ASTM D4762-2004 Standard Guide for Testing Polymer Matrix Composite Materials《聚合基质合成材料的试验用标准指南》.pdf

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1、Designation: D 4762 04Standard Guide forTesting Polymer Matrix Composite Materials1This standard is issued under the fixed designation D 4762; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in p

2、arentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.1. Scope1.1 This guide summarizes the application of ASTM stan-dard test methods (and other supporting standards) tocontinuous-fiber reinforced polymer matri

3、x composite materi-als. The most commonly used or most applicable ASTMstandards are included, emphasizing use of standards of Com-mittee D30 on Composite Materials.1.2 This guide does not cover all possible standards thatcould apply to polymer matrix composites and restricts discus-sion to the docum

4、ented scope. Commonly used but non-standard industry extensions of test method scopes, such asapplication of static test methods to fatigue testing, are notdiscussed. A more complete summary of general compositetesting standards, including non-ASTM test methods, is in-cluded in the Composite Materia

5、ls Handbook (MIL-HDBK-17).2Additional specific recommendations for testing textile(fabric, braided) composites are contained in Guide D 6856.1.3 This guide does not specify a system of measurement;the systems specified within each of the referenced standardsshall apply as appropriate. Note that the

6、referenced standardsof ASTM Committee D30 are either SI-only or combined-unitstandards with SI units listed first.1.4 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate s

7、afety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:32.1.1 Standards of Committee D30 on Composite MaterialsC 393 Test Method for Flexural Properties of SandwichConstructionsC 480 Test Method for Flexure Creep o

8、f Sandwich Con-structionsC 613/C 613M Test Method for Constituent Content ofComposite Prepreg by Soxhlet ExtractionD 2344/D 2344M Test Method for Short Beam Strength ofComposite Materials and Their LaminatesD 3039/D 3039M Test Method for Tensile Properties ofPolymer Matrix Composite MaterialsD 3171

9、Test Method for Constituent Content of CompositeMaterialsD 3410/D 3410M Test Method for Compressive Propertiesof Polymer Matrix Composite Materials with UnsupportedGage Section by Shear LoadingD 3479/D 3479M Test Method for Tension-Tension Fatigueof Polymer Matrix Composite MaterialsD 3518/D 3518M T

10、est Method for In-Plane Shear Responseof Polymer Matrix Composite Materials by Tensile Test ofa 645 LaminateD 3529/D 3529M Test Method for Matrix Solids Contentand Matrix Content of Composite PrepregD 3530/D 3530M Test Method for Volatiles Content ofComposite Material PrepregD 3531 Test Method for R

11、esin Flow of Carbon Fiber-EpoxyPrepregD 3532 Test Method for Gel Time of Carbon Fiber-EpoxyPrepregD 3544 Guide for Reporting Test Methods and Results onHigh Modulus Fibers4D 3800 Test Method for Density of High-Modulus FibersD 3878 Terminology of Composite MaterialsD 4018 Test Methods for Properties

12、 of Continuous FilamentCarbon and Graphite Fiber TowsD 4102 Test Method for Thermal Oxidative Resistance ofCarbon FibersD 4255/D 4255M Test Method for In-Plane Shear Proper-ties of Polymer Matrix Composite Materials by the RailShear MethodD 5229/D 5229M Test Method for Moisture AbsorptionProperties

13、and Equilibrium Conditioning of Polymer Ma-trix Composite MaterialsD 5379/D 5379M Test Method for Shear Properties ofComposite Materials by the V-Notched Beam Method1This guide is under the jurisdiction of ASTM Committee D30 on CompositeMaterials and is the direct responsibility of Subcommittee D30.

14、01 on Editorial andResource Standards.Current edition approved May 1, 2004. Published May 2004. Originallyapproved in 1988. Last previous edition approved in 2001 as D 4762 88 (2001).2Available from ASTM, and also from the U.S. DoD Standardization DocumentsOrder Desk, Bldg. 4 Section D, 700 Robbins

15、Ave., Philadelphia, PA 19111-5094,Attn: NPODS.3For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.4Withdrawn.1Cop

16、yright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.D 5448/D 5448M Test Method for In-Plane Shear Proper-ties of Hoop Wound Polymer Matrix Composite CylindersD 5449/D 5449M Test Method for Transverse CompressiveProperties of Hoop Wound Polym

17、er Matrix CompositeCylindersD 5450/D 5450M Test Method for Transverse Tensile Prop-erties of Hoop Wound Polymer Matrix Composite Cylin-dersD 5467/D 5467M Test Method for Compressive Propertiesof Unidirectional Polymer Matrix Composites Using aSandwich BeamD 5528 Test Method for Mode I Interlaminar F

18、ractureToughness of Unidirectional Fiber-Reinforced PolymerMatrix CompositesD 5687/D 5687M Guide for Preparation of Flat CompositePanels With Processing Guidelines for Specimen Prepara-tionD 5766/D 5766M Test Method for Open Hole TensileStrength of Polymer Matrix Composite LaminatesD 5961/D 5961M Te

