ASTM E353-2014 3724 Standard Test Methods for Chemical Analysis of Stainless Heat-Resisting Maraging and Other Similar Chromium-Nickel-Iron Alloys《不锈钢 耐热钢 马氏体钢和其它类似的铬镍铁合金化学分析的标准试验方.pdf
《ASTM E353-2014 3724 Standard Test Methods for Chemical Analysis of Stainless Heat-Resisting Maraging and Other Similar Chromium-Nickel-Iron Alloys《不锈钢 耐热钢 马氏体钢和其它类似的铬镍铁合金化学分析的标准试验方.pdf》由会员分享,可在线阅读,更多相关《ASTM E353-2014 3724 Standard Test Methods for Chemical Analysis of Stainless Heat-Resisting Maraging and Other Similar Chromium-Nickel-Iron Alloys《不锈钢 耐热钢 马氏体钢和其它类似的铬镍铁合金化学分析的标准试验方.pdf(44页珍藏版)》请在麦多课文档分享上搜索。
1、Designation: E353 14Standard Test Methods forChemical Analysis of Stainless, Heat-Resisting, Maraging,and Other Similar Chromium-Nickel-Iron Alloys1This standard is issued under the fixed designation E353; the number immediately following the designation indicates the year oforiginal adoption or, in
2、 the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 These test methods cover the chemical analysis ofstainless, heat-resisting, maragin
3、g, and other similarchromium-nickel-iron alloys having chemical compositionswithin the following limits:Element Composition Range, %Aluminum 0.002 to 5.50Boron 0.001 to 0.20Carbon 0.01 to 1.50Chromium 0.01 to 35.00Cobalt 0.01 to 15.00Niobium 0.01 to 4.00Copper 0.01 to 5.00Lead 0.001 to 0.50Manganese
4、 0.01 to 20.00Molybdenum 0.01 to 7.00Nickel 0.01 to 48.00Nitrogen 0.001 to 0.50Phosphorus 0.002 to 0.35Selenium 0.01 to 0.50Silicon 0.01 to 4.00Sulfur 0.002 to 0.50Tantalum 0.01 to 0.80Tin 0.001 to 0.05Titanium 0.01 to 4.50Tungsten 0.01 to 4.50Vanadium 0.005 to 1.00Zirconium 0.001 to 0.201.2 The tes
5、t methods in this standard are contained in thesections indicated below:SectionsAluminum, Total, by the 8-QuinolinolGravimetric Method (0.20 % to7.00 %)119Aluminum, Total, by the 8-QuinolinolSpectrophotometric Method (0.003 %to 0.20 %)71Carbon, Total, by theCombustionThermal ConductivityMethodDiscon
6、tinuedCarbon, Total, by the CombustionGravimetric Method (0.05 % to1.50 %)DiscontinuedChromium by the Atomic AbsorptionMethod (0.006 % to 1.00 %)202SectionsChromium by the PeroxydisulfateOxidationTitration Method (0.10 %to 35.00 %)212Chromium by the Peroxydisulfate-Oxidation Titrimetric MethodDiscon
7、tinuedCobalt by the Ion-ExchangePotentiometric TitrationMethod(2%to15%)53Cobalt by the Nitroso-R-SaltSpectrophotometric Method (0.01 %to 5.0 %)61Copper by the NeocuproineSpectrophotometric Method (0.01 %to 5.00) %)109Copper by the Sulfide Precipitation-Electrodeposition Gravimetric Method(0.01 % to
8、5.00 %)82Lead by the Ion-Exchange-AtomicAbsorption Method (0.001 % to0.50 %)127Manganese by the PeriodateSpectrophotometric Method (0.01 %to 5.00 %)8Molybdenum by the Ion Exchange8-Hydroxyquinoline Gravimetric Method242Molybdenum by the SpectrophotometricMethod (0.01 % to 1.50 %)190Nickel by the Dim
9、ethylglyoximeGravimetric Method (0.1 % to 48.0 %)172Phosphorus by the Alkalimetric Method(0.02 % to 0.35 %)164Phosphorus by the Molybdenum BlueSpectrophotometric Method (0.002 %to 0.35 %)18Silicon by the Gravimetric Method (0.05%to4.00%)46Sulfur by the Gravimetric Method DiscontinuedSulfur by the Co
10、mbustion-IodateTitration Method (0.005 % to 0.5 %)DiscontinuedSulfur by the ChromatographicGravimetric MethodDiscontinuedTin by the Solvent ExtractionAtomicAbsorption Method (0.002 % to0.10 %)180Tin by the Sulfide-Iodometric TitrationMethod (0.01 % to 0.05 %)90Titanium, Total, by theDiantipyrylmetha
11、neSpectrophotometric Method (0.01 %to 0.35 %)231Vanadium by the Atomic AbsorptionMethod (0.006 % to 0.15 %)2211.3 Test methods for the determination of carbon and sulfurnot included in this standard can be found in Test MethodsE1019.1These test methods are under the jurisdiction of ASTM Committee E0
