SAE AMS 3021D-2007 Fluid Reference for Testing Di-Ester (Polyol) Resistant Material《耐二酯(多元醇)材料测试用参考流体》.pdf

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1、 SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising theref

2、rom, is the sole responsibility of the user.” SAE reviews each technical report at least every five years at which time it may be reaffirmed, revised, or cancelled. SAE invites your written comments and suggestions. Copyright 2007 SAE International All rights reserved. No part of this publication ma

3、y be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE. TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada) Tel: 724-776-4970 (outside USA)

4、Fax: 724-776-0790 Email: custsvcsae.org SAE WEB ADDRESS: http:/www.sae.org AMS 3021D AEROSPACE MATERIAL SPECIFICATION Issued AUG 1979 Reaffirmed MAR 2004 Revised JAN 2007 Superseding AMS 3021C Fluid, Reference for Testing Di-Ester (Polyol) Resistant Material RATIONALE To revise source of fluid. 1. S

5、COPE 1.1 Form This specification covers a neopentyl polyol ester fluid. 1.2 Application This fluid has been used typically to evaluate the ability of elastomeric and other polymeric compounds to conform to designated requirements after immersion in the fluid at a specific temperature and time, as re

6、quired by an applicable specification, and its use is limited to such applications. This fluid is not intended for operational use in gas turbine engines (See 8.2). Each application should be considered separately. 1.3 Safety - Hazardous Materials While the materials, methods, applications, and proc

7、esses described or referenced in this specification may involve the use of hazardous materials, this specification does not address the hazards which may be involved in such use. It is the sole responsibility of the user to ensure familiarity with the safe and proper use of any hazardous materials a

8、nd to take necessary precautionary measures to ensure the health and safety of all personnel involved. 2. APPLICABLE DOCUMENTS The issue of the following documents in effect on the date of the purchase order forms a part of this specification to the extent specified herein. The supplier may work to

9、a subsequent revision of a document unless a specific document issue is specified. When the referenced document has been cancelled and no superseding document has been specified, the last published issue of that document shall apply. 2.1 SAE Publications Available from SAE International, 400 Commonw

10、ealth Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada) or 724-776-4970 (outside USA), www.sae.org. AMS 2825 Material Safety Data Sheets Copyright SAE International Provided by IHS under license with SAENot for ResaleNo reproduction or networking permitted without license f

11、rom IHS-,-,-SAE AMS 3021D - 2 - 2.2 ASTM Publications Available from ASTM International, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, Tel: 610-832-9585, www.astm.org. ASTM D 445 Kinematic Viscosity of Transparent and Opaque Liquids (and the Calculation of Dynamic Viscosity

12、) ASTM D 664 Neutralization Number by Potentiometric Titration ASTM D 1218 Refractive Index and Refractive Dispersion of Hydrocarbon Liquids ASTM D 1298 Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method ASTM D 1744 Wate

13、r in Liquid Petroleum Products by Karl Fischer Reagent ASTM D 4057 Manual Sampling of Petroleum and Petroleum Products 3. TECHNICAL REQUIREMENTS 3.1 Material Test fluid shall consist of a refined product of neopentyl ester with 0.5% phenothiazine added as an antioxidant. 3.2 Properties The product s

14、hall conform to the requirements shown in Table 1; tests shall be performed on the fluid supplied and in accordance with specified test methods. TABLE 1 - PROPERTIES Paragraph Property Requirement Test Method3.2.1 Specific Gravity at 60/60 F (16/16 C) 0.961 to 0.967 ASTM D 12983.2.2 Viscosity at 100

15、 F (38 C) 14.60 to 15.60 cst ASTM D 445 3.2.3 Viscosity at 210 F (99 C) 3.0 to 4.0 cst ASTM D 445 3.2.4 Acid Number, max 0.10 milligrams KOH/gram ASTM D 664 3.2.5 Water Content by weight, max 0.10% ASTM D 17443.2.6 Refractive Index at 73 F (23 C) 1.449 to 1.455 ASTM D 12183.2.7 C7 Acid Component, mi

16、n 93% 4.5 3.2.8 Hydroxyl Content, max 0.1% 4.5 3.3 Quality The fluid, as received by purchaser, shall be free from water, sediment, and suspended matter. The odor shall not be irritating or nauseating. No substance of known toxicity under normal conditions of handling and use shall be present. 4. QU

17、ALITY ASSURANCE PROVISIONS 4.1 Responsibility for Inspection The manufacturer of fluid shall be responsible for the performance of all required tests. Purchaser reserves the right to sample and to perform any confirmatory testing deemed necessary to ensure that the fluid conforms to specified requir

