ASTM D2486-2006(2012)e1 Standard Test Methods for Scrub Resistance of Wall Paints《壁漆的耐擦洗标准试验方法》.pdf

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1、Designation: D2486 06 (Reapproved 2012)1Standard Test Methods forScrub Resistance of Wall Paints1This standard is issued under the fixed designation D2486; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision.

2、A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.1NOTEFootnotes in 6.3.1 were editorially updated in February 201

3、2.1. Scope1.1 These test methods cover a procedure for determiningthe resistance of wall paints to erosion caused by scrubbing,referred to herein after as “scrub resistance.”1.2 Two test methods are covered as follows:1.2.1 Test Method ACycles-to-failure obtained on testpaint.1.2.2 Test Method BRati

4、o expressed as a percentage ofcycles-to-failure obtained on the test paint to that obtained ona concurrent run with a known reference paint.1.3 The values stated in SI units are to be regarded as thestandard. The values given in parentheses are for informationonly.1.4 This standard does not purport

5、to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D3924 S

6、pecification for Environment for Conditioning andTesting Paint, Varnish, Lacquer, and Related MaterialsD4213 Test Method for Scrub Resistance of Paints byAbrasion Weight Loss3. Summary of Test Method3.1 In Test Method A, the test paint is applied to a blackplastic panel. After curing, the coated pan

7、el is placed over a12.7 wide by 0.25-mm thick (12-in. by 10-mil) shim and heldin place on a drawdown plate in a washability machine bymeans of a gasketed frame. The coated panel is then scrubbedwith a bristle brush and an abrasive scrub medium until thepaint film is removed in one continuous thin li

8、ne across theshim.3.2 In Test Method B, the test paint and a reference paint areapplied simultaneously perpendicular to the length of the blackplastic panel. After curing, the coated panel is placed over two12.7 by 0.25-mm (12-in. by 10-ml) shims that are positionedunder each coating. The coatings a

9、re then scrubbed with abristle brush and an abrasive scrub medium until each paintfilm is removed in one continuous thin line across its ownshim.4. Significance and Use4.1 Paints often become soiled, especially near doorways,windows, and in work and play areas. These test methods coverthe determinat

10、ion of the relative resistance of different paints toerosion when repeatedly scrubbed during the life of the paint.4.2 Test Method D4213 is a similar scrub resistance testusing a weight-loss technique and reporting volumetric filmerosion rates.4.3 Test Method A measures scrub resistance by the tradi

11、-tional cycles-to-failure concept. Poor correlation in scrubtesting can be attributable to among other things variations inthe stiffness of the brush bristles, condition of washabilitytester, application and drying conditions. In an attempt toimprove reproducibility, Test Method B has been developed

12、.5. Apparatus5.1 Straight Line Washability Machine.5.1.1 Accessory Apparatus: (see Figs. 1 and 2).5.1.1.1 Nylon Bristle Brush and Accessories,(total weight454 6 10 g).5.1.1.2 Drawdown Plate, 454 by 165 by 6.3 mm (1778 by612 by14 in.).5.1.1.3 Brass Shims, 12.7- by 0.25-mm (12-in. by 10-mils).Its leng

13、th can be fitted to the width of the drawdown plate.5.2 Film Applicator, having 0.18-mm (7-mil) clearance and6.25-mm (14-in.) edge and width of 135 mm (514-in.).1These test methods are under the jurisdiction of ASTM Committee D01 onPaint and Related Coatings, Materials, and Applications and are the

14、directresponsibility of Subcommittee D01.42 on Architectural Coatings.Current edition approved Feb. 1, 2012. Published February 2012. Originallyapproved in 1966. Last previous edition approved in 2006 as D2486 06. DOI:10.1520/D2486-06R12E01.2For referenced ASTM standards, visit the ASTM website, www

15、.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.6. Re

16、agents and Materials6.1 Purity of ReagentsReagent grade chemicals shall beused in all tests.6.2 Black Plastic Panels.3,46.3 Abrasive Scrub Medium.4,56.3.1 Laboratory standardized abrasive scrub medium con-sisting of the following:gramsWater, distilled or deionized 49.4AHydroxyethyl cellulose4,60.8Am

