DB37 T 1305-2009 土壤中重金属微波消解快速测定方法.pdf

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1、 DB37/T a0a1a2 a3a4a5a6a7a6a5a6a8 a9 a3a3 山 东 省 地 方 标 准 DB37/T 13052009 土壤中重金属微波消解快速测定方法 Quick determination of heavy metals in soil with microwave digestion 2009-07-15发布 2009-08-01实施 山东省质量技术监督局 发 布 DB37/T 13052009 I 前 言 a10a11a12a13a14a15a16a17a18a19a20a21a22 a10a11a12a13a14a15a17a18a11a12a23a24a25

2、a26a27a28a29a30a22 a10a11a12a31a32a33a34a35a36a37a38a17a18a39a40a41a42a43a22 a10a11a12a44a45a31a32a46a35a47a48a40a49a50a51a52a49a53a54a49a55a56a57a49 a58a59a60 a49a61a62a63a49a64a65a66a49a67a68a69a49a70a71a72a49 a73a74a65a22 DB37/T 13052009 1 a75 a76a77 a78a79a80a81a82a83a84a85a86a87a88a89a90a91a92a

3、93a94a95a96a97a98a99a100a101a102a103a104a105a106a106a107a108a109a101a102a110a106a106a107a108a98a111a82 a84a85a112a113a114a115a116a117a97a118 a78a79a80a119a92a120a84a85a112a121a122 a123a124a125 a109a126a122 a127a128a125 a109a129a122 a127 a130 a125a109a131a122a127 a132 a125a109 a133a122 a134 a135 a125

4、a109a136 a122 a137a138a125 a109a139a122 a140a141a125 a142a143a116 a111a82a118 a78a117a97a144a145a146a122a147a148a86a149a150 a151a152a138 a98a82a153a154 a152 a149a155a156 a125 a157a158 a123a124 a159 a155 a138 a160a161 a138 a98 a127a128 a149a150a149a149 a152 a155 a138 a160a161 a138 a98 a127 a130 a159

5、a155 a138 a160a161 a138 a98 a127 a132 a149a150 a162 a155 a138 a160a161 a138 a98 a134 a135 a159 a155 a138 a160a161 a138 a98 a137a138 a149a150a149a149 a163 a155 a138 a160a161 a138 a98 a140a141 a149a150a149 a151 a155 a138 a160a161 a138 a118 a164 a165a166 a84a85a167a86a168a93a94a169a170a171a98a172a173a1

6、74- a175a176 a174a95a96a98a177a178a111a179a180a181a182a183a184a167a185a98a186a101a102a103a104a105a106a106a107a108 a111a82a121a109a126a109a129a109a131a109a133a179a180a116a103a106a107a187a91a92a93a94-a173a174a95a96a97a188a189a139a109a136a178a111a185a98a186a190a174a191a185a157a192a193a98 a186a194 a175a

7、195 a196- a175 a197 a195 a198a191a185a157a199a101a200a98a186a101a102a110a106a106a107a108a111a82a139a109a136a179a180a116a110a106a201a107a118a202a179a180a142a143a203a103 a106a107a204a110a106a201a107a205a206a207a118 a208 a209a210 a211a212a213a214a215a216a98a168a105a217a112a218a177a92a219a220a157a105a21

8、7a221a116a167a200a222a223a100GB/T 6682 a112a81a82a116 a224a225 a226a118 a208a227a75 a173a174 a122 a137a228a229a230a125 a98a231 a232 a159 a150 a163a151 a138a160 a155a156a98a233 a225 a221a118 a208a227a164 a175a176 a174 a122 a137a234a125 a98a231 a232 a159 a150 a163a235 a138a160 a155a156a98a233 a225 a22

9、1a118 a208a227a208 a190a174 a122 a137a127a236a125 a98a231 a232 a159 a150 a159a235 a138a160 a155a156a98a233 a225 a221a118 a208a227a237 a238 a239a174 a122 a137a127a236a229 a240 a125a98a231 a232 a159 a150 a241a242 a138a160 a155a156a98a233 a225 a221a118 a208a227a243 a175 a197 a195 a198a244 a228a245a229a

10、137a246 a118 a208a227a247 a194 a175a195 a196a244 a248a249a137 a240 a246 a118 a208a227a250 a251a252 a122 a228a137a253a127a254a228a137a253a246 a118 a208a227a255 a0a1 a2a174a244 a127 a3 a137a4a229 a3 a246 a118 a208a227a5 a173a174a191a185a6a7a244 a137a228a229a230a246 a232 a149a150 a151a8a9 a158a92 a162

