DIN ISO 6617-2011 Petroleum-based lubricating oils - Aging characteristics - Determination of change in Conradson carbon residue after oxidation (ISO 6617 1994)《石油基润滑油 老化特性 用康氏法测定氧.pdf

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1、April 2011 Translation by DIN-Sprachendienst.English price group 8No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 7

2、5.100!$nOV“1754451www.din.deDDIN ISO 6617Petroleum-based lubricating oils Aging characteristics Determination of change in Conradson carbon residue after oxidation(ISO 6617:1994)English translation of DIN ISO 6617:2011-04Schmierle auf Minerallbasis Alterungsverhalten Bestimmung der nderung des Koksr

3、ckstandes nach Conradson nach Oxidation(ISO 6617:1994)Englische bersetzung von DIN ISO 6617:2011-04Huile de graissage base de ptrole Caractristiques de vieillissement Dtermination de laugmentation du rsidu de carbone Conradson aprs oxydation(ISO 6617:1994)Traduction anglaise de DIN ISO 6617:2011-04S

4、upersedesDIN 51352-1:1985-08www.beuth.deDocument comprises pagesIn case of doubt, the German-language original shall be considered authoritative.1003.11 DIN ISO 6617:2011-04 A comma is used as the decimal marker. 2 Contents Page National foreword 3 National Annex NA (informative) Bibliography .4 1 S

5、cope .5 2 Normative references .5 3 Definition .5 4 Principle.5 5 Apparatus 5 6 Reagents and materials .7 7 Sampling 8 Preparation of the apparatus.8 9 Test procedure8 10 Expression of results .8 11 Precision8 12 Test report .9 Annex A (normative) Thermometer specification.10 7DIN ISO 6617:2011-04 N

6、ational foreword This standard has been prepared by Technical Committee ISO/TC 28 “Petroleum products and lubricants” (Secretariat: ANSI, USA). The responsible German body involved in its preparation was the Normenausschuss Materialprfung (Materials Testing Standards Committee), Working Committee NA

7、 062-06-61 AA Prfung von Schmierlen, sonstigen len und Paraffinen of the Fachausschuss Minerall- und Brennstoffnormung (FAM). As an alternative to chromiumsulfuric acid cleaning solution, nitric acid and sulphuric acid can also be used, but care must be taken to ensure that all cleaned parts are fre

8、e of grease. The DIN Standards corresponding to the International Standards referred to in this document are as follows: ISO 3170 DIN EN ISO 3170, DIN 51750-1, DIN 51750-2 ISO 3585 DIN ISO 3585 Amendments This standard differs from DIN 51352-1:1985-08 as follows: a) the standard has been prepared on

9、 the basis of DIN 51352-1:1985-08, thus specifying the same subject of standardization. In accordance with the DIN Guidelines, DIN 51352-1:1985-08 must therefore be withdrawn; b) normative references have been updated. Previous editions DIN 51352: 1967-09 DIN 51352-1: 1972-11, 1976-05, 1985-08 3 DIN

10、 ISO 6617:2011-04 National Annex NA (informative) Bibliography DIN 51750-1, Sampling of petroleum products General information DIN 51750-2, Sampling of liquid petroleum products DIN EN ISO 3170, Petroleum liquids Manual sampling DIN ISO 3585, Borosilicate glass 3.3 Properties 4 DIN ISO 6617:2011-04

11、5 Petroleum-based lubricating oils Aging characteristics Determination of change in Conradson carbon residue after oxidation WARNING - The use of this International Standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problem

12、s associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 1 Scope This International Standard specifies a procedure for determination of the ageing char

13、acteristics of petroleum-based lubricating oils. It is applicable to those oils which have an evaporation loss of less than 15 % mass fraction, as determined by the procedure specified in 9.3 of this standard. 2 Normative references The following standards contain provisions which, through reference

