EN ISO 105-C09-2003 en Textiles - Tests for colour fastness - Part C09 Colour fastness to domestic and commercial laundering - Oxidative bleach response using a non-phosphate refer.pdf

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1、BRITISH STANDARD BS EN ISO 105-C09:2003 Incorporating amendments nos. 1 (renumbers BS ISO 105-C09:2001 as BS EN ISO 105-C09:2003) and 2 Textiles Tests for colour fastness Part C09: Colour fastness to domestic and commercial laundering Oxidative bleach response using a non-phosphate reference deterge

2、nt incorporating a low temperature bleach activator The European Standard EN ISO 105-C09:2003, incorporating amendment A1:2007, has the status of a British Standard ICS 59.080.01 BS EN ISO 105-C09:2003 This British Standard was published under the authority of the Standards Policy and Strategy Commi

3、ttee on 28 January 2002 BSI 2007 ISBN 978 0 580 60553 6 National foreword This British Standard is the UK implementation of EN ISO 105-C09:2003, incorporating amendment A1:2007. It is identical with ISO 105-C09:2001, incorporating amendment 1:2003. The start and finish of text introduced or altered

4、by amendment is indicated in the text by tags !“. Tags indicating changes to ISO text carry the number of the ISO amendment. For example, text altered by ISO amendment 1 is indicated by !“. The UK participation in its preparation was entrusted to Technical Committee TCI/81, Colour fastness and colou

5、r measurement. A list of organizations represented on this committee can be obtained on request to its secretary. This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard cannot conf

6、er immunity from legal obligations. Amendments issued since publication Amd. No. Date Comments 15184 17 May 2004 Renumbers BS ISO 105-C09:2001 as BS EN ISO 105-C09:2003 17456 31 October 2007 See national forewordEUROPEANSTANDARD NORMEEUROPENNE EUROPISCHENORM ENISO105C09 March2003 ICS59.080.01 Englis

7、hversion TextilesTestsforcolourfastnessPartC09:Colourfastness todomesticandcommerciallaunderingOxidativebleach responseusinganonphosphatereferencedetergent incorporatingalowtemperaturebleachactivator(ISO105 C09:2001) TextilesEssaisdesoliditdesteinturesPartieC09: Soliditdesteinturesauxlavagesdomestiq

8、ueset industrielsBlanchimentparoxydationutilisantun dtergentderfrencesansphosphatecomprenantun activateurdeblanchimentbassetemprature(ISO105 C09:2001) TextilienFarbechtheitsprfungenTeilC09:Farbechtheit gegenoxidativeBleicheinderHaushaltswscheundder gewerblichenWscheunterVerwendungeines phosphatfreie

9、nTestwaschmittelsundeinesbeiniedrigen TemperaturenwirkendenBleichaktivators(ISO105 C09:2001) ThisEuropeanStandardwasapprovedbyCENon9January2003. CENmembersareboundtocomplywiththeCEN/CENELECInternalRegulationswhichstipulatetheconditionsforgivingthisEurope an Standardthestatusofanationalstandardwithou

10、tanyalteration.Uptodatelistsandbibliographicalreferencesconcernings uchnational standardsmaybeobtainedonapplicationtotheManagementCentreortoanyCENmember. ThisEuropeanStandardexistsinthreeofficialversions(English,French,German).Aversioninanyotherlanguagemadebytra nslation undertheresponsibilityofaCEN

11、memberintoitsownlanguageandnotifiedtotheManagementCentrehasthesamestatusasthe official versions. CENmembersarethenationalstandardsbodiesofAustria,Belgium,CzechRepublic,Denmark,Finland,France,Germany,Greece, Hungary,Iceland,Ireland,Italy,Luxembourg,Malta,Netherlands,Norway,Portugal,SlovakRepublic,Spa

12、in,Sweden,Switzerland and UnitedKingdom. EUROPEANCOMMITTEEFORSTANDARDIZATION COMITEUROPENDENORMALISATION EUROPISCHESKOMITEEFRNORMUNG ManagementCentre:ruedeStassart,36B1050Brussels 2003CEN Allrightsofexploitationinanyformandbyanymeansreserved worldwideforCENnationalMembers. Ref.No.ENISO105C09:2003E +

13、A1 August 2007INESO015:90C2300(E) 2 Foreword ThetextofISO105C09:2001hasbeenpreparedbyTechnicalCommitteeISO/TC38“Textiles“ oftheInternationalOrganizationforStandardization(ISO)andhasbeentakenoverasENISO 105C09:2003byTechnicalCommitteeCEN/TC248“Textilesandtextileproducts“,the secretariatofwhichisheldb

