ASTM D1792-2006(2012)e1 Standard Test Method for Long-Term Removability Properties of Emulsion Floor Polishes《乳化地板擦亮剂长期可除污性的标准测试方法》.pdf

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1、Designation: D1792 06 (Reapproved 2012)1Standard Test Method forLong-Term Removability Properties of Emulsion FloorPolishes1This standard is issued under the fixed designation D1792; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision,

2、the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1NOTEEditorial changes were made in October 2012.1. Scope1.1 This test method covers the determination of the relative

3、ease of removal of dried films of water-emulsion floor polishesfrom common flooring substrates under accelerated conditions,which correspond to extended service aging.1.2 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of

4、the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D1436 Test Methods for Application of Emulsion FloorPolishes to Substrates for Testing Purposes3. Summary

5、 of Test Method3.1 The dried films are conditioned at 37.8C (100F) inorder to simulate service aging. This method utilizes theGardner straight-line washability apparatus as a means forcontrolled removal of the dried films. A heavily weighted padis employed as a means of arriving at a scrubbing force

6、 similarto that of hand scrubbing. In order to distinguish between therelative removal properties of different polishes, the number ofoscillations required for complete removal is taken as ameasure of removability.4. Significance and Use4.1 This test method is used to predict removability of floorpo

7、lish after a treatment period that simulates aging in the field.It allows for uniform mechanical and detergent action leavingthe only variable the actual removability of the polish.5. Apparatus5.1 Volumetric Pipet, 1-mL, graduated in 0.2-mL units.5.2 ApplicatorDoctor blade 51 mm (2 in.) wide by 25 m

8、m(1 in.) deep and having 0.203-mm (0.008-in.) clearance alongthe 51-mm (2-in.) length.5.3 Test Flooring SubstrateOfficial Vinyl CompositionTile (OVCT),3shall be used in the test.5.4 Oven, capable of maintaining a temperature of 37.8 61.1C (100 6 2F).5.5 Washability ApparatusThe Gardner straight-line

9、washability machine.5.6 Abrading Surface Nylon Polishing Floor Pad,4attachedto a wood block of dimensions 89 by 38 mm (312 by 112 in.).Presoaked in stripper solution.5.7 WeightThe boat containing the pad is fitted to achievea total weight of 1-kg (212 614-lb). The weight should beproperly mounted fo

10、r uniform load distribution.1This test method is under the jurisdiction of Committee D21 on Polishes and isthe direct responsibility of Subcommittee D21.04 on Performance Tests.Current edition approved Oct. 1, 2012. Published October 2012. Originallyapproved in 1960 as D1792 60 T. Last previous edit

11、ion approved in 2006 asD1792 06. DOI: 10.1520/D1792-06R12.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.3Th

12、e sole source of supply of the apparatus known to the committee at this timeis Chemical Specialties Manufacturers Assn., 1913 Eye St., N.W., Washington, DC20006. If you are aware of alternative suppliers, please provide this information toASTM Headquarters.Your comments will receive careful consider

13、ation at a meetingof the responsible technical committee, which you may attend.4The sole source of supply of the apparatus known to the committee at this timeis 3M Co., 3M Center, St. Paul, MN 55101. If you are aware of alternative suppliers,please provide this information toASTM Headquarters. Your

14、comments will receivecareful consideration at a meeting of the responsible technical committee, whichyou may attend.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States16. Reagent6.1 Stripper Solution at Use Concentration:Alkaline cleaner5

15、3%Monoethanol amine (MEA) 1 %Water 96 %7. Sample7.1 The sample shall be thoroughly representative of thematerial in question and the portion used for the test shall bethoroughly representative of the sample itself.8. Procedure8.1 Preparation of Test SurfacesClean the test tiles withthe stripper solu

16、tion and steel wool. Rinse thoroughly withwater and dry at room temperature.8.2 Polish ApplicationProceed in accordance withMethod D of Methods D1436. Apply in duplicate as shown inFig. 1 0.8 mL of test polish, A to 51 by 203-mm (2 by 8-in.)section of OTVAT. Tile should be on a level bench top toens

17、ure uniform film thickness. Apply in similar fashion dupli-cate samples of a control test polish B. Repeat process for otherpolishes. Allow the coated panels to dry for 2 h at ambientconditions; then apply a second coat of polish in the samemanner as the first coat. Let coated panels dry1hatambientc

18、onditions.8.3 Accelerated Aging ConditionsStore the coated panelsin an oven maintained at a temperature of 37 6 1.1C andcondition there for 48 h.8.4 RemovabilityPlace the coated and conditioned panelon the plate of the washability apparatus in such a manner thatthe oscillating pad will travel at rig

19、ht angles to the longer sideof the dried polish film. Place a clean dummy panel on eitherside of the test panel to hold the latter panel in place and toprovide a uniform surface for the oscillating pad to travel upon.Soak the pad for at least 1 min in the stripper solution, insertpad assembly into t

20、he weighted (1-kg) boat, invert, and turn onthe motor for one cycle. Stop for 1 min. Restart motor. Keepthe pad wet by adding additional stripper solution dropwiseonto the pad or into the coated panel. After 50 oscillations stopthe machine and remove and rinse the panel with water. Blotdry. If polis

21、h film remains, repeat the scrubbing for anadditional 50 oscillations and again examine the film afterrinsing and drying. Thereafter, if any film remains, repeat theprocess of scrubbing, rinsing, and drying after each additional50 oscillations until complete removal is obtained or to amaximum of 200

22、 total oscillations.9. Report9.1 The report shall include a qualitative rating according tothe following terminology:Removal EaseNumber of Oscillations Required forComplete RemovalExcellent 50 but 100 but 20010. Precision and Bias10.1 Duplicate determinations should not differ by morethan one rating

23、 group.11. Keywords11.1 emulsion; floor polishes; removability5Recipe for alkaline cleaner:Parts by WeightSodium sesquicarbonate 52Trisodium phosphate (anhydrous) 22Disodium phosphate (anhydrous) 25Alkyl aryl sulfonate (40 % active) 1FIG. 1 Polish ApplicationD1792 06 (2012)12ASTM International takes

24、 no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own resp

25、onsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addresse

26、d to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the

27、address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).D1792 06 (2012)13