DLA MIL-DTL-24293 B-2009 PACKING HYDRAULIC LEATHER CATTLEHIDE MINERAL-TANNED IMPREGNATED.pdf

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1、AMSC N/A FSC 5330 MIL-DTL-24293B 7 JANUARY 2009 SUPERSEDING MIL-P-24293A(SH) 19 August 1987 DETAIL SPECIFICATION PACKING, HYDRAULIC, LEATHER, CATTLEHIDE, MINERAL-TANNED, IMPREGNATED This specification is approved for use by all Departments and Agencies of the Department of Defense. 1. SCOPE 1.1 Scop

2、e. This specification covers packing composed of impregnated, mineral tanned leather. 1.2 Classification. The leather packings are furnished in the following types and weights, as specified (see 6.2): Type I - Impregnated with wax. Type II - Impregnated with liquid polymer of polysulfide rubber. Med

3、ium. Heavy. Extra heavy. 2. APPLICABLE DOCUMENTS 2.1 General. The documents listed in this section are specified in sections 3, 4, or 5 of this standard. This section does not include documents cited in other sections of this standard or recommend for additional information or as examples. While eve

4、ry effort has been made to ensure the completeness of this list, document users are cautioned that they must meet all specified requirements of documents cited in sections 3, 4, or 5 of this standard, whether or not they are listed. 2.2 Government documents. INCH-POUND INACTIVE FOR NEW DESIGN AFTER

5、16 JUNE 1997. Comments, suggestions, or questions on this document should be addressed to Defense Supply Center Philadelphia (DSCP), ATTN: DSCP-NASA, 700 Robbins Avenue, Philadelphia, PA 19111-5096 or e-mail to dscpg&ispecommentsdla.mil . Since contact information can change, you may want to verify

6、the currency of this address information using the ASSIST Online database at http:/assist.daps.dla.mil . Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-DTL-24293B 22.2.1 Specifications, standards, and handbooks. The following specifications and

7、standards form a part of this document to the extent specified herein. Unless otherwise specified, the issues of these documents are those cited in the solicitation or contract. FEDERAL STANDARDS FED-STD-311 Leather, Methods of Sampling and Testing (Copies of these documents are available online at

8、http:/assist.daps.dla.mil/quicksearch/ or from the Standardization Document Order Desk, 700 Robbins Avenue, Building 4D, Philadelphia, PA 19111-5094.) 2.3 Order of precedence. In the event of a conflict between the text of this document and the references cited herein, the text of this document take

9、s precedence. Nothing in this document, however, supersedes applicable laws and regulations unless a specific exemption has been obtained. 3. REQUIREMENTS 3.1 Material. The packing shall be made of cattlehide leather. 3.2 Tannage. The leather packing shall be tanned with chromium salts without the u

10、se of vegetable tanning materials. 3.3 Finish. The leather packing shall be full-grain with the flesh side smooth and free from loose flesh. It may be lightly split or skived to facilitate impregnation. 3.4 Trim. The leather packing shall be in the form of belting butt bends as specified in FED-STD-

11、311. 3.5 Selection. When provided in the form of belting butt bends, the leather packing shall have no defects such as deep cuts, damaged grain, open scratches, open grub holes, brands, hip marks, or any other defects which effect a loss in cutting value greater than 6 percent of the total area. Whe

12、n purchased in the form of finished packing, the leather packing shall be free from defects. 3.6 Thickness for weights. The leather packing shall be furnished in the thickness specified for each weight shown in table I. TABLE I. Thickness for each weight of leather packing. Thickness Weight Minimum

13、Maximum Medium Heavy Extra heavy 64ths inch 8 (.125) 11 (.172) 14 (.219) 64ths inch 10 (.156) 13 (.203) 17 (.266) 3.7 Cracking. The leather packing shall not crack (see 4.5). 3.8 Tensile strength. The tensile strength shall be not less than 2,500 psi (17.24 MPa) for any one specimen (see 4.3). Provi

14、ded by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-DTL-24293B 33.9 Elongation. The elongation under a load of 2,500 psi (17.24 MPa) shall be not more than 30 percent when tested with the long direction parallel to the backbone. When tested in the belly-b

15、elly direction, the elongation shall not exceed the following limits (see 4.3): Medium - 30 percent maximum. Heavy - 35 percent maximum. Extra heavy - 40 percent maximum. 3.10 Shrinkage. The reduction in area of the leather packing shall be not more than 5 percent (see 4.3.2). 3.11 Porosity. The imp