14、yBSI. ThisEuropeanStandardshallbegiventhestatusofanationalstandard,eitherbypublicationof anidenticaltextorbyendorsement,atthelatestbySeptember2003,andconflictingnational standardsshallbewithdrawnatthelatestbySeptember2003. AccordingtotheCEN/CENELECInternalRegulations,thenationalstandardsorganization

15、sof thefollowingcountriesareboundtoimplementthisEuropeanStandard:Austria,Belgium,Czech Republic,Denmark,Finland,France,Germany,Greece,Hungary,Iceland,Ireland,Italy, Luxembourg,Malta,Netherlands,Norway,Portugal,SlovakRepublic,Spain,Sweden, SwitzerlandandtheUnitedKingdom. Endorsementnotice ThetextofIS

16、O105C09:2001hasbeenapprovedbyCENasENISO105C09:2003without anymodifications. NOTENormativereferencestoInternationalStandardsarelistedinAnnexZA(normative). ENISO105C09:2003The text of ISO 105-C09:2001/Amd 1:2003 has been prepared by Technical Committee ISO/TC 38 “Textiles” of the International Organiz

17、ation for Standardization (ISO) and has been taken over as EN ISO 105-C09:2003/A1:2007 by Technical Committee CEN/TC 248 “Textiles and textile products“, the secretariat of which is held by BSI. This European Standard shall be given the status of a national standard, either by publication of an iden

18、tical text or by endorsement, at the latest by February 2008, and conflicting national standards shall be withdrawn at the latest by February 2008. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European

19、Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.

20、 Endorsement notice The text of ISO 105-C09:2001/Amd 1:2003 has been approved by CEN as C09:2003/A1:2007 without any modifications. Foreword to amendment A1EN ISO 105-INTERNATIONAL STANDARD ISO 105-C09 First edition 2001-12-01 Reference number ISO 105-C09:2001(E) OSI 2001 Textiles Tests for colour f

21、astness Part C09: Colour fastness to domestic and commercial laundering Oxidative bleach response using a non-phosphate reference detergent incorporating a low temperature bleach activator Textiles Essais de solidit des teintures Partie C09: Solidit des teintures aux lavages domestiques et industrie

22、ls Blanchiment par oxydation utilisant un dtergent de rfrence sans phosphate comprenant un activateur de blanchiment basse temprature ENISO105C09:2003ii ISO 1002 All rithgs rreseved ISO 1002 All rsthgi reserv.de sselnU torehesiw scepfi,dei on rapt of tihs bupliactino may be rrpedecudo ro tuzilide ni

23、 nay from or by any means, tcelercino or mnahceicla, icnidulng tohppocoying dna micrfomli, tiwtuoh perminoiss ni wrtigni fmor eitreh ISO at teh serddas lebow ro ISOs memreb ydob in the cotnury fo the rtseuqeer. ISO cporythgi fofiec esaC tsopael 65 1121-HC Geneva 02 Te.l + 41 22 947 10 11 Fax + 14 22

24、 479 09 47 E-liam copyrightsio.ch Web wwwsi.oc.hISO -501C01002:9)E( ISO 1002 All rithgs rreseved iii Foreword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally

25、 carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the w

26、ork. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 3. Draft International Standards adopted by the technical

27、committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this part of ISO 105 may be the subject of patent rights. ISO

28、 shall not be held responsible for identifying any or all such patent rights. International Standard ISO 105-C09 was prepared by Technical Committee ISO/TC 38, Textiles, Subcommittee SC 1, Tests for coloured textiles and colorants. ISO 105 was previously published in thirteen “parts”, each designate

29、d by a letter (e.g., “Part A”), with publication dates between 1978 and 1985. Each part contained a series of “sections”, each designated by the respective part letter and by a two-digit serial number (e.g. “Section A02”). These sections are now being republished as separate documents, themselves de

30、signated “parts” but retaining their ealier alphanumeric designations. A complete list of these parts is given in ISO 105-A01. Annex A forms a normative part of this part of ISO 105. ENISO105C09:2003ISO -50102:90C)E(10 iv ISO 1002 All rithgs rreseved Introduction The test method in this section of I

31、SO 105 is intended to reflect the effect of multicycle laundering using an activated bleach detergent by domestic and commercial laundering procedures. The washes are carried out in a similar manner to the ISO 105-C06 tests using an activated oxygen bleach and reference detergent at . A paper descri

