ARMY UFGS-01 35 45 00 10-2006 CHEMICAL DATA QUALITY CONTROL《化学物质数据质量控制(代替 ARMY UFGS-01450A 07 01 04 ARMY UFGS-01450A)》.pdf

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1、*USACE / NAVFAC / AFCESA / NASA UFGS-01 35 45.00 10 (April 2006)-Preparing Activity: USACE Replacing without changeUFGS-01450A (July 2004)UNIFIED FACILITIES GUIDE SPECIFICATIONSReferences are in agreement with UMRL dated 1 April 2006Latest change indicated by CHG tags*SECTION TABLE OF CONTENTSDIVISI

2、ON 01 - GENERAL REQUIREMENTSSECTION 01 35 45.00 10CHEMICAL DATA QUALITY CONTROL04/06PART 1 GENERAL1.1 REFERENCES1.2 ACRONYMS1.3 MEASUREMENT AND PAYMENT1.4 CHEMISTRY REQUIREMENTS1.4.1 Site History1.4.2 Data Quality Objectives (DQO)1.4.3 Sampling, Analysis and Measurement1.4.3.1 Soil/Sediment and Grou

3、nd/Surface Water Samples1.4.3.2 Process Solid and Liquid Samples1.4.3.3 Borrow or Fill Material Samples1.4.3.4 Investigation Derived Waste Samples1.4.3.5 Manifesting Samples1.4.3.6 Process Gas and Particulate Emission Samples1.4.3.7 Real-Time Instrumental Measurement Samples1.4.3.8 Perimeter Air Mon

4、itoring Samples1.4.3.9 Compatibility Field Testing for Bulking Operations1.4.3.10 Demolition Samples1.4.3.11 Field Screening1.5 SUBMITTALS1.6 QUALITY ASSURANCE ELEMENTS1.6.1 Laboratory Validation Requirements1.6.2 QA Sample Collection and Analysis1.6.3 Single or Double Blind Performance Evaluation S

5、amples1.6.4 Review of Primary Laboratory Data1.6.5 Validation of Data1.6.6 Electronic Tape Audits1.7 QUALIFICATIONS1.7.1 Chemical Quality Control Officer1.7.2 Project Chemist1.7.3 Environmental Sampler1.8 COORDINATION MEETINGSECTION 01 35 45.00 10 Page 1Provided by IHSNot for ResaleNo reproduction o

6、r networking permitted without license from IHS-,-,-PART 2 PRODUCTS (NOT APPLICABLE)PART 3 EXECUTION3.1 GENERAL REQUIREMENTS3.2 QUALITY CONTROL PLAN3.2.1 Additional Requirements3.2.2 Chemistry Elements of the CQC Plan3.2.2.1 Qualifications3.2.2.2 Authority and Responsibility3.3 SAMPLING AND ANALYSIS

7、 PLAN3.3.1 Field Sampling Plan3.3.2 Quality Assurance Project Plan3.4 CHEMISTRY DATA PACKAGE3.5 CONTROL OF CHEMICAL DATA QUALITY3.6 ANALYTICAL TESTING LABORATORIES3.6.1 Laboratory Analytical Requirements3.6.2 Laboratory Performance3.7 CHEMICAL DATA FINAL REPORT3.8 DOCUMENTATION3.9 NOTIFICATION OF NO

8、N-COMPLIANCE- End of Section Table of Contents -SECTION 01 35 45.00 10 Page 2Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-*USACE / NAVFAC / AFCESA / NASA UFGS-01 35 45.00 10 (April 2006)-Preparing Activity: USACE Replacing without changeUFGS-01450

9、A (July 2004)UNIFIED FACILITIES GUIDE SPECIFICATIONSReferences are in agreement with UMRL dated 1 April 2006Latest change indicated by CHG tags*SECTION 01 35 45.00 10CHEMICAL DATA QUALITY CONTROL04/06*NOTE: This guide specification covers requirements for Chemical Data Quality Control (CDQC) for rem

10、edial and removal actions at Hazardous, Toxic, and Radioactive Waste (HTRW) contaminated sites.Comments and suggestions on this guide specification are welcome and should be directed to the technical proponent of the specification. A listing of technical proponents, including their organization desi

