IEC 61249-4-5-2005 Materials for printed boards and other interconnecting structures - Part 4-5 Sectional specification for prepreg materials unclad - Polyimide modified or unmodif.pdf

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1、 INTERNATIONAL STANDARD IEC 61249-4-5First edition 2005-09Materials for printed boards and other interconnecting structures Part 4-5: Sectional specification set for prepreg materials, unclad Polyimide, modified or unmodified, woven E-glass prepreg of defined flammability Reference number IEC 61249-

2、4-5:2005(E) Publication numbering As from 1 January 1997 all IEC publications are issued with a designation in the 60000 series. For example, IEC 34-1 is now referred to as IEC 60034-1. Consolidated editions The IEC is now publishing consolidated versions of its publications. For example, edition nu

3、mbers 1.0, 1.1 and 1.2 refer, respectively, to the base publication, the base publication incorporating amendment 1 and the base publication incorporating amendments 1 and 2. Further information on IEC publications The technical content of IEC publications is kept under constant review by the IEC, t

4、hus ensuring that the content reflects current technology. Information relating to this publication, including its validity, is available in the IEC Catalogue of publications (see below) in addition to new editions, amendments and corrigenda. Information on the subjects under consideration and work

5、in progress undertaken by the technical committee which has prepared this publication, as well as the list of publications issued, is also available from the following: IEC Web Site (www.iec.ch) Catalogue of IEC publications The on-line catalogue on the IEC web site (www.iec.ch/searchpub) enables yo

6、u to search by a variety of criteria including text searches, technical committees and date of publication. On-line information is also available on recently issued publications, withdrawn and replaced publications, as well as corrigenda. IEC Just Published This summary of recently issued publicatio

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8、 custserviec.ch Tel: +41 22 919 02 11 Fax: +41 22 919 03 00 INTERNATIONAL STANDARD IEC 61249-4-5First edition 2005-09Materials for printed boards and other interconnecting structures Part 4-5: Sectional specification set for prepreg materials, unclad Polyimide, modified or unmodified, woven E-glass

9、prepreg of defined flammability IEC 2005 Copyright - all rights reserved No part of this publication may be reproduced or utilized in any form or by any means, electronic or mechanical, including photocopying and microfilm, without permission in writing from the publisher. International Electrotechn

10、ical Commission, 3, rue de Varemb, PO Box 131, CH-1211 Geneva 20, Switzerland Telephone: +41 22 919 02 11 Telefax: +41 22 919 03 00 E-mail: inmailiec.ch Web: www.iec.ch M For price, see current catalogue PRICE CODE Commission Electrotechnique Internationale International Electrotechnical Commission

11、2 61249-4-5 IEC:2005(E) CONTENTS FOREWORD.3 1 Scope.5 2 Normative references .5 3 Materials and construction6 3.1 Reinforcement.6 3.2 Resin system.6 4 Properties.6 4.1 Properties related to the appearance of the prepreg6 4.2 Properties related to B-stage prepreg7 4.3 Properties related to prepreg af

12、ter curing 8 5 Delivery form9 5.1 Rolls9 5.2 Sheets.9 5.3 Cut panels.10 6 Quality assurance.10 6.1 Quality system.10 6.2 Responsibility for inspection10 6.3 Qualification inspection .10 6.4 Quality conformance inspection.10 6.5 Certificate of conformance.10 6.6 Safety data sheet 10 7 Packaging and m

13、arking 11 8 Shelf life.11 9 Ordering information.11 Bibliography13 Table 1 Flammability9 61249-4-5 IEC:2005(E) 3 INTERNATIONAL ELECTROTECHNICAL COMMISSION _ MATERIALS FOR PRINTED BOARDS AND OTHER INTERCONNECTING STRUCTURES Part 4-5: Sectional specification for prepreg materials, unclad Polyimide, mo

14、dified or unmodified, woven E-glass prepreg of defined flammability FOREWORD 1) The International Electrotechnical Commission (IEC) is a worldwide organization for standardization comprising all national electrotechnical committees (IEC National Committees). The object of IEC is to promote internati

15、onal co-operation on all questions concerning standardization in the electrical and electronic fields. To this end and in addition to other activities, IEC publishes International Standards, Technical Specifications, Technical Reports, Publicly Available Specifications (PAS) and Guides (hereafter re

16、ferred to as “IEC Publication(s)”). Their preparation is entrusted to technical committees; any IEC National Committee interested in the subject dealt with may participate in this preparatory work. International, governmental and non- governmental organizations liaising with the IEC also participate