14、 in this text, constitute provisions of this International Standard. At the time of publi- cation, the editions indicated were valid. All standards are subject to revision, and parties to agreements based on this International Standard are encouraged to investigate the possibility of applying the mo

15、st re- cent editions of the standards indicated below. Members of IEC and IS0 maintain registers of cur- rently valid International Standards. IS0 3170:1988, Petroleum liquids - Manual sampling. IS0 3585:1991, Borosilicate glass 3.3 - Properties. IS0 6615: 1993, Petroleum products - Determination of

16、 carbon residue - Conradson method. 3 Definition For the purposes of this International Standard, the following definition applies. 3.1 ageing characteristics: Characteristics of a petroleum-based lubricating oil as determined by the increase in the Conradson carbon residue of the oil aged in accord

17、ance with this International Standard in comparison to that of the same non-aged oil. 4 Principle The oil sample to be tested is aged for two 6-h peri- ods at a temperature of 200 “C while air is passed through the oil. The value of the Conradson carbon residue of the aged sample is determined accor

18、ding to IS0 6615. The Conradson carbon residue of the non-aged oil, also determined according to IS0 6615, is subtracted from this value. The increase in the value of the carbon residue of the aged oil over that of the non-aged oil is reported as the result. Under no circumstance may the procedure s

19、pecified in IS0 6615 be modified, or any other procedure substituted for this procedure. 5 Apparatus 5.1 Testing apparatus, consisting of an ageing vessel and a holder with an air inlet tube and an air outlet tube (figure I), all parts being manufactured from borosilicate glass in accordance with IS

20、0 3585. 0 IS0 5.1 .l Ageing vessel, manufactured from 28 mm x I,4 mm borosilicate glass pipe in accord- ance with IS0 3585, complete with a 29/32 conical ground glass joint. 5.1.2 Vessel for temperature measurement, con- structed as specified for the ageing vessel (5.1.1), but without the ground gla

21、ss joint. 5.1.3 Holder, with air inlet tube and air outlet tube. The air inlet tube shall be manufactured from 7 mm x 1 mm borosilicate glass pipe in accordance with IS0 3585, and sealed into the holder as illus- trated in figure 1. The air inlet tube shall be mounted in the centre of the holder and

22、 its lower end cut square. The length of the air inlet tube shall be such that, with the holder securely in place in the ageing vessel, its lower end is 1 mm b) a reference to this International Standard; c) the results of the test (see 10.2); d) any deviation, by agreement or otherwise, from the pr

23、ocedure specified; e) the date of the test. DIN ISO 6617:2011-04 9 Annex A (normative) Thermometer specification Range: . 195 “C to 205 “C Immersion, mm: 100 Graduation Subdivisions: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

24、 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0,l “C Long lines at each: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

25、. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0,5 “C Numbers at each: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

26、. . . . . . . . . . . . . . . . . . . . . . . . . 1 “C Scale error, max.: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

27、. . . . . . . . 0,2 “C Expansion chamber to permit heating: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . “ Required Total length, mm: . . . . . . . . . . . . . . . . . . . . . . . . . . . .

28、 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 300 + 10 - Stem outer diameter, mm: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

29、 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6,5 + I,5 - Bulb length, mm: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

30、. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30 + 5 - Bulb outer diameter: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

31、. . . . . . . . . . . . . . . . . . . . . . . . . Not greater than stem Minimum distance, in mm, from bottom of bulb to line at 195 “C: . 165 Length of scale range, mm: . 90 + 20 - Stem enlargement Diameter, mm: . Length, mm: . . Distance to bottom, mm: . . Thread reference temperature Over entire l

32、ength: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ,. 40 “C Expansion extension (safety bubble) for a volume equivalent of: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50 “C Thermometer filling: Mercury and protective gas Head of thermometer: . . . Equipped with ring or button NOTE 3 Thermometers to DIN 12785 and IP 22 C oxidation test are suitable. There is no equivalent International Standard at this time. DIN ISO 6617:2011-04 10