11、a150 a159a10a188a118 a208a227a75a11 a190a174a191a185a6a7a244 a137a127a236a246 a232 a152a8a9 a158a92 a162 a150 a162a10 a188a118 a208a227a75a75 a175 a197 a195 a198a191a185a6a231a244 a228a245a229a137a246 a232 a152a138a160 a156 a9a12 a92 a162 a150 a152a10 a188a118 a208a227a75a164 a194 a175a195 a196a191a

12、185a6a231a244 a248a249a137 a240 a246 a232 a151 a149 a138 a160a156a9a12a148a13a159a149 a138 a194 a175a195 a196 a122 a162 a150 a241a125 a191a120 a152 a149a149a155a156 a175 a197 a195 a198a191a185 a122 a162 a150 a159a159a125 a112a98a14a92a14 a10a118 a208a227a75a208 a251a252a15a0a1 a2a174a16a100a191a185a

13、158a148a13 a152a138a251a252 a122 a162 a150a17 a125a109a152a138a0a1a2 a174 a122 a162 a150 a242a125 a191a120 a159 a149a149a155a156a226a112a98a16a18a118 a14a92a14a10a118 a208a227a75a237 a131a109a133a109a121a109a129a109a126a109a136a109a139a79a80a19a189a185a157a159a149a149a149a155 a138 a160a156 a122a20a2

14、1a214a22a116a23a24a79a80a191a185 a246 a118 a237 a25a26 a237a227a75 a101a102a103a104a105a106a106a107a108a118 a237a227a164 a101a102a110a106a106a107a108a118 a237a227a208 a27 a102a28a29 a122a30a143a149a150a149a149a149a159 a138a125 a118 a237a227a237 a27 a102a31a32a33a34a35a118 a237a227a243 a36a37 a38a158

15、a39a40a157 a151 a155a155a222a149a150 a159a163a235 a155a155a118 土壤中重金属微波消解快速测定方法 DB37/T 13052009 2 a41a42a43 a44 a45a46a47a48 a49 a50 a51a52a53 a54a55a56a57a58a59a60a61a62a63 a64a64 a65a66 a67a68a69a70 a66 a71a72a73a74a75a73a76a77 a64a64 a65a66 a78a79a54a55a80a81a82a83a84a85a86a87a88a89 a90a86 a66 a5

16、8a59a91a92a93a94a95a96 a66 a71a97a98a99a100 a66 a101a102a103a103a104a105a106a107a108a78a102a103a103a109a110a111a112a81a113 a66 a69a68a114a115a71a116a117a118a58 a74a118a58a119a102a63 a65a66 a120a121a62a122a123a99a124a125a126a99a127a128a129a130a131a101 a64a132 a77 a133a134 a103a103a104a105a106 a66 a13

17、5a73a69a68a96a136a62a58a59a137a138a139a57a114 a140 a141 a142a143a144 a140a145a146 a147a148a149 a150a151 a140a145a146a145a146 a152a153 a154 a153 a155 a153 a156 a153 a157a58a59a158a159a111a160a161 a162a163a164a118a139a57a58a59 a64a132 a77 a65 a165 a64a132 a63 a65a166 a167a163a76 a64a132a64a64a64 a77 a

18、65a168a66 a121a62a169a170a171a100a172a173a174a138 a66 a175a176a177a103a178a179a180 a166a181a132 a77 a168 a182a169a183a84a184a58a59a185a180a159a135a73a69a70 a66 a93a96a186a174a187a175a176 a181 a103a178a188a189a180 a166a181a132 a102 a168a66 a69a67 a66 a175a190a96 a66 a191a192a171a100a172a173 a174 a66

19、a121a62a193a194a195a196a197a111a169a170a172a173a198a138a199a200a58a59a172a173a114a139a169a170a198a172a173a196a197a201a202a96 a66 a203a204a205a76a206 a64a207a66 a208a171 a100a172a173a174a118a209 a66 a210a211a76a212a203a96a213a190a214a71a77 a64 a103a178a78a215a216a217a125a126a218a219a174a190 a181 a126