17、monium hydroxide, 28 % 0.1Detergent4,72.0Trisodium phosphate, anhydrous 2.0Silica4,845.0Acetic acid (glacial) 0.7BPreservative4,90.03g_AAdjust to achieve viscosity of 110 to 120 Krebs units before use.BVary to achieve a pH of 9.5 to 10.6.4 Reference paint when using Test Method B.3Dull black plastic

18、 panels, P-121-10N, 165 by 432 by 0.25 mm (612 by 17 in.by 10 mils) manufactured by The Leneta Co., 15 Whitney Rd., Mahwah, NJ 07430were used in the original development of this standard in order to get the results inthese test methods.4If you are aware of alternative suppliers, please provide this

19、information toASTM International Headquarters. Your comments will receive careful consider-ation at a meeting of the responsible technical committee,1which you may attend.5The sole source of supply of the abrasive scrub medium known to thecommittee at this time is The Leneta Company.6Cellosize QP-44

20、00H, The Dow Chemical Company, Midland, Michigan, wasused in developing the Precision and Bias statement. Other equivalent molecularweight cellulosic thickeners can be used such as Natrosol 250 MR, AshlandAqualon, Wilmington, Delaware.7The sole source of supply of the Triton X-100 detergent known to

21、 thecommittee at this time is The Dow Chemical Company, Midland, Michigan.8The sole source of supply of the Imsil 45 known to the committee at this timeis Unimin Specialty Minerals Inc., 258 Elm St., New Canaan, CT 06840.9The preservative package recommended is BIT, 1,2Benzisothiazol-3(2H)-one.There

22、 are several suppliers who offer BIT-based agents.FIG. 1 Accessory Apparatus for Scrub TestFIG. 2 Accessory Apparatus for Scrub TestD2486 06 (2012)127. Preparation of Apparatus7.1 Washability MachineThe straight line washabilitymachine should be leveled before use and operated at 37 6 1cycles per mi

23、nute.7.2 BrushReplace the brush when the bristles have be-come worn to a point that the bristles extend less than 15 mm(58 in.) from the block. Mark the ends of the brush to ensure itis oriented in the same direction for each use.7.2.1 Brushes (that are in frequent use)Brushes that are infrequent us

24、e shall be stored in water. Each time before startingthe first test of the day, remove the brush and rinse in water,then precondition the brush, by running it for 400 cycles on ascrub panel, after which it is ready for test work.7.2.2 Brushes (that are not in regular use)Brushes thatwill not be used

25、 on a regular basis shall be washed outthoroughly in water after their last use and stored with thebristling side up under ambient conditions. Before being usedagain, the brush should be soaked in water for at least 24 h.Precondition the brush as directed in 7.2.1 before starting thetest work.7.3 Br

26、ush HolderFor washability testers that include aseparate brush holder, insert a 3.2-mm (18-in.) thick rubber matin the holder above the brush block. When in operation, thismat allows the brush to ride evenly on the paint surface withouttilting. The brush must fit loosely in the holder. Mount thebrus

27、h in the holder being sure that the mat is in place above thebrush block and that the brush and holder are always in thesame position.TEST METHOD A8. Procedure8.1 Stir the test paint thoroughly and strain to remove allskins and particles. Make three drawdowns of each paint. Drawdown the paint on the

28、 black plastic panel using the sameoperator and same 0.18-mm (7.0-mil) clearance film applicator.The time for application should be fairly slow 3 to 4 s fromend to end to prevent formation of pinholes or holidays in thefilm. Air dry in a horizontal position for 7 days in anconditioning chamber at 23

29、 6 2C (73.5 6 3.5F) and 50 65 % relative humidity in accordance with Specification D3924.8.2 Soak the brush in water overnight. Clean the plate andset it in the pan of the washability tester. Ensure that the shimis smooth and free of burrs and placed perpendicular to the pathof the brush. Wipe the t

30、est panel carefully and place it on topof the shimmed plate with the painted side up. Be sure thatthere are no defects in the film above the shim and that the testarea is level. Place the frame over the drawdown being surethat the entire gasket is on the painted surface. Clamp thegasket in place. Th

31、e clamps should be tight enough to ensureclose contact, but not tight enough to cause warping of thepanel.8.3 Before beginning the test, it should be confirmed that thebrush has been preconditioned for 400 cycles as outlined in7.2.1. Remove the brush and shake vigorously to remove anyexcess water. S

