BS ISO 19332-2007 Oil of blue chamomile [Chamomilla recutita (L ) Rauschert syn Matricaria chamomilla auct ]《洋甘菊油[Chamomilla recutita (L ) Rauschert syn Matricaria chamomilla auct .pdf

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1、 g49g50g3g38g50g51g60g44g49g42g3g58g44g55g43g50g56g55g3g37g54g44g3g51g40g53g48g44g54g54g44g50g49g3g40g59g38g40g51g55g3g36g54g3g51g40g53g48g44g55g55g40g39g3g37g60g3g38g50g51g60g53g44g42g43g55g3g47g36g58Matricaria chamomilla auct.ICS 71.100.60Oil of blue chamomile Chamomilla recutita (L.) Rauschert sy

2、n. BRITISH STANDARDBS ISO 19332:2007BS ISO 19332:2007This British Standard was published under the authority of the Standards Policy and Strategy Committee on 30 November 2007 BSI 2007ISBN 978 0 580 55822 1Amendments issued since publicationAmd. No. Date CommentsCompliance with a British Standard ca

3、nnot confer immunity from legal obligations.National forewordThis British Standard is the UK implementation of ISO 19332:2007.The UK participation in its preparation was entrusted to Technical Committee AW/54, Essential oils.A list of organizations represented on this committee can be obtained on re

4、quest to its secretary.This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application.Reference numberISO 19332:2007(E)INTERNATIONAL STANDARD ISO19332First edition2007-10-15Oil of blue chamomile Chamomilla recutita (L.) Raus

5、chert syn. Matricaria chamomilla auct. Huile essentielle de camomille bleue Chamomilla recutita (L.) Rauschert syn. Matricaria chamomilla auct. BS ISO 19332:2007ii iiiForeword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member

6、bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental

7、and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directive

8、s, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies c

9、asting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 19332 was prepared by Technical Committee ISO/TC 54, Essential oils. BS ISO 19332:

10、2007blank1Oil of blue chamomile Chamomilla recutita (L.) Rauschert syn. Matricaria chamomilla auct. 1 Scope This International Standard specifies certain characteristics of the oil of blue chamomile Chamomilla recutita (L.) Rauschert syn. Matricaria chamomilla auct., in order to facilitate assessmen

11、t of its quality. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO/TR 2

12、10, Essential oils General rules for packaging, conditioning and storage ISO/TR 211, Essential oils General rules for labelling and marking of containers ISO 212, Essential oils Sampling ISO 279, Essential oils Determination of relative density at 20 C (Reference method) ISO 11024-1, Essential oils

13、General guidance on chromatographic profiles Part 1: Preparation of chromatographic profiles for presentation in standards ISO 11024-2, Essential oils General guidance on chromatographic profiles Part 2: Utilization of chromatographic profiles of samples of essential oils 3 Terms and definitions For

14、 the purposes of this document, the following terms and definitions apply. 3.1 oil of blue chamomile essential oil obtained by steam distillation from the fresh or dried flower-heads or flowering tops of blue chamomile Chamomilla recutita (L.) Rauschert syn. Matricaria chamomilla auct. produced main

15、ly in Hungary and Egypt. NOTE For information on the CAS number, see ISO/TR 21092. 4 Requirements 4.1 Appearance Slightly viscous, clear liquid. 4.2 Colour Egyptian type Hungarian type Greenish blue to dark blue Dark blue 4.3 Odour Characteristic. 4.4 Relative density at 20 C, 2020d Egyptian type Hu

16、ngarian type Minimum 0,910 0,910 Maximum 0,970 0,950 BS ISO 19332:20072 4.5 Chromatographic profile Analysis of the essential oil shall be carried out by gas chromatography. In the chromatogram obtained, the representative and characteristic components shown in Table 1 shall be identified. The propo

17、rtions of these components, indicated by the integrator, shall be as shown in Table 1. This constitutes the chromatographic profile of the essential oil. Table 1 Chromatographic profile Egyptian type Hungarian type Component Minimum % Maximum% Minimum % Maximum% trans-Farnesene 15 35 20 51 -Bisabolo

18、l oxide B 2 8 2 21 Bisabolone oxide A 2 6,5 1 4 -Bisabolol 1 10 15 40 Chamazulene 2 5 5 22 -Bisabolol oxide A 35 50 2 27 NOTE The chromatographic profile is normative, contrary to typical chromatograms given for information in Annex A. 4.6 Flashpoint Information on the flashpoint is given in Annex B

19、. 5 Sampling See ISO 212. Minimum volume of test sample: 25 ml. NOTE This volume allows each of the tests specified in this International Standard to be carried out at least once. 6 Test methods 6.1 Relative density at 20 C, 2020d See ISO 279. 6.2 Chromatographic profile See ISO 11024-1 and ISO 1102

20、4-2. 7 Packaging, labelling, marking and storage See ISO/TR 210 and ISO/TR 211. BS ISO 19332:20073Annex A (informative) Typical chromatograms of the analysis by gas chromatography of the essential oil of blue chamomile Chamomilla recutita (L.) Rauschert syn. Matricaria chamomilla auct. BS ISO 19332:

21、20074 A.1 Essential oil of blue chamomile, Egyptian type Peak identification Operating conditions 1 trans-Farnesene 2 -Bisabolol oxide B 3 Bisabolone oxide A 4 -Bisabolol 5 Chamazulene 6 -Bisabolol oxide A Column: fused silica capillary, length 30 m, internal diameter 0,25 mm Stationary phase: polyd

