ASTM D975-2017a Standard Specification for Diesel Fuel Oils.pdf

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1、Designation: D975 17D975 17aStandard Specification forDiesel Fuel Oils1This standard is issued under the fixed designation D975; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in parentheses ind

2、icates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the U.S. Department of Defense.1. Scope*1.1 This specification covers seven grades of diesel fuel oils suitable for v

3、arious types of diesel engines. These grades aredescribed as follows:1.1.1 Grade No. 1-D S15A special-purpose, light middle distillate fuel for use in diesel engine applications requiring a fuelwith 15 ppm sulfur (maximum) and higher volatility than that provided by Grade No. 2-D S15 fuel.21.1.2 Gra

4、de No. 1-D S500A special-purpose, light middle distillate fuel for use in diesel engine applications requiring a fuelwith 500 ppm sulfur (maximum) and higher volatility than that provided by Grade No. 2-D S500 fuel.21.1.3 Grade No. 1-D S5000Aspecial-purpose, light middle distillate fuel for use in d

5、iesel engine applications requiring a fuelwith 5000 ppm sulfur (maximum) and higher volatility than that provided by Grade No. 2-D S5000 fuels.1.1.4 Grade No. 2-D S15A general purpose, middle distillate fuel for use in diesel engine applications requiring a fuel with15 ppm sulfur (maximum). It is es

6、pecially suitable for use in applications with conditions of varying speed and load.21.1.5 Grade No. 2-D S500A general-purpose, middle distillate fuel for use in diesel engine applications requiring a fuel with500 ppm sulfur (maximum). It is especially suitable for use in applications with condition

7、s of varying speed and load.21.1.6 Grade No. 2-D S5000Ageneral-purpose, middle distillate fuel for use in diesel engine applications requiring a fuel with5000 ppm sulfur (maximum), especially in conditions of varying speed and load.1.1.7 Grade No. 4-DA heavy distillate fuel, or a blend of distillate

8、 and residual oil, for use in low- and medium-speed dieselengines in applications involving predominantly constant speed and load.NOTE 1A more detailed description of the grades of diesel fuel oils is given in X1.2.NOTE 2The Sxxx designation has been adopted to distinguish grades by sulfur rather th

9、an using words such as “Low Sulfur” as previously becausethe number of sulfur grades is growing and the word descriptions were thought to be not precise. S5000 grades correspond to the so-called “regular” sulfurgrades, the previous No. 1-D and No. 2-D. S500 grades correspond to the previous “Low Sul

10、fur” grades. S15 grades were not in the previous grade systemand are commonly referred to as “Ultra-Low Sulfur” grades or ULSD.1.2 This specification, unless otherwise provided by agreement between the purchaser and the supplier, prescribes the requiredproperties of diesel fuels at the time and plac

11、e of delivery.1.2.1 Nothing in this specification shall preclude observance of federal, state, or local regulations which can be more restrictive.NOTE 3The generation and dissipation of static electricity can create problems in the handling of distillate diesel fuel oils. For more information onthe

12、subject, see Guide D4865.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This international standard was developed in accordance with internationally recognized principles on standardizationestablished in the Decision

13、on Principles for the Development of International Standards, Guides and Recommendations issuedby the World Trade Organization Technical Barriers to Trade (TBT) Committee.2. Referenced Documents2.1 ASTM Standards:3D56 Test Method for Flash Point by Tag Closed Cup Tester1 This specification is under

14、the jurisdiction ofASTM Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of SubcommitteeD02.E0 on Burner, Diesel, Non-Aviation Gas Turbine, and Marine Fuels.Current edition approved May 1, 2017Dec. 15, 2017. Published May 2017January 2018. Originally

15、 approved in 1948. Last previous edition approved in 20162017 asD975 16a.D975 17. DOI: 10.1520/D0975-17.10.1520/D0975-17A.2 This fuel complies with 40 CFR Part 80Control of Air Pollution from New Motor Vehicles: HeavyDuty Engines and Vehicle Standards and Highway Diesel FuelSulfur Control Requiremen

16、ts: Final Rule. Regulation of Fuels and Fuel Additives: Fuel Quality Regulations for Highway Diesel Fuel Sold in 1993 and Later Calendar Years.3 For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at serviceastm.org. For Annual Book of ASTM Standardsvol

17、ume information, refer to the standards Document Summary page on the ASTM website.This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Becauseit may not be technically possible to adeq