16、regnated leather packing shall show no leakage of water (see 4.3.3). 3.12 Chemical composition. The leather packing shall conform to the chemical composition shown in table II (see 4.3, 4.3.1, and 4.3.5). TABLE II. Chemical composition. Percent by weight Type I Type II Min Max Min Max Chromic oxide

17、1/ Grease (petroleum ether extract) 2/ Impregnating wax (benzol extract) 2/ Chlorides as sodium chloride 1/ Sulfates as sulfuric acid 1/ Total polysulfide polymer (Thiokol) 3/ Chloroform extract 3/ 4.5 8 23 - - - - - 20 30 0.30 0.30 - - 4.5 8 - - - 35 - - 15 - 0.30 0.30 - 15 1/ Moisture, wax, and gr

18、ease-free basis. 2/ Moisture-free basis. 3/ Determined on finished leather packing. Ash and all remaining chemical tests shall be determined on a representative sample prior to application of polysulfide polymer. 3.12.1 Ash (moisture, wax, and grease-free basis). Ash shall be not more than 120 perce

19、nt of the chromic oxide (see 4.3). 3.12.2 Impregnating wax. The leather packing shall be impregnated with a wax having a melting point within the range of 170 to 185 F (76.7 to 85 C). 4. VERIFICATION 4.1 Sampling for conformance inspection. 4.1.1 Inspection lot. All leather packing of the same type

20、and weight presented at one time shall be considered a lot for purposes of inspection. 4.1.2 Sample for examination. A random sample of leather packing units shall be selected in accordance with table III from each inspection lot of material offered for examination of visual and dimensional characte

21、ristics. Acceptance quality level (AQL) equals 1.5 percent defective. Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-DTL-24293B 4TABLE Ill. Sampling for visual and dimensional examination. Number of units in inspection lot Number of units in sam

22、ple Acceptance number (defectives) Rejection number (defectives) 15 and under 16 to 40 41 to 110 111 to 300 301 to 500 501 to 800 801 to 1300 1301 and over 7 10 15 25 35 50 75 110 0 0 0 1 1 2 3 4 1 1 1 2 2 3 4 5 4.1.3 Sampling for tests. Samples for all physical and chemical tests of type I packing

23、and for all physical tests and for the determination of the polysulfide rubber and chloroform extract in type II packing shall be taken from the impregnated packing. Samples for the chromic oxide, chlorides, sulfates, and ash chemical tests on type II packing shall be taken from the unimpregnated pa

24、cking representative of the lot. Sampling shall be in accordance with the sample size of sampling and acceptance procedures of FED-STD-311. 4.1.4 Test specimens. Specimens shall be cut from the sample units selected as specified in 4.1.3 in accordance with figure 1. Physical test specimens shall be

25、cut as shown on figure 2 from piece “A“ shown on figure 1. Specimens for chemical analysis shall be composited from pieces “B“, “C1”,“C2“, and from remainder of “A“ in accordance with method 6002.1 of FED-STD-311. Samples for chemical tests on unimpregnated type II packing shall be composited from p

26、ieces “B“, “C1” and “C2“. 4.2 Conformance inspection. 4.2.1 Visual and dimensional examination. Each of the sample units selected in accordance with table III shall be visually and dimensionally examined to verify conformance to this specification. Any unit in the sample containing one or more visua

27、l or dimensional defects shall be subject to rejection and if the number of defective units in any sample exceeds the acceptance number for that sample, this shall be cause for rejection of the lot represented by the sample. 4.2.2 Conformance tests. Unless otherwise specified, conformance tests shal

28、l include the tests specified in 4.3 for each type and weight. Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-DTL-24293B 54.3 Tests. Tests shall be conducted in accordance with the following methods as specified in FED-STD-311 and as hereinafter

29、 specified: Test Method Moisture Grease (petroleum ether boiling below 176F (80C) Chromic oxide, perchloric acid Soluble chlorides (on grease and wax-free sample) Soluble sulfates (on grease and wax-free sample) Total ash Tensile strength Elongation (at a stress of 2,500psi (17.24 MPa) Cracking, vis

30、e Thickness, unit 6221 6311 6515 6351 6361 6421 2021 2021 4011 1011.1 4.3.1 Impregnating wax (benzol extract). After completing the petroleum ether extraction the same packing and extract with benzol shall be used, using a Soxhlet extractor and keeping the benzol extraction separate from the petrole