17、 in this preparation. IEC collaborates closely with the International Organization for Standardization (ISO) in accordance with conditions determined by agreement between the two organizations. 2) The formal decisions or agreements of IEC on technical matters express, as nearly as possible, an inter

18、national consensus of opinion on the relevant subjects since each technical committee has representation from all interested IEC National Committees. 3) IEC Publications have the form of recommendations for international use and are accepted by IEC National Committees in that sense. While all reason

19、able efforts are made to ensure that the technical content of IEC Publications is accurate, IEC cannot be held responsible for the way in which they are used or for any misinterpretation by any end user. 4) In order to promote international uniformity, IEC National Committees undertake to apply IEC

20、Publications transparently to the maximum extent possible in their national and regional publications. Any divergence between any IEC Publication and the corresponding national or regional publication shall be clearly indicated in the latter. 5) IEC provides no marking procedure to indicate its appr

21、oval and cannot be rendered responsible for any equipment declared to be in conformity with an IEC Publication. 6) All users should ensure that they have the latest edition of this publication. 7) No liability shall attach to IEC or its directors, employees, servants or agents including individual e

22、xperts and members of its technical committees and IEC National Committees for any personal injury, property damage or other damage of any nature whatsoever, whether direct or indirect, or for costs (including legal fees) and expenses arising out of the publication, use of, or reliance upon, this IE

23、C Publication or any other IEC Publications. 8) Attention is drawn to the Normative references cited in this publication. Use of the referenced publications is indispensable for the correct application of this publication. 9) Attention is drawn to the possibility that some of the elements of this IE

24、C Publication may be the subject of patent rights. IEC shall not be held responsible for identifying any or all such patent rights. International Standard IEC 61249-4-5 has been prepared by IEC technical committee 91: Electronics assembly technology. The text of this standard is based on the followi

25、ng documents: FDIS Report on voting 91/527/FDIS 91/537/RVD Full information on the voting for the approval of this standard can be found in the report on voting indicated in the above table. This publication has been drafted in accordance with the ISO/IEC Directives, Part 2. 4 61249-4-5 IEC:2005(E)

26、IEC 61249-4 consists of the following parts, under the general title Materials for printed boards and other interconnecting structures Part 4: Sectional specification set for prepreg materials, unclad: Part 4-1: Epoxide woven E-glass prepreg of defined flammability 1Part 4-2: Multifunctional epoxide

27、 woven E-glass prepreg of defined flammability Part 4-5: Polyimide, modified or unmodified, woven E-glass prepreg of defined flammability Part 4-11: Non-halogenated epoxide, woven E-glass prepreg of defined flammability Part 4-12: Non-halogenated multifunctional epoxide woven E-glass prepreg of defi

28、ned flammability The committee has decided that the contents of this publication will remain unchanged until the maintenance result date indicated on the IEC web site under “http:/webstore.iec.ch“ in the data related to the specific publication. At this date, the publication will be reconfirmed; wit

29、hdrawn; replaced by a revised edition, or amended. A bilingual version of this publication may be issued at a later date. 1Under consideration. 61249-4-5 IEC:2005(E) 5 MATERIALS FOR PRINTED BOARDS AND OTHER INTERCONNECTING STRUCTURES Part 4-5: Sectional specification set for prepreg materials, uncla

30、d Polyimide, modified or unmodified, woven E-glass prepreg of defined flammability 1 Scope This part of IEC 61249 gives requirements for properties of prepreg that is mainly intended to be used as bonding sheets in connection with laminates according IEC 61249-2-11 when manufacturing multilayer boar

31、ds according to IEC 62326-4. This material may be also used to bond other types of laminates. Prepreg according to this standard is of defined flammability (vertical burning test). The flammability rating on fully cured prepreg is achieved through the use of brominated fire retardants contained as a

32、n integral part of the polymeric structure. After curing according to the suppliers instructions, the glass transition temperature is defined to be 170 C minimum. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, o

33、nly the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. IEC 61189-2:1997, Test methods for electrical materials, printed boards and other inter- connecting structures and assemblies Part 2: Test methods for materials fo

34、r interconnection structures Amendment 1 (2000) IEC 61249-2-11, Materials for printed boards and other interconnecting structures Part 2-11: Sectional specification set for reinforced base materials clad and unclad Polyimide woven E-glass laminated sheet of defined flammability copper-clad IEC 61249