18、uately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current versionof the standard as published by ASTM is to be considered the official document.*A Summary of Changes section appears at the end of this standardCopyright ASTM

19、International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States1D86 Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric PressureD93 Test Methods for Flash Point by Pensky-Martens Closed Cup TesterD129 Test Method for Sulfur in Petrole

20、um Products (General High Pressure Decomposition Device Method)D130 Test Method for Corrosiveness to Copper from Petroleum Products by Copper Strip TestD445 Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)D482 Test Method for Ash from Petro

21、leum ProductsD524 Test Method for Ramsbottom Carbon Residue of Petroleum ProductsD613 Test Method for Cetane Number of Diesel Fuel OilD1266 Test Method for Sulfur in Petroleum Products (Lamp Method)D1319 Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorpti

22、onD1552 Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or ThermalConductivity Detection (TCD)D1796 Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)D2274 Test Method for Oxidation Stability of Dist

23、illate Fuel Oil (Accelerated Method)D2500 Test Method for Cloud Point of Petroleum Products and Liquid FuelsD2622 Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence SpectrometryD2624 Test Methods for Electrical Conductivity of Aviation and Distillate FuelsD2709

24、Test Method for Water and Sediment in Middle Distillate Fuels by CentrifugeD2880 Specification for Gas Turbine Fuel OilsD2887 Test Method for Boiling Range Distribution of Petroleum Fractions by Gas ChromatographyD3117 Test Method for Wax Appearance Point of Distillate Fuels (Withdrawn 2010)4D3120 T

25、est Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative MicrocoulometryD3828 Test Methods for Flash Point by Small Scale Closed Cup TesterD4057 Practice for Manual Sampling of Petroleum and Petroleum ProductsD4177 Practice for Automatic Sampling of Petroleum and

26、 Petroleum ProductsD4294 Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence SpectrometryD4306 Practice for Aviation Fuel Sample Containers for Tests Affected by Trace ContaminationD4308 Test Method for Electrical Conductivity of Liquid Hydrocarbons by

27、Precision MeterD4539 Test Method for Filterability of Diesel Fuels by Low-Temperature Flow Test (LTFT)D4737 Test Method for Calculated Cetane Index by Four Variable EquationD4865 Guide for Generation and Dissipation of Static Electricity in Petroleum Fuel SystemsD5304 Test Method for Assessing Middl

28、e Distillate Fuel Storage Stability by Oxygen OverpressureD5453 Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel,and Engine Oil by Ultraviolet FluorescenceD5771 Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Opti

29、cal Detection Stepped Cooling Method)D5772 Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Linear Cooling Rate Method)D5773 Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Constant Cooling Rate Method)D5842 Practice for Sampling and Handling of Fuels for Volat

30、ility MeasurementD5854 Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum ProductsD6078 Test Method for Evaluating Lubricity of Diesel Fuels by the Scuffing Load Ball-on-Cylinder Lubricity Evaluator(SLBOCLE)D6079 Test Method for Evaluating Lubricity of Diesel Fuels by the

31、High-Frequency Reciprocating Rig (HFRR)D6217 Test Method for Particulate Contamination in Middle Distillate Fuels by Laboratory FiltrationD6304 Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric KarlFischer TitrationD6371 Test Method for Cold

32、 Filter Plugging Point of Diesel and Heating FuelsD6468 Test Method for High Temperature Stability of Middle Distillate FuelsD6469 Guide for Microbial Contamination in Fuels and Fuel SystemsD6751 Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate FuelsD6890 Test Method for Det

33、ermination of Ignition Delay and Derived Cetane Number (DCN) of Diesel Fuel Oils by Combustionin a Constant Volume ChamberD6898 Test Method for Evaluating Diesel Fuel Lubricity by an Injection Pump RigD7039 Test Method for Sulfur in Gasoline, Diesel Fuel, Jet Fuel, Kerosine, Biodiesel, Biodiesel Ble

34、nds, and Gasoline-EthanolBlends by Monochromatic Wavelength Dispersive X-ray Fluorescence SpectrometryD7042 Test Method for Dynamic Viscosity and Density of Liquids by Stabinger Viscometer (and the Calculation of KinematicViscosity)4 The last approved version of this historical standard is reference

35、d on www.astm.org.D975 17a2D7094 Test Method for Flash Point by Modified Continuously Closed Cup (MCCCFP) TesterD7170 Test Method for Determination of Derived Cetane Number (DCN) of Diesel Fuel OilsFixed Range Injection Period,Constant Volume Combustion Chamber MethodD7220 Test Method for Sulfur inA