19、st Method for Bearing Response ofPolymer Matrix Composite LaminatesD 6115 Test Method for Mode I Fatigue DelaminationGrowth Onset of Unidirectional Fiber-ReinforcedPolymer-Matrix CompositesD 6264 Test Method for Measuring the Damage Resistanceof a Fiber-Reinforced Polymer-Matrix Composite to aConcen

20、trated Quasi-Static Indentation ForceD 6415 Test Method for Measuring the Curved BeamStrength of a Fiber-Reinforced Polymer-Matrix CompositeD 6416/D 6416M Test Method for Two-Dimensional Flex-ural Properties of Simply Supported Sandwich CompositePlates Subjected to a Distributed LoadD 6484/D 6484M T

21、est Method for Open-Hole CompressiveStrength of Polymer Matrix Composite LaminatesD 6507 Practice for Fiber Reinforcement Orientation Codesfor Composite MaterialsD 6641/D 6641M Test Method for Determining the Com-pressive Properties of Polymer Matrix Composite Materi-als Using the Combined Loading C

22、ompression (CLC) TestFixtureD 6671 Test Method for Mixed Mode I-Mode II Interlami-nar Fracture Toughness of Unidirectional Fiber ReinforcedPolymer Matrix CompositesD 6742/D 6742M Practice for Filled-Hole Tension andCompression Testing of Polymer Matrix Composite Lami-natesD 6856 Guide for Testing Fa

23、bric Reinforced Textile Com-posite MaterialsD 6873 Practice for Bearing Fatigue Testing of PolymerMatrix Composite LaminatesE 1309 Guide for the Identification of Fiber-ReinforcedPolymer Matrix Composite Materials in DatabasesE 1434 Guide for Recording Mechanical Test Data of Fiber-Reinforced Compos

24、ite Materials in DatabasesE 1471 Guide for the Identification of Fibers, Fillers, andCore Materials in Computerized Material Property Data-bases2.1.2 Standards of Committee D20 on PlasticsC 581 Practice for Determining Chemical Resistance ofThermosetting Resins Used in Glass-Fiber-ReinforcedStructur

25、es Intended for Liquid ServiceD 256 Test Method for Determining the Izod PendulumImpact Resistance of PlasticsD 543 Test Method for Evaluating the Resistance of Plasticsto Chemical ReagentsD 618 Practice for Conditioning Plastics for TestingD 638 Test Method for Tensile Properties of PlasticsD 648 T

26、est Method for Deflection Temperature of PlasticsUnder Flexural Load in the Edgewise PositionD 671 Test Method for Flexural Fatigue of Plastics byConstant-Amplitude-of- Force4D 695 Test Method for Compressive Properties of RigidPlasticsD 696 Test Method for Coefficient of Linear Thermal Ex-pansion o

27、f Plastics Between -30C and 30C With aVitreous Silica DilatometerD 790 Test Methods for Flexural Properties of Unreinforcedand Reinforced Plastics and Electrical Insulating MaterialsD 792 Test Methods for Density and Specific Gravity (Rela-tive Density) of Plastics by DisplacementD 953 Test Method f

28、or Bearing Strength of PlasticsD 1505 Test Method for Density of Plastics by the Density-Gradient TechniqueD 1822 Test Method for Tensile-Impact Energy to BreakPlastics and Electrical Insulating MaterialsD 2471 Test Method for Gel Time and Peak ExothermicTemperature of Reacting Thermosetting ResinsD

29、 2583 Test Method for Indentation Hardness of RigidPlastics by Means of a Barcol ImpressorD 2584 Test Method for Ignition Loss of Cured ReinforcedResinsD 2734 Test Method for Void Content of Reinforced Plas-ticsD 2990 Test Methods for Tensile, Compressive, and Flex-ural Creep and Creep-Rupture of Pl

30、asticsD 3418 Test Method for Transition Temperatures of Poly-mers by Differential Scanning CalorimetryD 3846 Test Method for In-Plane Shear Strength of Rein-forced PlasticsD 4065 Practice for Plastics: Dynamical Mechanical Prop-erties: Determination and Report of ProceduresD 4473 Test Method for Pla

31、stics: Dynamic MechanicalProperties: Cure BehaviorD 5083 Test Method for Tensile Properties of ReinforcedThermosetting Plastics Using Straight-Sided SpecimensD 6272 Test Method for Flexural Properties of Unrein-forced and Reinforced Plastics and Electrical InsulatingMaterials by Four-Point Bending2.