31、um ether extraction. The benzol shall be evaporated off and dried to approximately constant weight. This extraction shall be used for the melting point of the impregnating material. 4.3.2 Shrinkage. The length and width of the specimen shall be measured to the nearest .02 inch (.508 mm) along the ce

32、nter lines of the specimen. The specimen shall be immersed in water at a temperature of 68 to 86 F (20 to 30C) for 24 hours and then heated to boiling at the rate of 17 to 21.5F (5 to 7C) per minute and boiled for 6 minutes. The specimen shall be removed and the length and width again measured immed

33、iately. The shrinkage shall be computed as percentage of the original area. 4.3.3 Porosity. A circular porosity specimen, 3 inch (76.2 mm) in diameter made from each sample marked “A“ shall support a head of 1 ft (304.8 mm) of water for 30 hours without showing porosity. For type II packing, Stoddar

34、d solvent shall be used in place of Water. 4.3.4 Chloroform extract. Approximately 10 grams of type II packing shall be extracted with chloroform using method 6311 of FED-STD-311. 4.3.5 Total polysulfide polymer. Total polysulfide polymer shall be determined as follows. Accurately weigh 0.25 to 0.30

35、 gram of impregnated packing and place in a Parr Bomb cup. Add approximately 0.50 gram of benzoic acid, 0.2 gram of potassium perchlorate and enough sodium peroxide to make the cup two-thirds full. Intimately mix the contents and ignite the bomb. When cool, dissolve the bomb contents in distilled wa

36、ter, filter, neutralize to methyl orange with hydrochloric acid then add a few drops in excess, bring solution to a boil and add 10 ml of 10 percent barium chloride with constant stirring. Let the solution stand for at least 16 hours and then filter. Wash the precipitate free of chlorides, then tran

37、sfer the filter paper and precipitate to a tared crucible. Ignite to constant weight. The weight of barium sulfate is converted to percent sulfur by multiplying by 0.1373, dividing by the same weight and multiplying by 100. Repeat the determination on a representative sample of unimpregnated packing

38、. Complete the percent of total polysulfide polymer content by subtracting the sulfur content of the unimpregnated sample from that of the impregnated and multiplying the difference by 2.74. (This factor is obtained by dividing 1/0.365 where 36.5 percent is representative of the sulfur content of th

39、e polysulfide polymer.) Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-DTL-24293B 6FIGURE 1. Location from which test specimens are to be taken FIGURE 2. Specimen A layout recommended Provided by IHSNot for ResaleNo reproduction or networking pe

40、rmitted without license from IHS-,-,-MIL-DTL-24293B 75. PACKAGING 5.1 Packaging. For acquisition purposes, the packaging requirements shall be as specified in the contract or order (see 6.2). When packaging of materiel is to be performed by DoD or in-house contractor personnel, these personnel need

41、to contact the responsible packaging activity to ascertain packaging requirements. Packaging requirements are maintained by the Inventory Control Points packaging activities within the Military Service or Defense Agency, or within the military services system commands. Packaging data retrieval is av

42、ailable from the managing Military Departments or Defense Agencys automated packaging files, CD-ROM products, or by contacting the responsible packaging activity. 6. NOTES 6.1 Intended use. This material is intended primarily for hydraulic leather packing furnished in the form of belting butt bends,

43、 but may be ordered as finished packing. Type I is intended for use with hydraulic pistons operating at pressures up to 3,000 psi (20.68 MPa) at temperatures up to 155F (68.3C). Type II is intended for use with oil pressures up to 5,000 psi (34.47 MPa) in the temperature range from -65 to +200F (-53

44、.8 to +93.3C). 6.2 Ordering data. Acquisition documents should specify the following: (a) Title, number, and date of this specification. (b) Type and weight required (see 1.2). (c) Packaging requirements (see 5.1). 6.3 Subject term (key word) listing. Belting butt bends Chromium salts Full-grain Sul

45、fate 6.4 Changes from previous issue. Marginal notations are not used in this revision to identify changes with respect to the previous issue due to the extent of the changes. Custodians: Preparing activity: Navy - SH DLA IS (Project 5330-2009-002) NOTE: The activities listed above were interested i

46、n this document as of the date of this document. Since organizations and responsibilities can change, you should verify the currency of the information above using the ASSIST Online database at http:/assist.daps.dla.mil . Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-