BS EN 12788-2005 Advanced technical ceramics — Mechanical properties of ceramic composites at high temperature under inert atmosphere - Determination of flexural strength《高级工业陶瓷 惰性.pdf

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1、BRITISH STANDARDBS EN 12788:2005Advanced technical ceramics Mechanical properties of ceramic composites at high temperature under inert atmosphere Determination of flexural strengthThe European Standard EN 12788:2005 has the status of a British StandardICS 81.060.99g49g50g3g38g50g51g60g44g49g42g3g58

2、g44g55g43g50g56g55g3g37g54g44g3g51g40g53g48g44g54g54g44g50g49g3g40g59g38g40g51g55g3g36g54g3g51g40g53g48g44g55g55g40g39g3g37g60g3g38g50g51g60g53g44g42g43g55g3g47g36g58Licensed Copy: Wang Bin, na, Fri Mar 23 01:03:56 GMT+00:00 2007, Uncontrolled Copy, (c) BSIBS EN 12788:2005This British Standard was p

3、ublished under the authority of the Standards Policy and Strategy Committee on 29 December 2006 BSI 2006ISBN 0 580 49862 XNational forewordThis British Standard was published by BSI. It is the UK implementation of EN 12788:2005. It supersedes DD ENV 12788:1998 which is withdrawn. The UK participatio

4、n in its preparation was entrusted to Technical Committee RPI/13, Advanced technical ceramics.A list of organizations represented on RPI/13 can be obtained on request to its secretary.This publication does not purport to include all the necessary provisions of a contract. Users are responsible for i

5、ts correct application.Compliance with a British Standard cannot confer immunity from legal obligations.Amendments issued since publicationAmd. No. Date CommentsLicensed Copy: Wang Bin, na, Fri Mar 23 01:03:56 GMT+00:00 2007, Uncontrolled Copy, (c) BSIEUROPEAN STANDARDNORME EUROPENNEEUROPISCHE NORME

6、N 12788August 2005ICS 81.060.99 Supersedes ENV 12788:1998 English VersionAdvanced technical ceramics - Mechanical properties of ceramiccomposites at high temperature under inert atmosphere -Determination of flexural strengthCramiques techniques avances - Proprits mcaniquesdes cramiques composites ha

7、ute temprature sousatmosphre inerte - Dtermination de la rsistance enflexionHochleistungskeramik - Mechanische Eigenschaften vonkeramischen Verbundwerkstoffen bei hoher Temperatur aninerter Atmosphre - Bestimmung der BiegefestigkeitThis European Standard was approved by CEN on 18 July 2005.CEN membe

8、rs are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application

9、to the Central Secretariat or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same s

10、tatus as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France,Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia,Slovenia

11、, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: rue de Stassart, 36 B-1050 Brussels 2005 CEN All rights of exploitation in any form and by any means reservedworldwide for CEN national

12、 Members.Ref. No. EN 12788:2005: ELicensed Copy: Wang Bin, na, Fri Mar 23 01:03:56 GMT+00:00 2007, Uncontrolled Copy, (c) BSIEN 12788:2005 (E) 2 Contents Page Foreword 3 1 Scope .4 2 Normative references .4 3 Terms, definitions and symbols 4 4 Principle.5 5 Apparatus 5 5.1 Test machine .5 5.2 Test j

13、ig .5 5.3 Gastight test chamber 7 5.4 Set-up for heating .7 5.5 Temperature measurement devices 7 5.6 Data recording system .7 5.7 Micrometers.7 6 Test specimens .7 7 Test specimen preparation.8 7.1 Machining and preparation 8 7.2 Number of test specimens .8 8 Test procedures 8 8.1 Test set-up: Temp

14、erature considerations.8 8.2 Test set-up: Other considerations.9 8.3 Testing technique .9 8.4 Test validity .11 9 Calculation of results11 9.1 Test specimen origin 11 9.2 Flexural strength.11 10 Test report .12 Licensed Copy: Wang Bin, na, Fri Mar 23 01:03:56 GMT+00:00 2007, Uncontrolled Copy, (c) B

15、SIEN 12788:2005 (E) 3 Foreword This European Standard (EN 12788:2005) has been prepared by Technical Committee CEN/TC 184 “Advanced technical ceramics”, the secretariat of which is held by BSI. This European Standard shall be given the status of a national standard, either by publication of an ident

16、ical text or by endorsement, at the latest by February 2006, and conflicting national standards shall be withdrawn at the latest by February 2006. This document supersedes ENV 12788:1998. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countri