12、1 onAnalytical Chemistry for Metals, Ores, and Related Materials and are the directresponsibility of Subcommittee E01.01 on Iron, Steel, and Ferroalloys.Current edition approved Sept. 15, 2014. Published November 2014. Originallyapproved in 1968. Last previous edition approved in 2006 as E353 93 (20
13、06).DOI: 10.1520/E0353-14.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States11.4 Some of the composition ranges given in 1.1 are toobroad to be covered by a single test method and therefore thisstandard contains multiple test methods for
14、 some elements.The user must select the proper test method by matching theinformation given in the Scope and Interference sections ofeach method with the composition of the alloy to be analyzed.1.5 The values stated in SI units are to be regarded asstandard.1.6 This standard does not purport to addr
15、ess all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use. Specific hazardsstatements are given in Section 6 and in
16、 special “Warning”paragraphs throughout these test methods.2. Referenced Documents2.1 ASTM Standards:2D1193 Specification for Reagent WaterE29 Practice for Using Significant Digits in Test Data toDetermine Conformance with SpecificationsE50 Practices for Apparatus, Reagents, and Safety Consid-eratio
17、ns for Chemical Analysis of Metals, Ores, andRelated MaterialsE60 Practice for Analysis of Metals, Ores, and RelatedMaterials by SpectrophotometryE135 Terminology Relating to Analytical Chemistry forMetals, Ores, and Related MaterialsE173 Practice for Conducting Interlaboratory Studies ofMethods for
18、 Chemical Analysis of Metals (Withdrawn1998)3E350 Test Methods for Chemical Analysis of Carbon Steel,Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, andWrought IronE351 Test Methods for ChemicalAnalysis of Cast IronAllTypesE352 Test Methods for ChemicalAnalysis of Tool Steels andOther Similar
19、 Medium- and High-Alloy SteelsE354 Test Methods for Chemical Analysis of High-Temperature, Electrical, Magnetic, and Other Similar Iron,Nickel, and Cobalt AlloysE882 Guide for Accountability and Quality Control in theChemical Analysis LaboratoryE1019 Test Methods for Determination of Carbon, Sulfur,
20、Nitrogen, and Oxygen in Steel, Iron, Nickel, and CobaltAlloys by Various Combustion and Fusion TechniquesE1024 Guide for Chemical Analysis of Metals and MetalBearing Ores by Flame Atomic Absorption Spectropho-tometry (Withdrawn 2004)3E1601 Practice for Conducting an Interlaboratory Study toEvaluate
21、the Performance of an Analytical MethodE1806 Practice for Sampling Steel and Iron for Determina-tion of Chemical Composition2.2 Other Document:ISO 5725 Precision of Test MethodsDetermination ofRepeatability and Reproducibility for Inter-LaboratoryTests43. Terminology3.1 For definitions of terms used
22、 in these test methods, referto Terminology E135.4. Significance and Use4.1 These test methods for the chemical analysis of metalsand alloys are primarily intended as referee methods to testsuch materials for compliance with compositionalspecifications, particularly those under the jurisdiction ofAS
23、TM Committee A1 on Steel, Stainless Steel, and RelatedAlloys. It is assumed that all who use these test methods willbe trained analysts capable of performing common laboratoryprocedures skillfully and safely. It is expected that work will beperformed in a properly equipped laboratory under appropria
24、tequality control practices such as those described in GuideE882.5. Apparatus, Reagents, and Instrumental Practices5.1 ApparatusSpecialized apparatus requirements arelisted in the “Apparatus” Section in each method.5.2 Reagents:5.2.1 Purity of ReagentsUnless otherwise indicated, allreagents used in
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