SAE AMS 3617E-2014 Polyamide Type 6-6 Plastic Moldings and Extrusions.pdf

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1、_SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising theref

2、rom, is the sole responsibility of the user.”SAE reviews each technical report at least every five years at which time it may be revised, reaffirmed, stabilized, or cancelled. SAE invites your written comments and suggestions.Copyright 2013 SAE InternationalAll rights reserved. No part of this publi

3、cation may be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE.TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada)Tel: +1 724-776-4970 (out

4、side USA)Fax: 724-776-0790Email: CustomerServicesae.orgSAE WEB ADDRESS: http:/www.sae.orgSAE values your input. To provide feedbackon this Technical Report, please visithttp:/www.sae.org/technical/standards/AMS3617EAEROSPACE MATERIAL SPECIFICATIONAMS3617 REV. EIssued 1961-07Reaffirmed 2003-03Revised

5、 2014-01Superseding AMS3617DPolyamide Type 6-6, Plastic Moldings and ExtrusionsRATIONALEThis is a 5 year review of the specification which is a general update, corrects minor errors and has minor changes to format in accordance with SAE requirements1. SCOPE1.1 FormThis specification covers one type

6、of Polyamide Type 6-6 (nylon) thermoplastic resin in the form of moldings and extrusions. 1.2 DefinitionNylon 6-6, also referred to as nylon 6,6, is a polyamide from nylon class. The polymer is made of hexamethylenediamineand adipic acid, which give nylon 6,6 a total of 12 carbon atoms in each repea

7、ting unit, and its name.1.3 ApplicationThese products have been used typically for parts requiring high strength and resistance to aircraft fuels and lubricants up to 248 F (120 C), but usage is not limited to such applications. Users should test to confirm fluid compatibility at the systems maximum

8、 operating temperature before proceeding with part performance testing.1.4 Safety - Hazardous MaterialsWhile the materials, methods, applications, and processes described or referenced in this specification may involve the use of hazardous materials, this specification does not address the hazards w

9、hich may be involved in such use. It is the sole responsibility of the user to ensure familiarity with the safe and proper use of any hazardous materials and to take necessary precautionary measures to ensure the health and safety of all personnel involved.2. APPLICABLE DOCUMENTSThe issue of the fol

10、lowing documents in effect on the date of the purchase order forms a part of this specification to the extent specified herein. The supplier may work to a subsequent revision of a document unless a specific document issue is specified. When the referenced document has been cancelled and no supersedi

11、ng document has been specified, the last published issue of that document shall apply.SAE INTERNATIONAL AMS3617E Page 2 of 62.1 ASTM PublicationsAvailable from ASTM International, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, Tel: 610-832-9585, www.astm.org.ASTM D 256 Impac

12、t Resistance of Plastics and Electrical Insulating MaterialsASTM D 570 Water Absorption of PlasticsASTM D 638 Tensile Properties of PlasticsASTM D 638M Tensile Properties of Plastics (Metric)ASTM D 648 Deflection Temperature of Plastics Under Flexural LoadASTM D 790 Flexural Properties of Unreinforc

13、ed and Reinforced Plastics and Electrical Insulating MaterialsASTM D 790M Flexural Properties of Unreinforced and Reinforced Plastics and Electrical Insulating Materials (Metric)ASTM D 792 Specific Gravity (Relative Density) and Density of Plastics by DisplacementASTM D 3418 Transition Temperatures

14、of Polymers by Thermal Analysis2.2 U.S. Government PublicationsAvailable from DLA Document Services, Building 4/D, 700 Robbins Avenue, Philadelphia, PA 19111-5094, Tel: 215-697-6396,http:/quicksearch.dla.mil/.MIL-STD-2073-1 DOD Materiel, Procedures for Development and Application of Packaging Requir

15、ements3. TECHNICAL REQUIREMENTS3.1 MaterialShall be a polyamide resin with any necessary fillers, modifiers, and plasticizers necessary to meet the requirements of 3.1.1 and 3.2.3.1.1 ColorShall be light cream, opaque.3.2 PropertiesThe product shall conform to requirements shown in Table 1, Table 2,

16、 Table 3, tests shall be performed on the product supplied and in accordance with specified ASTM methods, insofar as practicable:3.2.1 Tensile StrengthShall be as shown in Table 1. TABLE 1 - MINIMUM TENSILE STRENGTHNominal ThicknessInchesNominal ThicknessMillimeters ValueTestMethodUp to 0.375, excl