35、-6-3, Material for printed boards and other interconnecting structures Part 6-3: Sectional specification set for reinforcement materials Woven E-glass (for the manufacture of prepregs and copper-clad base materials 2IEC 62326-4:1996, Printed boards Part 4: Rigid multilayer printed boards with interl

36、ayer connections - Sectional specification ISO 9000:2000, Quality management systems Fundamentals and vocabulary ISO 11014-1:1994, Safety data sheet for chemical products Part 1: Content and order of sections ISO 14001:2004, Environmental management systems Requirements with guidance for use 2In pre

37、paration. 6 61249-4-5 IEC:2005(E) 3 Materials and construction The prepreg consists of a reinforcing E-glass fabric which is impregnated with polyimide resin and partially cured to the B-stage. 3.1 Reinforcement Woven E-glass as specified in IEC 61249-6-3: Woven E-glass fabric (for the manufacture o

38、f prepreg and copper-clad laminate). 3.2 Resin system Polyimide, modified or unmodified, resulting in a cured laminate with a glass transition temperature of 170 C minimum. Contrast agents may be added to enhance processing such as automated optical inspection. Its flame resistance is defined in ter

39、ms of the flammability requirements of 4.3.2. 4 Properties 4.1 Properties related to the appearance of the prepreg The prepreg shall be substantially free from defects that may have an impact on the materials fitness for use for the intended purpose. For the following specific defects, the requireme

40、nts given shall apply when inspection is made in accordance with IEC 61189-2 method 2V01 (under consideration). 4.1.1 Dewetted areas (fish eyes) Dewetted areas with a diameter 10 mm are not permissible. Dewetted areas with a diameter 10 mm are permitted to an extent of a maximum 10 fish eyes in any

41、300 300 mm area of the prepreg. 4.1.2 Broken filaments When judging the presence of broken filaments their sizes and frequency of occurrence are important for assessing acceptability but also the flow characteristic of the prepreg must be taken into consideration. The acceptance conditions for broke

42、n filaments shall be as agreed upon between the user and supplier. 4.1.3 Distortion When the prepreg is tested in accordance with test method 2M29 (under consideration) of IEC 61189-2, the distortion or non-perpendicular orientation of the fill or weft yarns in the glass fabric shall not exceed 10 %

43、 measured over any 300 mm test distance. 4.1.4 Creases Creases caused by handling of the prepreg where only a negligible loss of resin has occurred are permitted. Creases where the glass yarns are exposed due to loss of resin are not permitted. 61249-4-5 IEC:2005(E) 7 4.1.5 Edge conditions Cut-to-si

44、ze panels shall have even edges and shall not show loss of resin at the edge due to the cutting process more than 2 mm. Excessive occurrence of resin dust released during the cutting shall be removed before packaging for shipment. 4.2 Properties related to B-stage prepreg A number of characteristics

45、 can describe thickness, reactivity and rheology of B stage prepreg. The choice of characteristics to be used as qualification and quality conformance testing as well as the nominal performance levels are as agreed upon between the user and supplier. Several of the characteristics shown below are in

46、terrelated and should not be specified individually. Ordering requirements should preferably be restricted to the glass style, one characteristics marked (a) in combination with one characteristic marked (b). A maximum of one optional characteristic (c) of B stage prepreg may be included. Glass styl

47、e Thickness parameter Resin content (a) Treated weight (a) Reactivity/rheology parameter Resin flow (b) Scaled flow thickness (b) Melt viscosity (b) Cured thickness (b) Optional parameter Volatile content (c) Gel time (c) 4.2.1 Resin content When tested in accordance with test method 2C03 or 2C10 of

48、 IEC 61189-2, the nominal resin content shall be as agreed upon between the user and supplier. The tolerance around the ordered nominal value shall be 3 %, e.g. (45 3) %. 4.2.2 Treated weight When tested in accordance with test method 2C03 of IEC 61189-2, the nominal treated weight shall be as agree

49、d upon between the user and supplier. The tolerance around the ordered nominal value shall be 3 %, e.g. (350 10,5) g. 4.2.3 Resin flow When tested in accordance with test method 2M09 of IEC 61189-2, the nominal resin flow shall be as agreed upon between the user and supplier. The tolerance around the ordered nominal value shall be 5 %, e.g. (25 5) %. 8 61249-4-5 IEC:2005(E) 4.2.4 Sca