22、imethyl siloxane SPB 1 (SE-30)1) Film thickness: 0,25 m Oven temperature: temperature programming from 50 C to 180 C at a rate of 3 C/min and 180 C to 220 C at a rate of 10 C/min Injector temperature: 260 C Detector temperature: 280 C Detector: flame ionization type Carrier gas: helium Volume inject

23、ed: 1 l Carrier gas flow rate: 1 ml/min Split ratio: 1/50 Figure A.1 Typical chromatogram taken on an apolar column 1) SPB 1 (SE-30) is an example of a suitable product available commercially. This information is given for the convenience of users of this International Standard and does not constitu

24、te an endorsement by ISO of this product. BS ISO 19332:20075Peak identification Operating conditions 1 trans-Farnesene 2 -Bisabolol oxide B 3 Bisabolone oxide A 4 -Bisabolol 5 Chamazulene 6 -Bisabolol oxide A Column: fused silica capillary, length 30 m, internal diameter 0,25 mm Stationary phase: po

25、lyethylene glycol Supelcowax 10 2) Film thickness: 0,25 m Oven temperature: temperature programming from 50 C to 180 C at a rate of 3 C/min and 180 C to 220 C at a rate of 10 C/min Injector temperature: 260 C Detector temperature: 280 C Detector: flame ionization type Carrier gas: helium Volume inje

26、cted: 1 l Carrier gas flow rate: 1 ml/min Split ratio: 1/50 Figure A.2 Typical chromatogram taken on a polar column 2) Supelcowax 10 is an example of a suitable product available commercially. This information is given for the convenience of users of this International Standard and does not constitu

27、te an endorsement by ISO of this product. BS ISO 19332:20076 A.2 Essential oil of blue chamomile, Hungarian type Peak identification Operating conditions 1 trans-Farnesene 2 -Bisabolol oxide B 3 Bisabolone oxide A 4 -Bisabolol 5 Chamazulene 6 -Bisabolol oxide A Column: fused silica capillary, length

28、 30 m, internal diameter 0,25 mm Stationary phase: polydimethyl siloxane SPB 1 (SE-30)3) Film thickness: 0,25 m Oven temperature: temperature programming from 50 C to 180 C at a rate of 3 C/min and 180 C to 220 C at a rate of 10 C/min Injector temperature: 260 C Detector temperature: 280 C Detector:

29、 flame ionization type Carrier gas: helium Volume injected: 1 l Carrier gas flow rate: 1 ml/min Split ratio: 1/50 Figure A.3 Typical chromatogram taken on an apolar column 3) SPB 1 (SE-30) is an example of a suitable product available commercially. This information is given for the convenience of us

30、ers of this International Standard and does not constitute an endorsement by ISO of this product. BS ISO 19332:20077Peak identification Operating conditions 1 trans-Farnesene 2 -Bisabolol oxide B 3 Bisabolone oxide A 4 -Bisabolol 5 Chamazulene 6 -Bisabolol oxide A Column: fused silica capillary, len

31、gth 30 m, internal diameter 0,25 mm Stationary phase: polyethylene glycol Supelcowax 10 4) Film thickness: 0,25 m Oven temperature: temperature programming from 50 C to 180 C at a rate of 3 C/min and 180 C to 220 C at a rate of 10 C/min Injector temperature: 260 C Detector temperature: 280 C Detecto

32、r: flame ionization type Carrier gas: helium Volume injected: 1 l Carrier gas flow rate: 1 ml/min Split ratio: 1/50 Figure A.4 Typical chromatogram taken on a polar column 4) Supelcowax 10 is an example of a suitable product available commercially. This information is given for the convenience of us

33、ers of this International Standard and does not constitute an endorsement by ISO of this product. BS ISO 19332:20078 Annex B (informative) Flashpoint B.1 General information For safety reasons, transport companies, insurance companies, and people in charge of safety services require information on t

34、he flashpoints of essential oils, which in most cases are flammable products. A comparative study on the relevant methods of analysis (see ISO/TR 11018) concluded that it was difficult to recommend a single apparatus for standardization purposes, given that: there is a wide variation in the chemical

35、 composition of essential oils; the volume of the sample needed for certain requirements would be too costly for high-priced essential oils; as there are several different types of equipment which can be used for the determination, users cannot be expected to use one specified type only. Consequentl

36、y, it was decided to give a mean value for the flashpoint in an informative annex to each International Standard in order to meet the requirements of the interested parties. The equipment with which this value was obtained should be specified. For further information see ISO/TR 11018. B.2 Flashpoint

37、 of the essential oil of blue chamomile The mean value is: Egyptian type Hungarian type + 104 C + 108 C NOTE Values obtained with “closed cup” equipment. BS ISO 19332:20079Bibliography 1 ISO/TR 11018, Essential oils General guidance on the determination of flashpoint 2 ISO/TR 21092, Essential oils C

38、haracterization 3 GILDEMEISTER, E., HOFFMANN, F. Die therischen le Volatile oils, Treibs W., ed., Vol. 7, pp. 649-60, Akademie-Verlag, Berlin, 1961 4 HTHELYI, ., PLFIN-LEDNICZKY, M., WILDE, F.P., ZMB, I., PLINKS, J. Gas chromatographic examination of oil and extract of chamomile. J. Oil Soap Cosmeti

39、cs 1999, 48(1), pp. 16-32 BS ISO 19332:2007BS ISO BSI389 Chiswick High RoadLondonW4 4AL19332:2007BSI British Standards InstitutionBSI is the independent national body responsible for preparing British Standards. It presents the UK view on standards in Europe and at the international level. It is inc

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