17、es are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerlan

18、d and United Kingdom. Licensed Copy: Wang Bin, na, Fri Mar 23 01:03:56 GMT+00:00 2007, Uncontrolled Copy, (c) BSIEN 12788:2005 (E) 4 1 Scope This European Standard specifies the conditions for determination of the flexural strength of ceramic matrix composite materials with continuous fibre reinforc

19、ement under three-point or four-point bending for temperatures up to 2 000 C under vacuum or a gas atmosphere which is inert to the material under test. NOTE 1 The use of these environments is aimed at avoiding changes of the material affecting its flexural strength caused by chemical reaction with

20、its environment during the test. This European document applies to all ceramic matrix composites with a continuous fibre reinforcement, unidirectional (1D), bidirectional (2D), and tridirectional (xD, with 2 x 3), loaded along one principal axis of reinforcement. NOTE 2 The method outlined in this d

21、ocument should not be used to obtain values of flexural strength for design purposes. 2 Normative references The following referenced documents are indispensable for the application of this European Standard. For dated references, only the edition cited applies. For undated references, the latest ed

22、ition of the referenced document (including any amendments) applies. EN 12789, Advanced technical ceramics Mechanical properties of ceramic composites at high temperature under air at atmospheric pressure Determination of flexural strength EN 60584-1:1995, Thermocouples Part 1: Reference tables (IEC

23、 60584-1:1995) EN 60584-2:1993, Thermocouples Part 2: Tolerances (IEC 60584-2:1982 + A1:1989) ENV 843-5:1996, Advanced technical ceramics Monolithic ceramics Mechanical tests at room temperature Part 5: Statistical analysis EN ISO 7500-1:1999, Metallic materials Verification of static uniaxial testi

24、ng machines Part 1: Tension/compression testing machines Verification and calibration of the force-measuring system ISO 3611:1978, Micrometer callipers for external measurement 3 Terms, definitions and symbols For the purposes of this European Standard, the following terms, definitions and symbols a

25、pply. 3.1 test temperature, T temperature at the centre of the test piece 3.2 maximum flexural force, Fmhighest recorded force in a flexural test on the test specimen when tested to failure 3.3 flexural stress, nominal stress on the outer surface of the test specimen, calculated at mid span NOTE Thi

26、s stress is conventionally calculated according to the simple beam theory, the basic assumptions of which may not be met by ceramic matrix composite materials. Licensed Copy: Wang Bin, na, Fri Mar 23 01:03:56 GMT+00:00 2007, Uncontrolled Copy, (c) BSIEN 12788:2005 (E) 5 3.4 flexural strength, f,mmax

27、imum flexural stress applied to a test specimen that fractures during a flexural test 4 Principle A test specimen of specified dimensions is heated to the test temperature. It is subsequently flexion loaded to fracture in such a way that failure occurs in tension, or in compression, along one princi

28、pal axis of reinforcement. The test is performed at constant crosshead displacement rate. The test duration is limited to reduce any time-dependent effects (e.g. creep). 5 Apparatus 5.1 Test machine The machine shall be equipped with a system for measuring the force applied to the test specimen. The

29、 system shall conform to grade 1 according to EN ISO 7500-1:1999. 5.2 Test jig The test jig is composed of two parts, linked to the fixed and mobile parts of the machine. It has two outer support rollers and one (three-point bending) or two (four-point bending) inner support rollers. The material of

30、 the jig and that of the rollers shall not react with that of the specimen, or with the environment. The cylindrical rollers shall have a diameter of 4 mm to 10 mm. Their length shall be at least equal to the width of the specimen. They shall be made of a material with a hardness at least equal to t

31、hat of the specimen. The axes of the rollers shall be parallel to within 0,01 mm/mm. The outer rollers (three and four-point bending) and inner rollers (four-point bending) shall be free to rotate (see Figure 1). Either two or three rollers, for three-point or four-point bending respectively, shall

32、be free to pivot around an axis parallel to the longitudinal direction of the test specimen, in order to adapt to the non-parallelism of the upper and lower faces of unmachined test specimens (see Figure 1). The rolling and pivoting ability of the rollers shall not be affected by heating. The distan

33、ce between rollers shall be in accordance with Clause 6. The inner roller(s) shall be centred with respect to the outer rollers to within 0,2 mm. In the case of four-point bending, a levelling system shall be used to ensure symmetrical loading of the test specimen. The performance shall not change b