36、utomotive, Heating, and Jet Fuels by Monochromatic Energy Dispersive X-ray FluorescenceSpectrometryD7345 Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure (Micro DistillationMethod)D7371 Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) C

37、ontent in Diesel Fuel Oil Using Mid InfraredSpectroscopy (FTIR-ATR-PLS Method)D7467 Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)D7545 Test Method for Oxidation Stability of Middle Distillate FuelsRapid Small Scale Oxidation Test (RSSOT)D7619 Test Method for Sizing and Counting Part

38、icles in Light and Middle Distillate Fuels, by Automatic Particle CounterD7668 Test Method for Determination of Derived Cetane Number (DCN) of Diesel Fuel OilsIgnition Delay and CombustionDelay Using a Constant Volume Combustion Chamber MethodD7683 Test Method for Cloud Point of Petroleum Products a

39、nd Liquid Fuels (Small Test Jar Method)D7688 Test Method for Evaluating Lubricity of Diesel Fuels by the High-Frequency Reciprocating Rig (HFRR) by VisualObservationD7689 Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Mini Method)D7861 Test Method for Determination of FattyAcid

40、Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF)ArrayBased Mid-Infrared SpectroscopyE29 Practice for Using Significant Digits in Test Data to Determine Conformance with SpecificationsE1064 Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration2.2 Other Docu

41、ments:26 CFR Part 48 Manufacturers and Realtors Excise Taxes540 CFR Part 80 Regulation of Fuels and Fuel Additives5API RP 2003 Protection Against Ignitions Arising Out of Static, Lightning, and Stray Currents6EN 14078 Liquid petroleum productsDetermination of fatty acid methyl esters (FAME) in middl

42、e distillatesInfraredspectroscopy method7EN 15751 Automotive fuels - Fatty acid methyl ester (FAME) fuel and blends with diesel fuel - Determination of oxidationstability by accelerated oxidation method7ISO 4406 Hydraulic Fluid PowerFluidsMethod for Coding the Level of Contamination by Solid Particl

43、es6ISO 16889 Hydraulic Fluid PowerFiltersMulti-pass Method for Evaluating Filtration Performance of a Filter Element3. Terminology3.1 Definitions:3.1.1 additive, nin fuel oils, a substance added to fuel oil at a blend level not greater than 1 % by volume of the finished fuel.3.1.1.1 DiscussionAdditi

44、ves are generally included in finished fuel oil to enhance performance properties (for example, cetane number, lubricity, coldflow, etc.).3.1.1.2 DiscussionAdditives that contain hydrocarbon oil blended with other substances may exclude the hydrocarbon oil portion for determinationof the volume perc

45、ent of the additive in the finished fuel.3.1.2 alternative blendstock, nin fuel oils, a non-hydrocarbon oil substance added to fuel oil at blend levels greater than 1 %by volume of the finished fuel.3.1.2.1 DiscussionAn alternative blendstock should normally have an industry consensus standard or an

46、 annex in this specification that defines itsphysical and chemical properties.5 Available from U.S. Government Printing Office, Superintendent of Documents, 732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401.6 Available from American National Standards Institute (ANSI), 25 W. 43rd St., 4th

47、 Floor, New York, NY 10036, http:/www.ansi.org.7 Available from the National CEN members listed on the CEN website (www.cenorm.be) or from the CEN/TC 19 Secretariat (astm.nen.nl).D975 17a33.1.2.2 DiscussionSee Appendix X7 for guidance regarding new materials for #1-D and #2-D grades of diesel fuels.

48、3.1.3 biodiesel, nfuel comprised of mono-alkyl esters of long chain fatty acids derived from vegetable oils or animal fats,designated B100.3.1.4 biodiesel blend (BXX), nblend of biodiesel fuel with diesel fuel oils.3.1.4.1 DiscussionIn the abbreviation, BXX, the XX represents the volume percentage o

49、f biodiesel fuel in the blend.3.1.5 hydrocarbon oil, na homogeneous mixture with elemental composition primarily of carbon and hydrogen that may alsocontain sulfur, oxygen, or nitrogen from residual impurities and contaminants associated with the fuels raw materials andmanufacturing processes and excluding added oxygenated materials.3.1.5.1 DiscussionNeither macro nor micro emulsions are included in this definition since neither are homogeneous mixtures.3.1.5.2 DiscussionExamples of excluded oxygenated materials are alcohols, esters, ethers,