32、1.3 Standards of Other ASTM CommitteesE 228 Test Method for Linear Thermal Expansion of SolidMaterials With a Vitreous Silica DilatometerE 289 Test Method for Linear Thermal Expansion of RigidSolids with InterferometryE 1269 Test Method for Determining Specific Heat Capac-ity by Differential Scannin

33、g CalorimetryD4762042E 1461 Test Method for Thermal Diffusivity of Solids bythe Flash MethodE 1922 Test Method for Translaminar Fracture Toughnessof Laminated Polymer Matrix Composite Materials3. Terminology3.1 Definitions related to composite materials are defined inTerminology D 3878.3.2 Symbology

34、 for specifying the orientation and stackingsequence of a composite laminate is defined in PracticeD 6507.3.3 For purposes of this document, “low modulus” compos-ites are defined as being reinforced with fibers having amodulus #20 GPa (#3.0 3 106psi), while “high-modulus”composites are reinforced wi

35、th fiber having a modulus 20GPa (3.0 3 106psi).4. Significance and Use4.1 This guide is intended to aid in the selection of standardsfor polymer matrix composite materials. It specifically sum-marizes the application of standards from ASTM CommitteeD30 on Composite Materials that apply to continuous

36、-fiberreinforced polymer matrix composite materials. For referenceand comparison, many commonly used or applicable ASTMstandards from other ASTM Committees are also included.5. Standard Specimen Preparation5.1 Preparation of polymer matrix composite test specimensis described in Guide D 5687.6. Stan

37、dard Test Methods6.1 ASTM test methods for the evaluation of polymermatrix composites are summarized in Tables 1-5. Advantages,disadvantages, and other comments for each test method areincluded where appropriate. Where possible, a single preferredtest method is identified.TEST METHOD CATEGORY TABLEL

38、amina/Laminate Static Properties Table 1Lamina/Laminate Dynamic Properties Table 2Laminate/Structural Response Table 3Constituent/Precursor/Thermophysical Properties Table 4Environmental Conditioning/Resistance Table 57. Standard Data Reporting7.1 Constituent Material DescriptionData reporting ofthe

39、 description of composite material constituents is docu-mented in Guide E 1471.7.2 Composite Material DescriptionData reporting of thedescription of composite materials is documented in GuideE 1309.7.3 Composite Material Test DataData reporting of me-chanical test data results for composite material

40、s is docu-mented in Guide E 1434.8. Keywords8.1 bearing strength; coefficient of thermal expansion; com-posite materials; composites; compression; compressivestrength; constituent content; crack-growth testing; creep;creep strength; CTE; curved-beam strength; damage; datarecording; data records; del

41、amination; density; elastic modu-lus; fatigue; fiber; fiber volume; filament; filled-hole compres-sion strength; filled-hole tensile strength; flatwise tensilestrength; flexural modulus; flexure; fracture; fracture tough-ness; gel time; glass transition temperature; hoop-wound;impact; impact strengt

42、h; lamina; laminate; matrix content;mixed mode; mode I; mode II; mode III; modulus of elasticity;moisture content; moisture diffusivity; Poissons ratio; OHC;OHT; open-hole compressive strength; open-hole tensilestrength; out-of-plane compressive strength; out-of-plane shearstrength; out-of-plane ten

43、sile strength; panel; plate; polymermatrix composites; prepreg; reinforcement; reinforcement con-tent; reinforcement volume; resin; resin content; shear; shearmodulus; shear strength; short-beam strength; specific heat;strain energy release rate; strength; structure; tensile strength;tension; therma

44、l conductivity; thermal diffusivity; thermalexpansion coefficient; tow; V-notched beam strength; voidcontent; winding; yarnD4762043TABLE 1 Lamina/Laminate Static Test MethodsTest Method Specimen Measured PropertyDescription andAdvantagesDisadvantages CommentsIn-Plane Tensile Test MethodsD 3039 Tensi

45、le Strength Straight sided specimen.Suitable for both random,discontinuous andcontinuous-fibercomposites. Tabbed anduntabbed configurationsavailable.Tabbed configurationsrequire careful adhesiveselection and specialspecimen preparation.Certain laminate layupsprone to edgedelamination which canaffect

46、 tensile strengthresults.Preferred for most uses.Provides additionalconfigurations,requirements, andguidance that are notfound in D 5083.Limited to laminates thatare balanced andsymmetric with respect tothe test direction.Tensile Modulus,Poissons Ratio,Stress-Strain ResponseRequires use of strain or

47、displacement transducers.Modulus measurementsdo not require use oftabs.Modulus measurementstypically robust.D 638 Tensile Strength,Tensile Modulus“Dumbbell” shapedspecimen.Ease of test specimenpreparation.Stress concentration atthe radii.Unsuitable for highlyoriented fiber composites.Not recommended

48、 forhigh-modulus composites.Technically equivalent toISO 527-1.D 5083 Tensile Strength,Tensile ModulusStraight-sided, untabbedspecimen only.Suitable for plastics andlow-modulus composites.A straight-sidedalternative to D 638.Technically equivalent toISO 527-4 except asnoted below:(a) This test metho

49、d doesnot include testing of theType I dog-bone shapedspecimen described inISO 527-4. Testing of thistype of specimen,primarily used forreinforced andunreinforced thermoplasticmaterials, is described inD 638.(b) The thickness of testspecimens in this testmethod includes the 2mm to 10 mm thicknessrange of ISO 527-4, butexpands the allowabletest thickness to 14 mm.D 5450 Transverse (90) TensileStrengthHoop wound cylinder withall 90 (hoop) plies loadedin axial tension.Develops data forspecialized process/form.Limited to hoop-woundcylinders.Limited to transversetensile propertie