20、a109a110 a66 a93a96a121a62a131a94a220a138a221a216a222 a203a175a223a224a77a206 a64a207 a165 a77a177 a64a207 a199a200a225a180a226a227 a66 a228a229a102 a64 a103a230 a231 a182a169a183a84a172a173a174 a66 a232a233a225a180a101a196a80a172a173a159a80a234a235a86 a236a237a172a173a201a129 a66 a238a239a172a173a6

21、0a201a129a240a241a242a243a175 a181 a243a171a244a180a114a139a180a225a245a96 a66 a172a173a159a246a247a248a249a250a251a252a253a254a251 a66 a118a255a172a173a174a210a211a76a212a203 a66 a0a1a76a63 a64 a103a178a2a130a137a138a175a217a194a2a76a3a4 a66 a183a68a96a5a121 a181a64 a103a230 a231 a66 a238a58a159a69

22、a6a240 a101a7 a66 a8a9a58a59a139a57a159 a166a10a168 a114 a11a242a12a102a13a58a59a14a250a114 a140a145a146a145a15 a16a153 a17a58a59a158a159a111a160a161 a162a163a164a118a139a57a58a59 a64a132 a77 a65 a165 a64a132 a63 a65a166 a167a163a76 a64a132a64a64a64 a77 a65a168a66 a121a62a169a170a171a100a172a173a174

23、a138 a66 a175a176 a133 a103a178a179a180 a166a181a132 a77 a168 a182a169a183a84a184a58a59a185a180a159a135a73a69a70 a66 a175a190a96 a66 a11a110a206 a132 a77 a132 a77a18a19 a66 a93a96a62a131a94a220a138a221a216a222a203a175a223a224a77a102 a64a207 a165 a77 a133a64 a207 a199a200a225a180a226a227 a66 a228a229

24、a102 a64 a103a230 a231 a182a169a183a84a172a173a174 a66 a139a180a225a245a96 a66 a172a173a159a246a247a248a249a242 a66 a118a255a172a173a174a210 a211a76a212a203 a66 a0a1a76a63 a64 a103a178a2a130a137a138 a66 a175a102 a132 a63a103a178a20a21a180 a166a181a132a181a168a153 a63a103a178a22a23a24a25a26a27a180a69

25、a70a28a159 a166a181a132 a77 a181a168a66 a175a217a194a2a76a3a4 a66 a183a68a96a29a121 a181a64 a103a230 a231 a66 a101a7 a66 a8a9a58a59a139a57a159 a166a30a168 a114 a11a242a12a102a13a58a59a14a250a114 a140a145a15 a31a32a33 a34a35a36a37a150 a140a145a15a145a146 a80a38a159a111a39a160 a140a145a15a145a146a145a

26、146 a152a153 a154 a153 a155 a153 a156 a153 a157a80a38a159a111a39a160a40a208a3a162a41a161a159 a166a181a132 a77 a133a168 a42a43a109a179a180a28a159 a166a181a132a134a168 a44a45 a66a152 a46a77 a64a64 a103 a65a47 a178 a66 a154a46a77 a64 a103 a65a47 a178 a66 a155a46a77 a64a64 a103 a65a47 a178 a66 a156a46a7

27、7 a64 a103 a65a47 a178 a66 a157a77 a64a64a48a65a47 a178a114 a140a145a15a145a146a145a15 a17 a153a16 a80a38a159a111a39a160a40a208a3a162a41a161a159 a166a181a132 a77 a133a168 a71a49a43a78a215a216a217a42a43a44a45 a66 a17a46 a77 a64a132a64 a103 a65a47 a178 a66 a16 a46a77 a132a64 a103 a65a47 a178a114 a140a

28、145a15a145a15 a3a162a50a51a52a19a28a159a111a39a160 a140a145a15a145a15a145a146 a152a153 a154 a153 a155 a153 a156a69a70a3a162a50a51a28a159a40a71a80a38a159a107a206 a132 a102 a132 a77 a132 a77a113a39a160 a66a152 a50a51a20a204a46 a64a132a64a66a64a132 a63 a66 a77 a132a64a66 a77 a132 a63 a66 a102 a132a64 a

29、103 a65a47 a178a53a154a50a51a20a204a46 a64a132a64a66a64a132 a77 a66a64a132 a102a63 a66a64a132 a63 a66 a77 a132a64 a103 a65a47 a178a53a155a50a51a20a204a46 a64a132a64a66a64a132 a63 a66 a77 a132a64a66a181a132a64a66 a63 a132a64 a103 a65a47 a178a53a156a50a51a20a204a46 a64a132a64a66a64a132 a77 a66a64a132a

