8、o wiring diagrams that have beenfound satisfactory for this purpose.4.3 The means for measuring the dimensions of the speci-men should be adequate to determine its gage length and itsmean area of cross section, each within 0.5 %.5. Test Specimen5.1 The test specimen may be in the form of a strip, ro

9、d, bar,or tube.5.2 In order to determine the resistivity, each specimen shallconform to the following:5.2.1 The cross-sectional area shall be uniform within0.75 %. In general, the diameter of circular cross section, or thethickness and width of a strip specimen shall be determined bymicrometer measu

10、rements, and a sufficient number of mea-surements shall be made to obtain a mean cross-sectional areato within 0.5 %. The test specimen shall be machined to yieldplanar and parallel end faces. These faces shall be perpendicu-lar to the specimen length to within 0.001 mm mm. Allsurfaces shall have a

11、surface finish visually comparable to0.8 m rms. Reasonable care should be exercised to assure thatall edges are sharp and without chips or other flaws.5.2.2 The test specimen shall show no defects observablewith normal vision and shall be free of surface deposits.5.2.3 The minimum ratio of specimen

12、length to maximumcross-sectional dimension (width or diameter) shall be 6 : 1.5.2.3.1 The gage length may be measured by any scale thatwill give an accuracy of 60.5 % in the length measured. In thedirection of the length of the specimen, the dimension of eachpotential contact shall be not more than

13、0.5 % of the distancebetween the potential contacts. The minimum distance betweeneach potential contact and the adjacent current contact shall bethe maximum cross-sectional dimension (width or diameter) ofthe specimen. If knife edges are used, they shall be parallel toeach other and perpendicular to

14、 the longitudinal direction ofthe sample. The minimum ratio of gage length to maximumcross-sectional dimension (width or diameter) shall be 4 : 1.5.2.4 No dimension shall be smaller than five times thelength of the largest visible particle.1This test method is under the jurisdiction of ASTM Committe

15、e D02 onPetroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility ofSubcommittee D02.F0 on Manufactured Carbon and Graphite Products.Current edition approved Oct. 1, 2016. Published November 2016. Originallyapproved in 2005. Last previous edition approved in 2010 as C611 98 (

16、2010)1.DOI:10.1520/C0611-98R16.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States15.2.5 No joints or splices are permissible, unless this is thevariable under study.6. Conditioning6.1 The specimen shall be dried for a minimum of 2 h at11

17、0 C, cooled to room temperature in a desiccator, and storedin a desiccator until tested.7. Procedure7.1 Resistance MeasurementMeasure resistance with in-struments accurate to 60.5 % or less (see Note 1). To ensure acorrect reading, the reference standard and the test specimenmust be allowed to come

18、to the same temperature as thesurrounding medium.NOTE 1For resistance below 10 , a Kelvin bridge method may beused, and for higher resistance, a Wheatstone bridge method may be used.7.1.1 Clean the surface of the specimen at current andpotential contact points to obtain good electrical contact.Mount

19、 the sample in the test apparatus, apply current, andmeasure the voltage. Take four measurements, on each side ofa rectangular specimen, or at 90 (/2 radians) apart on a roundspecimen. Reverse the current direction and take four measure-ments again. Remove the specimen from the test apparatus,turn i

20、t end for end, replace it in the apparatus, and repeat themeasurements. The total of 16 measurements is recommendedto minimize errors due to contact potential and forward andreverse currents. Average all individual values of measuredresistance and use this value to calculate the resistivity.7.2 Heat

21、ing of SpecimenIn all resistance measurements,the measuring current raises the temperature of the specimenabove that of the surrounding medium. Therefore, take care tokeep the magnitude of the current low, and the time shortenough, so that changes in resistance cannot be detected. Themeasuring curre

22、nt shall be so small that the resistance of aspecimen is not changed, thereby, as much as 0.1 %. Thiscondition may be determined experimentally, or calculatedfrom the power expended and the surface area of the specimen.A specimen heating check should be run after each group ofsamples. If resistance

23、change exceeds 0.1 %, the sample shouldbe cooled to ambient temperature and rerun at a lowermeasuring current.7.3 A sample data collection work sheet that may be usedfor the testing is shown in Fig. 3.1Base block 12Wire gauze holder2Pivot block 13Pivot red3Current block adjustable 14Screw: sockethea

24、d4Current block stationary 15Roundhead screw5Clamp block 16Roundhead screw6Clamp screw 17Roundhead screw7Brush holder 18Screw, sockethead8Contacts 19Set screw9Current block support 20Neoprene10Current block guide 21Wire gauze11Pivot bracket 22Set screwNOTE 1Contacts for the voltage and current probe

25、s may be made through channels drilled in the brush holders (7) and the current blocks (3 and 4),respectively.FIG. 1 Typical Test ApparatusC611 98 (2016)28. Report8.1 Report the following:8.1.1 Identification and previous history of the testspecimen,8.1.2 Sample orientation,8.1.3 Temperature of surr

26、ounding medium,8.1.4 Dimensions of specimen used,8.1.5 Method of measuring resistance, including gagelength and probe location,8.1.6 Value of resistance or potential plus the currentreadings, and8.1.7 Calculated value of resistivity.9. Precision and Bias29.1 A round-robin test series was run to dete

27、rmine theprecision and bias. The results of evaluating 20 test specimensof two different grades from 9 laboratories are as follows:Within-lab variability 0.75 %Between-lab variability 2.5 %9.2 The within-lab variability is a combination of both testerror and material variability since repetitious me

28、asurementswere not made on single specimens within a laboratory.Material variability was, however, minimized by normalizingthe results to values averaged from consistent results from fivelaboratories. This yielded the estimate of a fairly small within-laboratory variability from 0.5 % to 0.75 % whic

29、h still includesa minor material variability.9.3 Homogeneity of variance by the sensitive Barletts testwas not indicated, most likely, because of the very smallwithin-laboratory variance and sensitivity to non-normality.9.4 The between-lab variability estimation was made on themeasurement of the sam

30、e specimen between laboratories withthe obvious exception of the results from Laboratory A. Theresults still included some material variability as the resistivityvaries to some extent along the length of the specimens.9.5 The between-lab variability is fairly small and is prob-ably a result of a min

31、or lack of precision in the lengthmeasurement between voltage contacts on the specimen. Thissmall variability could be further reduced by the use of auniform standard specimen used to periodically check the2Supporting data have been filed at ASTM International Headquarters and maybe obtained by requ

32、esting Research Report RR:C05-1012.NOTE 1Adjustable, regulated dc power supplyline and load regulation to 0.1 % and ripple and noise 0.1 %.FIG. 2 Typical Schematic for Resistivity MeasurementsC611 98 (2016)3resistivity measurement apparatus. The results were essentiallyunchanged over the range of 17

33、 to 41 micro-ohm metres inelectrical resistivity.9.6 In effect, the overall conclusion is that this test methodwill yield repeatable test results giving a good estimation of theelectrical resistivity of a material as intended by the standardmethod of test.NOTE 1The sample history, ambient temperatur

34、e, and probe position should be recorded for each sample on a separate sheet.NOTE 2A specimen heating check should be run after each group of samples. If resistance change exceeds 0.1 %, the sample should be cooled toambient temperature and rerun at a lower measuring current.NOTE 3Remove the specime

35、n from test apparatus, turn end for end and replace the specimen in the test apparatus.FIG. 3 Electrical Resistivity WorksheetC611 98 (2016)4ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this

36、 standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five year

37、s andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committ

38、ee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428

39、-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 98 (2016)5