34、ecause of heating. Licensed Copy: Wang Bin, na, Fri Mar 23 01:03:56 GMT+00:00 2007, Uncontrolled Copy, (c) BSIEN 12788:2005 (E) 6 Key 1 Pivoting loading roller 2 Rolling and pivoting support roller 3 Rolling but non-pivoting support roller a) Key 1 Rolling and pivoting loading roller 2 Rolling and p

35、ivoting support roller 3 Rolling but non-pivoting support roller b) Figure 1 Articulation required for jigs Licensed Copy: Wang Bin, na, Fri Mar 23 01:03:56 GMT+00:00 2007, Uncontrolled Copy, (c) BSIEN 12788:2005 (E) 7 5.3 Gastight test chamber The gastight chamber shall allow proper control of the

36、test specimen environment in the vicinity of the test specimen during the test. The installation shall be such, that the variation of the load during the time of loading, which may occur due to parasitic effects (e.g. variation of pressure, seals, etc.), is less than 1 % of the range of the load cel

37、l being used. Where a gas atmosphere is used, the gas atmosphere shall be inert to the specimen material and test jig under test conditions. Where a vacuum chamber is used, the level of vacuum shall not induce chemical and/or physical instabilities of the test specimen material and test jig. 5.4 Set

38、-up for heating The set-up for heating shall be constructed in such a way that the variation of temperature of the test specimen, which is between the outer support rollers, is less than 50 C at test temperature. 5.5 Temperature measurement devices For temperature measurement, either thermocouples c

39、onforming to EN 60584-1 and EN 60584-2 shall be used or, where thermocouples not conforming to EN 60584-1 and EN 60584-2 are used, they shall be calibrated appropriately. 5.6 Data recording system A calibrated recorder shall be used to record force-time curve. NOTE The use of a digital data recordin

40、g system combined with an analogue recorder is recommended. 5.7 Micrometers Micrometers used for the measurement of the dimensions of the test specimen shall conform to ISO 3611. 6 Test specimens The amount of material under load shall be representative of the nature of the material and of the reinf

41、orcement structure. NOTE 1 This sets minimum limits to the span and to the width and thickness of the specimen. In the case of flexural, as opposed to tensile testing, the distribution of the longitudinal reinforcement through the thickness shall also be considered. When this distribution is not sym

42、metrical with respect to the neutral plane, care shall be taken to insure that it is similar between specimens. The thickness and the distance between the inner and outer roller(s) shall be chosen so as to avoid shear failure. This is achieved by setting a minimum limit to the ratio between the mome

43、nt arm and the specimen thickness. NOTE 2 A value of 10 is commonly used and translates into a minimum L/h ratio of 20 in three-point bending, and a minimum (L Li)/h ratio of 20 in four-point bending with Li = L/3. NOTE 3 Other factors affecting the size and dimensions of the specimens are the type

44、of the heating and of the loading system, as well as the size of the test chamber. Recommended specimen dimensions are given in Table 1. Licensed Copy: Wang Bin, na, Fri Mar 23 01:03:56 GMT+00:00 2007, Uncontrolled Copy, (c) BSIEN 12788:2005 (E) 8 Table 1 Recommended test specimen and span dimension

45、s Dimensions in millimetres 1D, 2D and xD Tolerance Lt, total length L + 10 1 b, width 10 0,2h, thickness 2,5 0,2 Inner span 25 0,1 Four-point bending, LiOuter span Four-point bending, L 75 0,1Outer span Three-point bending, 50 0,1 NOTE 4 If it is necessary to define test specimens of different dime

46、nsions, the conditions of Clause 6 should be taken into account. 7 Test specimen preparation 7.1 Machining and preparation During cutting out, care shall be taken to align the longitudinal test specimen axis with one of the principal axes of reinforcement. Specimens may be tested with either machine

47、d or non-machined top and bottom surfaces. In some cases machining is not recommended because it may cause breakage of the fibres near the top and bottom surfaces. When machining these surfaces, care shall be taken to maintain a reinforcement geometry across the thickness of the specimen, which is r

48、epresentative of the material in the as-processed condition. In particular, the symmetry of an originally symmetric reinforcement geometry shall be preserved in the specimen cross-section after machining. Machining parameters that avoid damage to the material shall be established and documented. The

49、se parameters shall be adhered to during test specimen preparation. 7.2 Number of test specimens At least five valid test results, as specified in 8.4, are required per loading condition. For specimens with a non-symmetric reinforcement geometry with respect to the neutral plane, tests in two orientations for which the tensile and compressive face are interchanged may be necessary. If a statistical evaluation of the flexural strength is required, the number of test specimens shall be in accordance with ENV 843-5. 8 Test procedur