18、ements. 4.2 Classification of Tests All technical requirements are acceptance tests and shall be performed prior to shipment of fluid by the manufacturer. Copyright SAE International Provided by IHS under license with SAENot for ResaleNo reproduction or networking permitted without license from IHS-

19、,-,-SAE AMS 3021D - 3 - 4.3 Sampling and Testing Shall be in accordance with ASTM D 4057. The number of determinations for each requirement shall be as specified in the applicable test procedure or, if not specified therein, not less than three. 4.3.1 A lot shall be all fluid from one batch presente

20、d for manufacturers inspection at one time. 4.3.2 When a statistical sampling plan has been agreed upon by purchaser and supplier, sampling shall be in accordance with such plan in lieu of sampling as in 4.3 and the report of 4.6 shall state that such plan was used. 4.4 Approval If requested by purc

21、haser, sample fluid shall be submitted for approval by the purchaser before fluid for production use is supplied. If necessary to make any change in ingredients, in type of equipment for processing, or in manufacturing procedures, manufacturer shall submit for reapproval a statement of the proposed

22、changes in ingredients and/or processing and, when requested, sample fluid (See 8.5). Production fluid made by the revised procedure shall not be shipped prior to receipt of approval. 4.5 Test Methods Shall be as agreed upon by purchaser and manufacturer for determining the C7 acid component (3.2.7)

23、 and hydroxyl content (3.2.8). 4.6 Reports The supplier of fluid shall furnish with each shipment a report from the manufacturer, showing the results of tests to determine conformance to the technical requirements. This report shall include the purchase order number, lot number, AMS 3021D, manufactu

24、rers identification, and quantity. 4.6.1 A material safety data sheet conforming to AMS 2825, or equivalent, shall be supplied to each purchaser prior to, or with the first shipment of fluid. 4.7 Resampling and Retesting If any sample used in the above tests fails to meet the specified requirements,

25、 disposition of the fluid may be based on the results of testing three additional samples for each original nonconforming sample. Failure of any retest sample to meet the specified requirements shall be cause for rejection of the fluid represented. Results of all tests shall be reported. 5. PREPARAT

26、ION FOR DELIVERY 5.1 Packaging and Identification 5.1.1 A lot of fluid may be packaged in small quantities and delivered under the basic lot approval provided lot identification is maintained. 5.1.2 The fluid shall be packaged in airtight containers of such size and design as to keep ullage to a min

27、imum. 5.1.3 Each container of fluid shall be legibly identified, with not less than the following information on an attached label, using characters which will not be obliterated by normal handling: FLUID, REFERENCE, FOR TESTING DI-ESTER (POLYOL) RESISTANT MATERIAL AMS 3021D PURCHASE ORDER NUMBER MA

28、NUFACTURERS IDENTIFICATION LOT (OR BATCH) NUMBER QUANTITY APPROPRIATE WARNINGS OR PRECAUTIONARY NOTICES Copyright SAE International Provided by IHS under license with SAENot for ResaleNo reproduction or networking permitted without license from IHS-,-,-SAE AMS 3021D - 4 - 5.1.4 Containers of fluid s

29、hall be prepared for shipment in accordance with commercial practice and in compliance with applicable rules and regulations pertaining to the handling, packaging and transportation of the fluid to ensure carrier acceptance and safe delivery. 6. ACKNOWLEDGMENT A supplier shall mention this specifica

30、tion number and its revision letter in all quotations and when acknowledging purchase orders. 7. REJECTIONS Fluid not conforming to this specification, or to modifications authorized by purchaser, will be subject to rejection. 8. NOTES 8.1 The change bar (l) located in the left margin is for the con

31、venience of the user in locating areas where technical revisions, not editorial changes, have been made to the previous issue of this specification. An (R) symbol to the left of the document title indicates a complete revision of the specification. 8.2 This fluid is intended for use in evaluating th

32、e response of materials in contact with, or immersion in, MIL-PRF-7808 and similar lubricants. 8.3 This fluid is also known Hatco 7700 and can be purchased from: Hatco Corporation Domestic Order Desk Attention: Loretta Gimbert Phone: 1 732 738 3600 Fax: 1 732 738 9385 Email: 8.4 Terms used in AMS a

33、re clarified in ARP1917. 8.5 Dimensions and properties in inch/pound units and the Fahrenheit temperatures are primary; dimensions and properties in SI units and the Celsius temperatures are shown as the approximate equivalents of the primary units and are presented only for information. 8.6 Purchas

34、e documents should specify not less than the following: AMS 3021D Size of containers desired Quantity of fluid desired Special packaging, if required. PREPARED BY AMS COMMITTEE “CE” Copyright SAE International Provided by IHS under license with SAENot for ResaleNo reproduction or networking permitted without license from IHS-,-,-