32、tir the abrasive scrub medium and spread 10 guniformly over the brush bristles. Place the brush at one end ofthe path. Wet the panel with 5 mL of water in the path of thebrush.8.4 Start the test. After each 400 cycles before failure,remove the brush (do not rinse), add 10 g of stirred abrasivescrub

33、medium and place 5 mL of water on the path of the brushbefore continuing.8.5 Record the number of cycles to remove one continuousthin line of paint film across the 12.7-mm (12-in.) width of theshim. Stop the machine and wipe off the shim area todetermine, if necessary, if the end point is achieved.8

34、.6 Test two of the drawdowns. If the two results differ bymore than 30 % of the average, test the third drawdown. If oneof the three results is obviously discrepant, discard it, thenaverage the results from the remaining drawdowns.TEST METHOD B9. Procedure9.1 Stir the test paint and reference paint

35、thoroughly andstrain to remove all skins and particles. Draw down the test andreference paints side by side perpendicular to the length of thepanel following procedures outlined in 8.1. Prepare threedrawdowns for each test/reference paint. The paints should bedrawn down simultaneously and the painte

36、d portion should bein the middle of the chart. Air dry in a horizontal position for7 days at standard conditions.9.2 Soak the brush in water overnight. Clean the plate andset it in the pan of the washability machine. Centrally place twoshims, one each under the test paint and one under thereference

37、paint drawdown areas on the chart. Wipe the testpanel carefully and place it on top of the shimmed plate withthe painted side up. Be sure that there are no defects in the filmabove the shims and that the test areas are level. Place thegasket over the painted surface and clamp in place.9.3 Remove the

38、 brush and shake it vigorously to removeany excess water. Before testing, the brush shall be conditionedfor 400 cycles as outlined in 7.2.1. Follow procedures outlinedin 8.3 and 8.4. It is recommended that the first two panels to betested are prepared by altering the position of the referencepaint,

39、that is, one panel has the reference paint on the right, andthe second panel has the reference paint on the left.9.4 Record respectively the number of cycles to remove onecontinuous thin line of paint film from both the test andreference paints across the 12.7-mm (12-in.) width of each ofthe shims.

40、Stop the machine and wipe off the shim areas todetermine, if necessary, if each end point is achieved.9.5 Test two of the drawdowns. If the two results differ bymore than 30 %, test the third drawdown. If one of the threeresults is obviously discrepant, discard it, then average theresults from the r

41、emaining drawdowns.10. Report10.1 Report the following information:10.1.1 When using Test Method A, report the mean numberof cycles to failure.10.1.2 When using Test Method B, report a percentage asfollows:Cycles for test paintCycles for reference paint3100 (1)D2486 06 (2012)13if:Result is 100 %, te

42、st paint has better scrub resistance thanreference paint.if:Result is 100 %, test paint has poorer scrub resistance thanreference paint.10.1.3 Method used (Test Method A or Test Method B).10.1.4 Referenced paint used, if using Test Method B.10.1.5 Outline any deviations from standard procedures.11.

43、Precision and Bias11.1 PrecisionIn an interlaboratory study of these testmethods, scrub resistance was recorded in five laboratoriesusing three coatings. The following criteria should be used forjudging the acceptability of results of scrub resistance tests ata 95 % confidence level.Test Method A11.

44、1.1 RepeatabilityDuplicate results by a single operatorshould be considered suspect if they differ by more than 30 %of their mean value.11.1.2 ReproducibilityTwo results (each the mean ofduplicate measurements) obtained by operators in differentlaboratories should be considered suspect if they diffe

45、r by morethan 58 % of their mean.Test Method B11.1.3 On the basis of an interlaboratory study in whichoperators in five laboratories tested five coatings, includingboth flat and semi-gloss coatings, the following criteria shouldbe used for judging the acceptability of the results at the 95 %confiden

46、ce level:11.1.3.1 RepeatabilityTwo results (each the mean of du-plicate measurements) obtained by the same operator should beconsidered suspect if they differ by more than 25 % of theirmean value.11.1.3.2 ReproducibilityTwo results (each the mean ofduplicate measurements) obtained by operators in di

47、fferentlaboratories should be considered suspect if they differ by morethan 58 % of their mean.11.2 BiasBias is not applicable to these test methods.12. Keywords12.1 scrub resistance; wet abrasion resistanceASTM International takes no position respecting the validity of any patent rights asserted in

48、 connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the re

49、sponsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the addres