11、gnation and telephone number, is on the Internet.Recommended changes to a UFGS should be submitted as a Criteria Change Request (CCR).Use of electronic communication is encouraged.Brackets are used in the text to indicate designer choices or locations where text must be supplied by the designer.*PAR

12、T 1 GENERAL*NOTE: This specification is applicable to remedial and removal actions involving HTRW that are conducted by the U.S. Army Corps of Engineers (USACE). It includes the collection and analysis of environmental samples and process parameter measurements required for the pre-remedial activiti

13、es, remediation, and post remediation phases. This includes chemical measurements of soil, water, air, and other chemical parameters required for Defense Environmental Restoration Program (DERP), Base Realignment and Closure (BRAC), installation environmental compliance, military construction, super

14、fund, civil works, and other construction projects involving HTRW.SECTION 01 35 45.00 10 Page 3Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-*1.1 REFERENCES*NOTE: This paragraph is used to list the publications cited in the text of the guide specif

15、ication. The publications are referred to in the text by basic designation only and listed in this paragraph by organization, designation, date, and title.Use the Reference Wizards Check Reference feature when you add a RID outside of the Sections Reference Article to automatically place the referen

16、ce in the Reference Article. Also use the Reference Wizards Check Reference feature to update the issue dates.References not used in the text will automatically be deleted from this section of the project specification when you choose to reconcile references in the publish print process.Publications

17、 included in this guide specification are applicable to chemical data quality control for HTRW remedial actions. Include all references necessary to attain project Data Quality Objectives (DQO). References for sampling and/or analytical procedures must be for the most recent update of the method. In

18、clude in the specification additional references that are unique to the project such as the Record of Decision (ROD), Federal, state and local Applicable or Relevant and Appropriate Requirements (ARAR), remedial and innovative technology requirements, unique contaminants, etc. Use references in the

19、CDQC section which are compatible with references in other sections of the specification. The designer should state in the specification whether a reference is mandatory or provided as guidance.*The publications listed below form a part of this specification to the extent referenced. The publication

20、s are referred to within the text by the basic designation only.U.S. ARMY CENTER FOR HEALTH PROMOTION AND PREVENTIVE MEDICINE (USACHPPM)USACHPPM Protocol (1993) Sampling Protocol Building Demolition Debris and Buildings Painted with Lead-Based PaintU.S. ARMY CORPS OF ENGINEERS (USACE)EM 200-1-1 (199

21、4) Validation of Analytical Chemistry LaboratoriesSECTION 01 35 45.00 10 Page 4Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-EM 200-1-3 (2001) Requirements for the Preparation of Sampling and Analysis PlansEM 200-1-6 (1997) Chemical Quality Assuran

22、ce for HTRW ProjectsER 1110-1-263 (1998) Chemical Data Quality Management for Hazardous, Toxic, Radioactive Waste Remedial ActivitiesU.S. ENVIRONMENTAL PROTECTION AGENCY (EPA)EPA 540/R 94-008 (1999) USEPA Contract Laboratory Program National Functional Guidelines for Organic Data ReviewEPA SW-846.3-

23、3 (1999, Third Edition, Update III-A) Test Methods for Evaluating Solid Waste: Physical/Chemical MethodsU.S. NATIONAL ARCHIVES AND RECORDS ADMINISTRATION (NARA)40 CFR 261 Identification and Listing of Hazardous Waste40 CFR 262 Standards Applicable to Generators of Hazardous Waste40 CFR 268 Land Disp

24、osal Restrictions49 CFR 172 Hazardous Materials Table, Special Provisions, Hazardous Materials Communications, Emergency Response Information, and Training Requirements49 CFR 178 Specifications for Packagings1.2 ACRONYMS*NOTE: Acronyms included in this UFGS are defined in the specification language,

25、 but are not required for all projects. Define all acronyms used in this section. Acronyms included in the CDQC section must not conflict and must be compatible with definitions and acronyms in other sections of the specification.*The definition of acronyms used by the Contractor that pertain to che

26、mical data quality control shall be clearly defined for all contract related products and communications.1.3 MEASUREMENT AND PAYMENT*NOTE: For some remedial action contracts, chemical parameter measurement may be acquired by both lump sum pricing and additional unit pricing. Unless adequately addres

