KS I 3546-2012 Reduction performance test of VOCs (volatile organic compound) and aldehyde by contamination reduction building material - the solid phase building material《低污染建筑材料的.pdf

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1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS I 3546 VOCs KS I 3546:2012 2012 12 27 http:/www.kats.go.krKS I 3546:2012 : ( ) ( ) ( ) : (ISO/TC146) () ( ) : (http:/www.standard.go.kr) ： ：2012 12 27 2012-0785 ： ： (ISO/TC146) ( 02-509-7270) (http:/www.kats.go.kr). 10 5 , . KS I 3546:2012 i 1 1 2 1 3 .1

2、4 3 5 4 6 4 6.1 .4 6.2 .5 6.3 .5 6.4 .5 6.5 5 6.6 .5 6.7 6 7 .6 7.1 .6 7.2 .6 7.3 6 7.4 .6 7.5 .7 7.6 7 8 7 8.1 7 8.2 7 8.3 .7 8.4 7 8.5 .8 8.6 .8 9 .8 10 .8 11 8 11.1 8 11.2 8 11.3 8 11.4 9 11.5 .9 11.6 9 12 9 13 .9 KS I 3546:2012 ii 13.1 9 13.2 .9 13.3 10 13.4 .10 13.5 10 14 .10 A( ) / (QA/AC) 12

3、A.1 .12 A.2 12 A.3 .12 A.4 QA/QC 12 B( ) 13 C( ) 14 C.1 .14 C.2 .14 C.3 14 D( ) 15 KS I 3546:2012 VOCs Performance test methods for evaluating the reduction of VOCs(volatile organic compounds) and aldehyde by building material Solid phase building material 1 VOCs . , , , . 2 . . ( ) . KS I ISO 16000

4、 3, 3： KS I ISO 16000 6, 6： Tenax TA , MS/FID KS I ISO 16000 9, 9： KS I ISO 16000 11, 11： , 3 . 3.1 (solid phase building material) , , , , . 3.2 (building material) KS I 3546:2012 2 3.3 (elasped time) ( ) 3.4 (supply air concentration) 3.5 (air) . 3.6 (air velocity) 3.7 (guideline concentration) 3.

5、8 (mass transfer coefficient) 3.9 (background concentration) 3.10 (product loading factor) 3.11 (sampling period) 3.12 (test start) 3.13 (test specimen) 3.14 (total amount of adsorption) KS I 3546:2012 3 3.15 (living environment) 3.16 (ventilation rate) 3.17 (equivalent ventilation rate) 3.18 (air e

6、xchange rate) ( ) 3.19 (adsorption flux) , 3.20 (adsorption test chamber) 3.21 (adsorption test chamber concentration) , 3.22 (adsorption rate) (%) 3.23 (recovery) , 4 . A ： Cd： ( ) Cout,t： t (g/m3) Cin,t： t (g/m3) ERr： g/(m2 h) F ： , g/(m2 h) L ： (m2/m3) KS I 3546:2012 4 QC： (m3/h) Qeq： m3/(m2 h) Q

7、S： (L/min) Ra： (%) SC： (g/m2) Ss： (g/m2) t ： ( ) V ： (m3) 5 , , , , . , , , , , , . 6 6.1 VOC . , 6.2 6.6 . / A . 1 . 1 KS I 3546:2012 5 6.2 KS I ISO 16000 9 . . , , . . , . 6.3 . . ( , mass flow controller , 5 % ) . 490 mL/min, 10 mL/min , 50 . . 6.3.1 . . 6.3.2 . . , . . 6.4 . . , . 6.5 . . 6.6 .

8、KS I 3546:2012 6 . . (fume) . 6.7 6.7.1 (VOCs) VOCs (TD) , (FID) (MS) . MS PFTBZ(perfluorotributylamine) m/z 69 100 % m/z 219 40 % 60 %, m/z 512 2 % . VOCs KS I ISO 16000 6 . 6.7.2 , KS I ISO 16000 3 . 7 7.1 7.2 7.5 . . 7.2 (25, 50 % R.H.) . . ： (251) ： (503) % R.H. , . 7.3 . , TVOC 20 g/m3 , VOC 2

9、g/m3g3 , 5 g/m3g3 . VOCs . 7.4 KS I 3546:2012 7 (153) m/h (0.250.05) m/s . 7.5 . (0.50.05) /h , (2.00.02) m2/m3 . 1 . , . 2 , , . . 7.6 . , (WHO) . , , . B . 10 % . 8 8.1 , , . 1.0 3 % R.H. 3 % 8.2 KS I ISO 16000 9 . , . 1 000 Pa 0.1 % 1 % 8.3 KS I ISO 16000 9 . 8.4 KS I 3546:2012 8 KS I ISO 16000 9

10、 . 8.5 . 10 % , 10 % . 8.6 , 80 % . . , , . 9 7.3 . , . 10 KS I ISO 16000 11 . . . . . . 11 11.1 VOC . 7.3 . 11.2 , 5 . 11.3 . . KS I 3546:2012 9 11.4 11.6 . . (242) h, (726) h, (12010) h, (14814) h, (141) (day) (282) . , . 28 , . . . 11.5 . . 24 . . , . 11.6 VOCs Tenax-TA(2,6-diphenyl-p-phenylene-o

11、xide polymer resin) KS I ISO 16000 6 . DNPH(2,4-dinitrophenylhydrazine) KS I ISO 16000 3 . 12 7.3 , KS I ISO 16000 3, KS I ISO 16000 6 . 13 13.1 F (F) (1) . F (Cin,t Cout,t)QC/A (1) F ： g/(m2 h) Cin,t： t (g/m3) Cout,t： t (g/m3) QC： (m3/h) 13.2 Qeq (Qeq) (2) . KS I 3546:2012 10 Qeq (Cin,t/Cout,t 1)QC

12、/A (2) 13.3 SC t (SC) (3) . SCiii)(e,TF 1e,e,e, =iiiTTT (3) Te： 13.4 Ra (Ra) (4) . Ra (Cin,t Cout,t)/Cin,t100 (4) 13.5 ERr (ERr) (5) . ERr (Cout,t Cin,t)QC/A (5) 14 . a) b) ( ) ( ) , (batch number), c) , , , , d) ( , , , , , ) , ( , , ) ( , ) KS I 3546:2012 11 e) ( , , , , , ) f) / (QA/QC) , , KS I

13、3546:2012 12 A ( ) / (QA/AC) A.1 (quality assurance project plan, QAPP) . QAPP , , / , QA/QC QA/QC . A.2 , , . A.3 , , . A.4 QA/QC QAPP QA/QC . a) , , b) GC c) HPLC d) ( ) ( ) e) f) g) , ID GC ID , HPLC ID h) QC / i) DNPH QC j) k) QC . . GC HPLC KS I 3546:2012 13 B ( ) . B.1 ： g/m3g3 (, 2010) (WHO, 2000) (, 2002) g3 30 1 000 1 000* 260* 260 360 3 800 700 870 300 70* 260* 220 210 100 100* 100 48 TVOC 400 400 * S * L KS I 3546:2012 14 C ( ) C.1 , . C.2 6. , 11. . . , 100 g/m3 1 000 g/m3 .