17、Up to 9.52, excl 9.0 ksi (62 MPa) ASTM D 638 or0.375 and over 9.52 and over 11.0 ksi (76 MPa) ASTM D 638MSAE INTERNATIONAL AMS3617E Page 3 of 63.2.2 ElongationShall be as shown in Table 2.TABLE 2 - MINIMUM ELONGATIONNominal ThicknessInchesNominal ThicknessMillimeters ValueTestMethodUp to 0.187, excl

18、 Up to 4.75, excl 50% ASTM D 638 or0.187 and over 4.75 and over 25% ASTM D 638MTABLE 3 - PROPERTIESParagraph Property Value Test Method3.2.3 Flexural Modulus of Elasticity(Tangent), min310 ksi(2137 MPa)ASTM D 790 orASTM D 790M3.2.4 Impact Resistance per unit ofnotch, min0.6 foot pounds/inch(32.0 J/m

19、)ASTM D 256,Method A3.2.5 Deflection Temperatureat 264 psi (1.82) MPa) fiberstress, min151 F (66 C) ASTM D 6483.2.6 Water Absorption(24 hour immersion),weight gain, max1.5% ASTM D 5703.2.7Specific Gravityat 73 F 4 (23 C 2)1.13 to 1.15 ASTM D 792,Method A3.2.8 Melting point 482 to 509 F(250 to 265 C)

20、ASTM D 3418DTA or DSC(See 8.2)3.2.3 Weather ResistanceWhen specified, the product shall have weather resistance acceptable to purchaser, determined by a procedure acceptable to purchaser.3.2.4 CorrosionWhen specified, the product shall not have a corrosive effect on other materials when exposed to c

21、onditions normally encountered in service, determined by a procedure acceptable to purchaser.3.3 QualityThe product, as received by purchaser, shall be uniform in quality and condition, smooth, and free from foreign materials and from imperfections detrimental to usage of the product.SAE INTERNATION

22、AL AMS3617E Page 4 of 64. QUALITY ASSURANCE PROVISIONS4.1 Responsibility for InspectionThe manufacturer of the product shall supply all samples for required tests and shall be responsible for performing all required tests. Purchaser reserves the right to sample and to perform any confirmatory testin

23、g deemed necessary to ensure that the product conforms to the requirements of this specification.4.2 Classification of Tests4.2.1 Acceptance TestsTests for tensile strength (3.2.1), elongation (3.2.2), specific gravity (3.2.7), and melting point (3.2.8) are acceptance tests and shall be performed on

24、 each lot.4.2.2 Preproduction TestsTests for all technical requirements are preproduction tests and shall be performed prior to or on the initial shipment of theproduct by a manufacturer, when a change in ingredients and/or processing requires reapproval as in 4.4.2, and when purchaser deems confirm

25、atory testing to be required.4.2.2.1 For direct U.S. Military procurement, substantiating test data and, when requested, preproduction test material shall be submitted to the cognizant agency as directed by the procuring activity, contracting officer, or request for procurement.4.3 Sampling and Test

26、ingShall be as follows:4.3.1 For Acceptance TestsSufficient product shall be taken at random from each lot to perform all required tests. The number of determinations for each requirement shall be as specified in the applicable test procedure or, if not specified therein, not less than three.4.3.1.1

27、 When the product is of such size or shape that suitable specimens cannot be obtained, separate specimens, injection molded from the same batch of molding powder and under conditions representative of those used in making the product, shall be supplied upon request.4.3.1.2 A lot shall be all product

28、 from the same batch of molding powder processed in one continuous run and presented for manufacturers inspection at one time.4.3.1.3 A batch of molding powder shall be all powder produced in one continuous set of operations.4.3.1.4 When a statistical sampling plan has been agreed upon by purchaser

29、and manufacturer, sampling shall be in accordance with such plan in lieu of sampling as in 4.3.1 and the report of 4.5 shall state that such plan was used.4.3.2 For Preproduction TestsAs agreed upon by purchaser and manufacturer.4.4 Approval4.4.1 Sample product shall be approved by purchaser before