30、181a66a64a132 a63 a66 a77 a132a64 a103 a65a47 a178a114a109a110a54a55a56a50a51a20a204a71a179a180a28a159 a166a181a132a134a168 a194 a2a76a57 a58a59a60 a2a130a137a138a114 a140a145a15a145a15a145a15 a157a61a3a162a50a51a28a159a40a71a80a38a159a62 a140a145a15a145a146a145a146a63a39 a160a157a111a50a51a20a204a4

31、6 a58a145a58a66a58a145 a57 a66a146a145a58a66 a57 a145a58a66a146a58a145a58 a64 a65a60a66 a71a179a180a28a159 a166a66a145a67a168 a194a2a76a57 a58a59a60 a2a130a137a138a114 a140a145a15a145a15a145a66 a17 a153a16 a69a70a3a162a50a51a28a159a40a71a80a38a159a62 a140a145a15a145a146a145a15a63a39 a160a68a69a20a20

32、4a111a17 a153a16 a3a162a184a71a159 a66 a17a111a50a51 a20a204a46a57 a145a58a66a146a58a145a58a66a15a58a145a58a66a70a58a145a58a66 a57 a58a145a58 a64 a65a60 a53 a16 a111a50a51a20a204a46 a58a145 a57 a153a146a145a58a66a15a145a58a66a70a145a58a66 a57 a145a58 a64 a65a60a114a175a176 a15a145 a57 a59a60 a20a21a

33、180 a166a66a145a66a168 a83 a15a145 a57 a59a60 a22a23 a71 a25a26a27a180a69a70a28a159 a166a66a145a146a66a168a66a71a49a43a78a215a216a217a194a2a76a57a58a59a60a2a130 a137a80 a66 a29a121 a66a58a59a72 a73 a109a110a114a109a57 a74 a21a180a28a159 a166a66a145a146a58a168 a46a14a250a114 a140a145a15a145a15a145a70

34、 a109a110a52a19a3a162a50a51a125a126a20a204a75a76a9a171a77a78a110a235a79a160a3a162a52a19a80a4a114 DB37/T 13052009 3 a81a82a83 a84a85 a86a87 a88a89a90a91a92a91a93a94a95a96a97a98a99a100a89a90a91a93a101a89a90a102a103a104a105a106a107a108a109a110a111a112a113a114a105a115a114a116 a117 a118a119 a120a121 a122

35、a123a124a115a114a116 a117 a125a119 a120a126a122a127a123a128a129a130a131a132a133a134a135a136a115a114a116 a117 a118a119 a124a115a114a116 a117 a125a119 a137a120a138a139a140a141a142a143a123a128 a144a145a146 a147a148 a149a150a151a152a149a153a154a155 a129a130a156a157a158a159a120a89a90a111a104a160a107a108a

36、161a162a163a164a94a165a166a102a103a128a167a168a169a131a132a170a96a120a91a92a102a103a171a172a173a101a172a174a101 a172a175a101a172a176a128 a177 a178a179a180a181a182 a147 a154a155 a177a183a184a185a186a187a188a189a190 a147a148 a191a192a154a155 a177a193a184a185a186a187a191a194a194a195a196a197a198a199a190

37、 a147a148 a191a192a154a155 a200a201 a202 a203a204a205 a206a207a208 a209a209 a210a211a210 a212a213a214a205 a207a215a208 a210a211a216 a217a218a205 a206a207a208 a216a211a219 a220a221 a222a223 a224a225a226a227 a228a216a216a229a230a219a216a231 a232a233a226a227 a234 a216a216a229a230 a209 a216a231 a235a236

38、a233a226a227 a228a216a216a216a229a230a234a231 a237a238a226a227 a209 a219a216a216a229a230 a234a231 a239a240a214a241a242 a243a244 a207a245a206a246 a216a211 a209 a247a248a241a242 a249 a250 a246 a209 a216 a177 a146 a184a185a251a194a194a195a196 a147a148 a191a192a154a155 a200a201 a252a253a254a255 a0 a1 a2

39、12a213a214a205 a207a215a208 a219a216 a234a216 a2a223a3 a242 a4 a246 a209 a210a216 a209 a5a216 a235a236a233a223a6a205 a207a207a208 a210a211a216 a210a211a216 a239a240a205 a207 a243a244 a207a245a206a208 a219a216a216 a219a216a216 a7a8a240a205 a207 a243a244 a207a245a206a208 a228a216a216a216 a228a216a216a

