ASTM E923-1997(2008) 402 Standard Specification for Glass Westergren Tube Reusable《可再使用韦斯特格伦玻璃试管的标准规范》.pdf

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1、Designation: E 923 97 (Reapproved 2008)Standard Specification forGlass Westergen Tube, Reusable1This standard is issued under the fixed designation E 923; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A

2、 number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This specification describes requirements for a tube thatmeasures the erythrocyte sedimentation rate (ESR). ESR is thesuspension stabi

3、lity of red cells in diluted, anti-coagulatedhuman blood.1.1.1 The use of the term “rate” is, strictly speaking, notcorrect. The test measures the amount of settling of red cellsafter a specified time.1.2 The tubes are used together with a special rack to ensurethey remain in a vertical position dur

4、ing the test.1.3 This specification includes many dimensional require-ments that are, for the most part, in agreement with the BritishStandards Institution, German Standards Institute, Interna-tional Committee for Standardization in Haematology, and theNational Committee for Clinical Laboratory Stan

5、dards publi-cations on Westergren tubes. The clinical procedure using thetube described in this specification is known as the “Wester-gren Method.”1.4 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this sta

6、ndard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2E 438 Specification for Glasses in Laboratory ApparatusE 920 Specification for Commercially Packaged LaboratoryApparatusE 921

7、 Specification for Export Packaged Laboratory Appa-ratusE 1133 Practice for Performance Testing of Packaged Labo-ratory Apparatus for United States Government Procure-mentsE 1157 Specification for Sampling and Testing of ReusableLaboratory Glassware3. Terminology3.1 Definitions of Terms Specific to

8、This Standard:3.1.1 reusablecapable of being used again.3.1.2 tubethe word “tube” rather than “pipet” is used todescribe this instrument. The word “pipet” should be reservedfor volume-measuring instruments thus designated. A tubeused for measurements of blood sedimentation rate is not avolume measur

9、ing instrument. In this connection, misunder-standing can occur when a Westergren “tube” is described as a“pipet.”3.1.3 WestergrenThe surname of the individual respon-sible for the design of the Westergren tube and the method ofuse.4. Classification4.1 This specification covers a tube that is intend

10、ed to beused until it is no longer considered functional for the purposeintended. The specification is specifically written for a reusableitem and is not to be confused with a disposable tube that isdescribed in other published standards.5. Materials5.1 The tubes made to this specification shall be

11、fabricatedfrom borosilicate glass, Type I, Class B; or soda lime glass,Type II, in accordance with Specification E 438.6. Dimensions, Mass, and Permissible Variations6.1 DesignThe Westergren tube shall be made of thick-walled glass tubing. It shall be of one-piece construction,straight and with unif

12、orm bore. The ends of the tube shall beground flat, perpendicular to the tube axis and beveled asspecified in Fig. 1.6.2 DimensionsThe tube shall be made of tubing with anoutside diameter (OD) of 6.5 6 0.5 mm with an insidediameter (ID) of 2.55 mm 6 0.15 mm. The uniformity of thebore shall be 6 0.1

13、mm throughout the tube. The tube shall be3006 1 mm long and ground and beveled at each end. The tube1This specification is under the jurisdiction of ASTM Committee E41 onLaboratory Apparatus and is the direct responsibility of Subcommittee E41.01 onApparatusCurrent edition approved Nov. 1, 2008. Pub

14、lished January 2009. Originallyapproved in 1983. Last previous edition approved in 2003 as E 923 97 (2003).2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the stand

15、ards Document Summary page onthe ASTM website.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.shall have an inscribed graduated scale extending over thelower 200 6 0.35 mm of the tube. The tube should containapproximately 1 mL of blo

16、od when filled and adjusted to the200 mm line. The word “Westergren” must be inscribed on thetop portion of the tube together with the makers or vendorsname or mark.6.3 Graduation LinesThe graduation lines shall be ofuniform thickness with a maximum thickness of 0.25 mm foretched and filled lines an

17、d 0.4 mm for amber stain lines that arefired into the glass tube. They shall lie in planes at right anglesto the axis of the tube and with a maximum tolerance betweentwo adjacent markings of 0.2 mm. Maximum tolerance for thetotal 200 mm scale shall not exceed 0.35 mm.6.4 Graduation Line NumberingThe

18、 tube shall be gradu-ated in millimetres with a scale of 200 mm from the tip of thetube. The scale shall be numbered every ten or twentygraduation lines starting with a numerical zero (0) and down-ward to a maximum value of 190 mm. The numerical markingsshall appear at the right side of the graduate

19、d scale when heldvertically with the scale facing the viewer.6.5 Length of Graduation LinesThe top graduation lineand every other tenth- or twentieth-numbered line shall en-circle, or near encircle the tube or be a minimum of 6 mm long.The medium (every fifth) line shall be a minimum of 4 mmlong. Th

20、e short (intermediate) lines shall be a minimum of 2.5mm long.6.6 Marking PermanencyInscriptions, graduation lines,and numerals shall be either etched and filled with a permanentpigment, or an amber stain fired into the glass tube. The colordepth of the markings on the tube shall be adequate to perm

21、itroutine functional use of the tube without creating a difficultyin setting a meniscus or reading the separation of blood cellsfrom plasma. The permanency of the markings shall meet therequirements of the test described in 7.1.6.7 Grinding BevelThe grinding bevel at the Westergrentube tip has an al

22、lowance of 2 to 8 mm in length. To minimizethe incidence of chipping, it is recommended the minimumwall thickness at the orifice of 0.5 mm be applicable for agrinding bevel length of 2 to 5 mm and a minimum of 0.7 mmwall thickness at the orifice for a grinding bevel of 5 to 8 mm.7. Workmanship, Fini

23、sh, and Appearance7.1 WorkmanshipThe tube shall be as free as possiblefrom visible defects that would detract from its appearance orimpair its serviceability when viewed by the human eye undernormal room lighting. The tube shall be free of ring strain andif present, any longitudinal strain shall be

24、faint and highlydiffused.8. Test Method8.1 Pigmentation and Amber Stain TestFreshly prepare achromic acid cleaning solution by combining 200 g of sodiumdichromate (Na2Cr2O72H2O), 1000 mL of distilled water,and 1500 mL of sulfuric acid (H2SO4, ACS Reagent 95 to98 %). Immerse the tube in the chromic a

25、cid solution. Let standat room temperature (20 to 25 C) for 15 min. Remove the tubefrom the solution and thoroughly rinse in distilled water. Drythe tube by rubbing vigorously, 5 to 10 strokes, with alaboratory cloth or tissue. The appearance of the markingsshould be the same as before the test, whe

26、n judged by the eyeunder normal room lighting.8.2 For additional sampling and testing data, see Specifica-tion E 1157.9. Packaging9.1 For packaging, select from either Specification E 920,E 921, or Practice E 1133.FIG. 1 Westergren TubeE 923 97 (2008)210. Keywords10.1 blood; glass; reusable; sedimen

27、tation rate; westergrenASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringem

28、ent of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or

29、 for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views kn

30、own to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).E 923 97 (2008)3