30、product for production use is supplied, unless such approval be waived by purchaser. Results of tests on production product shall be essentially equivalent to those on the approved sample.SAE INTERNATIONAL AMS3617E Page 5 of 64.4.2 Manufacturer shall use ingredients, manufacturing procedures, proces

31、ses, and methods of inspection on production product which are essentially the same as those used on the approved sample. If necessary to make any change in ingredients, in type of equipment for processing, in manufacturing procedures or methods of inspection, manufacturer shall submit for reapprova

32、l a statement of the proposed changes in ingredients and/or processing and, when requested, sample product. Production product made by the revised procedure shall not be shipped prior to receipt of reapproval.4.5 ReportsThe supplier of the product shall furnish with each shipment a report showing th

33、e results of tests to determine conformance to the acceptance test requirements and stating that the product conforms to the other technical requirements. This report shall include the purchase order number, lot number, AMS3617E, manufacturers compound number, form and size or part number, and quant

34、ity.4.6 Resampling and RetestingIf any specimen used in the above tests fails to meet the specified requirements, disposition of the product may be based on the results of testing three additional specimens for each original nonconforming specimen. Failure of any retest specimen to meet the specifie

35、d requirements shall be cause for rejection of the product represented. Results of all tests shall be reported.5. PREPARATION FOR DELIVERY5.1 Product Identification5.1.1 Molded PartsEach molded part of suitable size shall have the part number molded or permanently impressed therein. If size or use p

36、recludes integral marking, parts of each different part number shall be packed in separate, suitable containers marked with the part number.5.1.2 ExtrusionsShall be marked near one end with AMS3617E and the manufacturers designation. If extrusions are supplied in coils, the marking shall appear at t

37、he outside end of the coil.5.2 Packaging and Package Identification5.2.1 Packaging shall be accomplished to ensure that the product, during shipment and storage, will not be permanently distorted and will be protected against damage from exposure to moisture, weather, or any other normal hazard.5.2.

38、2 Each package shall be permanently and legibly marked with not less than the following information:POLYAMIDE MOLDINGS (or EXTRUSIONS) AMS3617ESIZE OR PART NUMBER _QUANTITY _PURCHASE ORDER NUMBER _MANUFACTURERS IDENTIFICATION _5.2.3 Packages of product shall be prepared for shipment in accordance wi

39、th commercial practice and in compliance with applicable rules and regulations pertaining to handling, packaging, and transportation of the product to ensure carrier acceptance and safe delivery.5.2.4 For direct U.S. Military procurement, packaging shall be in accordance with MIL-STD-2073-1, Commerc

40、ial Level, unless Level A is specified in the request for procurement.SAE INTERNATIONAL AMS3617E Page 6 of 66. ACKNOWLEDGMENTSupplier shall mention this specification number and its revision letter in all quotations and when acknowledging purchase orders.7. REJECTIONSProduct not conforming to this s

41、pecification, or to modifications authorized by purchaser, will be subject to rejection.8. NOTES8.1 A change bar (|) located in the left margin is for the convenience of the user in locating areas where technical revisions, not editorial changes, have been made to the previous issue of this document

42、. An (R) symbol to the left of the document title indicates a complete revision of the document, including technical revisions. Change bars and (R) are not used in original publications, nor in documents that contain editorial changes only.8.2 ASTM D 4066, notes C and D, Table PA, heating rate 10 C

43、(18 F) degrees/minute; the results of an international round robin (ISO-USA, Germany, Japan, Poland, and Italy) showed DSC melt point to be the method having the best reproducibility of results when compared to other available methods (ref. ISO 3146).8.3 Dimensions and properties in inch/pound units

44、 and the Fahrenheit temperatures are primary; dimensions and properties in SI units and the Celsius temperatures are shown as the approximate equivalents of the primary units and are presented only for information.8.4 For direct U.S. Military procurement, purchase documents should specify not less t

45、han the following:Title, number, and date of this specificationForm and size or part number of product desiredQuantity of product desiredMethod of test and acceptance standards for weather resistance (3.2.9) and corrosion (3.2.10)Level A packaging, if required (See 5.2.4).8.5 Similar SpecificationsF

46、ederal L-P-410 and ASTM D 4066 are listed for information only and shall not be construed as acceptable alternates unless all requirements of this AMS are met.8.6 Products meeting the requirements of this specification have been classified under Federal Supply Classification (FSC) 9330.PREPARED BY AMS COMMITTEE “P”