40、216 a9a241a10a11 a12a13a14a15a16 a12a13a14a15a16 a17a18a10a11 a222a19a20 a222a19a20 a21a22 a23a24 a242 a25 a246 a26 a27a28a29 a242 a207a245a206a246 a3a30 a242a31a32a33 a246 a27a6 a242a229 a246 a34a35 a28a29a205 a207a245a206a208 a228 a234 a216a216 a216a219a36a216a216 a234 a219a216 a228 a209 a216 a228

41、 a216a36a216a216 a209 a234 a216a216 a216a5a36a216a216 a234 a219a216 a228 a37a219 a228a219a36a216a216 a234 a234 a216a216 a216a5a36a216a216 a234 a219a216 a228 a210a219 a209 a219a36a216a216 a200a201 a252a253a254a255 a38 a39 a40 a41 a203a204a205 a206a207a208 a209 a228 a42a211a216 a234 a219a42a211a43 a23

42、4 a209 a5a211a210 a209 a228a234a211a43 a212a213a214a205 a207a215a208 a219 a37 a219 a219 a44a240a214a241a205 a243a244 a207a245a206a208 a228a211a228 a228a211 a209 a228a211a228 a228a211 a209 a44a45a46a223a6a205 a207a207a208 a42a211a216 a210a211a216 a42a211a216 a42a211a216 a47a48a49a50 a51a240 a52a53 a5

43、4 a55a233a46a56 a26 a28a29a205 a207a245a206a208 a5 a5 a5 a5 a9a241a28a29a205 a207a245a206a208 a5 a5 a5 a5 a57a58 a242a217a218 a246 a205 a206a207a208 a216a211a219 a216a211a219 a216a211a219 a216a211a219 DB37/T 13052009 4 a59 a60a61a62 a63 a59a64a65 a66 a67a68a69a70a71a70a72a73a74a75a76a77a78a79 a62 a6

44、3a80 a81a82a83 a84a85a86 a87a88a89a85a90a91a92a93a94a95a96a97a98a99a100a101a102a103a104a102a81a105a106a107a108a106a83a109 a87a91a110a88a89a111a112a113a85a90a91a92a93a94a95a96a97a98a99a100a114a102a103a115a81a106a107a116a83a109 a117a118a119a113a85a90a91a92a93a94a95a96a97a98a99a100a114a102a103a115a81a1

45、06a107a116a83a109 a120 a88a89a111 a112a113a110a121a122a123a97a98a99a100a101a115 a81 a105a124 a83a109 a125 a88a89a126 a96a97a98a99a100a102 a81 a106 a83a109 a127a128a129a130a131a132a133a99a134a135a136a137a138 a59a64a139 a66 a67a68a140a70a141a70a142a70a143a73a74a75a76a144a78a79 a62 a63a80 m V= )( 01 2

46、.(2) a84a85a86 a145a88a89a85a90a91a92a93a94a95a96a97a98a99a100a101a102a103a104a102a81a105a106a107a108a106a83a109 a87a91a110a88a89a111a112a113a85a90a91a92a93a94a95a96a97a98a99a100a101a102a103a115a81a105a106a107a116a83a109 a117a118a119a113a85a90a91a92a93a94a95a96a97a98a99a100a101a102a103a115a81a105a10

47、6a107a116a83a109 a120 a88a89a111 a112a113a110a121a122a123a97a98a99a100a101a115 a81 a105a124 a83a109 a125 a88a89a126 a96a97a98a99a100a102 a81 a106 a83a138 a127a128a129a130a131a132a133a99a134a135a136a137a138 a146 a147a148 a149 a150a92a151a152a153a154a155a156a157a158a159a160a161a162a91 a88 a129a130a158

48、a163a164a165a166a167 a168a169 a170 a171a172a173a174a175a176a177a178a179a180 a181a182a183a184a185a186a168 a187 a186a168 a188 a186 a189a190a186a191a192a186a193a194a195a196 a197a198a199a200a201a202a179a203a204a205a178a177 a170 a171a172a173a174a175a176a177a178a179 a206 a181a182a207 1000 )( 01 1 = m V DB37/T 13052009 5 DB 37 /T DB 37 /T DB 37 /T DB 37 /T 1 30 5 13 05 13 05 13 05 20 09 20 09 20 09 20 09