27、sed in the Special Contract SECTION 01 35 45.00 10 Page 5Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-Requirements section of the contract, make clear what chemical measurement pricing procedures are to be used for the contract and that payment wi

28、ll be withheld pending Government Approval (GA) of the chemical data final report. The designer should coordinate this paragraph with the bidding schedule.*Separate payment will not be made for providing and maintaining the chemical data quality requirements including the chemical data quality manag

29、ement, chemical data validation, minimum chemical data reporting requirements, and chemical data quality submittal requirements; these costs shall be included in the applicable unit prices or lump sum prices contained in the bidding schedule.1.4 CHEMISTRY REQUIREMENTS*NOTE: The designer may include

30、chemistry elements in other sections of the specification; however, all elements of chemical data quality control required by this guide specification must be included in that section or the chemistry must also be included in this section of the specification. In addition, the designer should review

31、 or have the Contractor review other sections of the specification to extract the list of sampling and analysis requirements.*Chemical Data Quality Control (CDQC) shall be as defined in ER 1110-1-263; this ER, which integrates USACE guidance on the subject, shall be supplemented by EM 200-1-6 for de

32、tail technical guidance on CDQC. Tables and charts defining Design Analysis (DA), ROD, and remedial technology specific chemistry shall be according to or consistent with EM 200-1-3.1.4.1 Site History*NOTE: The designer should provide a sufficient site history for the Contractor to meet the informat

33、ion requirements of the Sampling and Analysis Plan (SAP). The information in the Contractors SAP must provide field and laboratory personnel all necessary site specific chemical data. Include references containing this information.*_1.4.2 Data Quality Objectives (DQO)*NOTE: It is the responsibility

34、of the designer to identify and define chemical DQO in the construction specification either as previously determined in the DA, ROD, other decision documents or developed in accordance with EM 200-1-2. As prescribed within EM 200-1-2, the designers technical planning team is responsible for develop

35、ing project-specific data SECTION 01 35 45.00 10 Page 6Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-collection programs that define the quality and quantity of data needed to perform all the engineering and scientific evaluations required for the

36、project. Data users will determine initial data needs in order to perform specific evaluations and make the engineering and scientific judgments required to complete the necessary activities leading to site closeout. Implementors provide input to planning specific data collection tasks and are respo

37、nsible for task execution.*Sample acquisition, chemical analysis and chemical parameter measurements shall be performed so that the resulting data meet and support data use requirements. The chemical data shall be acquired, documented, verified and reported to ensure that the specified precision, ac

38、curacy, representativeness, comparability, completeness and sensitivity requirements are achieved.1.4.3 Sampling, Analysis and Measurement*NOTE: The process to determine number of samples and sample locations should be fully described here. The specification should describe sampling frequency (e.g.

39、per excavated area, per a certain number of cubic meters (yards) of soil, per a certain number of drums) and general procedures for sample locations (e.g. stained areas, grid pattern over the excavated area, center of stockpile). This provides adequate information for the Contractor bid preparation,

40、 as well as for field oversight of Contractor sampling, while allowing the Contractor the flexibility to do the best possible job given each sites unique characteristics.Analytical method requirements for all project chemical measurements must be specified, including number and type of samples to be

41、 collected and instrumental measurements. For National Priority List (NPL) sites, chemical data requirements for delisting the site from the NPL must be defined and included.For each type of sample, provide a table that identifies the number of samples, including Quality Control (QC) and Quality Ass

42、urance (QA) samples, extraction and analytical methods, precision, accuracy, representativeness, comparability, completeness and sensitivity for analytical determinations.*_1.4.3.1 Soil/Sediment and Ground/Surface Water SamplesSoil/sediment and ground/surface water samples shall be collected and ana

43、lyzed and/or shipped to a primary laboratory according to the following SECTION 01 35 45.00 10 Page 7Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-table: _.1.4.3.2 Process Solid and Liquid SamplesProcess solid and liquid samples shall be collected and analyzed and/or shipped to a primary laboratory according to the following table: _.1.4.3.3 Borrow or Fill