32、bing the development of this method has been published in the Journal of the Society of Dyers & Colourists, Vol. 112, No.10, Oct. 1996, p. 287-292. 60 C ENISO105C09:20031 Textiles Tests for colour fastness Part C09: Colour fastness to domestic and commercial laundering Oxidative bleach response usin

33、g a non-phosphate reference detergent incorporating a low temperature bleach activator 1 Scope This part of ISO 105 specifies a method for determining the consumer relevant shade change of textiles, of all kinds, (excluding silk and wool) and in all forms, to domestic/commercial laundering procedure

34、s in which a bleach activator (oxygen bleaching system) is used. The colour fastness resulting from oxygen bleaching in this test provides an indication of the shade change behaviour observed after multiple domestic/commercial launderings. This part of ISO 105 is not applicable for the assessment of

35、 the dye staining of adjacent fabrics, where suitable methods are described in ISO 105-A04. 2 Normative references The following normative documents contain provisions which, through reference in this text, constitute provisions of this part of ISO 105. For dated references, subsequent amendments to

36、, or revisions of, any of these publications do not apply. However, parties to agreements based on this part of ISO 105 are encouraged to investigate the possibility of applying the most recent editions of the normative documents indicated below. For undated references, the latest edition of the nor

37、mative document referred to applies. Members of ISO and IEC maintain registers of currently valid International Standards. ISO 105-A01:1994, Textiles Tests for colour fastness Part A01: General principles of testing ISO 105-A02:1993, Textiles Tests for colour fastness Part A02: Grey scale for assess

38、ing change in colour ISO 105-A05:1996, Textiles Tests for colour fastness Part A05: Instrumental assessment of change in colour for determination of grey scale rating ISO 105-J01:1997, Textiles Tests for colour fastness Part J01: General principles for measurement of surface colour 1) ENISO105C09:20

39、03 This part of ISO 105 specifies a procedure incorporating the use of ECE 1)(see Annex B). sodium perborate tetrahydrate, and the bleach activator tetra-acetylethylenediamine (TAED) non-phosphate reference detergent, (see AnnexA) andopticalbrightener), sodium perborate monohydrate and the bleach ac

40、tivator sodium detergent (without a procedure incorporating the use of AATCC 1993 zero phosphate reference (SNOBS) nonanoyloxybenzene sulfonate This method has been designed for the detergents and bleach systems given. Other detergents and bleach systems may require different conditions and levels o

41、f ingredient. ! “ European Colourfastness Establishment (ECE). ! “ !Textdeleted “ISO -50102:90C)E(10 2 ISO 1002 All rithgs rreseved ISO 105-J03:1995, Textiles Tests for colour fastness Part J03: Calculation of colour differences ISO 3696:1987, Water for analytical laboratory use Specification and te

42、st methods 3P r i n c i p l e A specimen of the textile is laundered, rinsed and dried. Specimens are laundered under specified conditions of temperature, alkalinity and bleach concentration such that a fading result which correlates with a multicycle machine washing is obtained in a conveniently sh

43、ort time. The change in colour of the specimen is assessed with reference to the original fabric, either with the grey scale or instrumentally. 4 Reagents and materials 4.1 Reference detergent. 4.1.1 ECE non-phosphate reference detergent base powder (1998 formulation). 4.1.2 Bleach activator, tetra-

44、acetylethylenediamine, TAED. 4.1.3 Sodium perborate tetrahydrate. 4.2 Grade 3 water, complying with ISO 3696. 4.3 Grey scale, for assessing change in colour complying with ISO 105-A02 or a spectrophotometer for assessing change in colour complying with ISO 105-J01. 4.4 Filter papers. 5 Apparatus 5.1

45、 Suitable mechanical laundering device, consisting of a water bath containing a rotatable shaft which supports, radially, stainless steel containers ( ) of capacity , the bottom of the containers being from the centre of the shaft. The shaft/container assembly is rotated at a frequency of . The temp

46、erature of the water bath is thermostatically controlled to maintain the test solution at the prescribed temperature . Other mechanical devices may be used for this test, provided that the results are identical with those obtained by the apparatus described in 5.1. 5.2 Balance, accurate to (see ISO

47、105-A01). 5.3 Mechanical Stirrer, minimum ( ) to ensure thorough dispersion and prevent settling. 6T e s t s p e c i m e n 6.1 If the textile to be tested is fabric, cut a piece. 6.2 Yarn may be knitted into fabric of dimensions , and tested in this form. Alternatively, for yarns and threads, form a wick of parallel lengths long and about in diameter. Determine the mass of the specimen and either tie both ends or sew on to a piece of polypropylene backing cloth ( ) as support. In the latter case, only the mass of yarns and threads are take