ASTM D665-2014 Standard Test Method for Rust-Preventing Characteristics of Inhibited Mineral Oil in the Presence of Water《加抑制剂矿物油在水存在下防锈性能的标准试验方法》.pdf
《ASTM D665-2014 Standard Test Method for Rust-Preventing Characteristics of Inhibited Mineral Oil in the Presence of Water《加抑制剂矿物油在水存在下防锈性能的标准试验方法》.pdf》由会员分享,可在线阅读,更多相关《ASTM D665-2014 Standard Test Method for Rust-Preventing Characteristics of Inhibited Mineral Oil in the Presence of Water《加抑制剂矿物油在水存在下防锈性能的标准试验方法》.pdf(10页珍藏版)》请在麦多课文档分享上搜索。
1、Designation: D665 12D665 14Designation: 135/06Standard Test Method forRust-Preventing Characteristics of Inhibited Mineral Oil inthe Presence of Water1This standard is issued under the fixed designation D665; the number immediately following the designation indicates the year oforiginal adoption or,
2、 in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the U.S. Department of Defense.1. Sco
3、pe*1.1 This test method covers the evaluation of the ability of inhibited mineral oils, particularly steam-turbine oils, to aid inpreventing the rusting of ferrous parts should water become mixed with the oil. This test method is also used for testing other oils,such as hydraulic oils and circulatin
4、g oils. Provision is made in the procedure for testing heavier-than-water fluids.NOTE 1For synthetic fluids, such as phosphate ester types, the plastic holder and beaker cover should be made of a chemically resistant material,such as polytetrafluoroethylene (PTFE).chemically resistant material suita
5、ble for the type of fluid tested.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibilityof the use
6、r of this standard to establish appropriate safety and health practices and determine the applicability of regulatorylimitations prior to use. For specific warning statements, see 6.47.4 6.67.6.2. Referenced Documents2.1 ASTM Standards:2A108 Specification for Steel Bar, Carbon and Alloy, Cold-Finish
7、edA240/A240M Specification for Chromium and Chromium-Nickel Stainless Steel Plate, Sheet, and Strip for Pressure Vessels andfor General ApplicationsD91 Test Method for Precipitation Number of Lubricating OilsD1193 Specification for Reagent WaterD2422 Classification of Industrial Fluid Lubricants by
8、Viscosity SystemD3603 Test Method for Rust-Preventing Characteristics of SteamTurbine Oil in the Presence ofWater (Horizontal Disk Method)D4057 Practice for Manual Sampling of Petroleum and Petroleum ProductsE1 Specification for ASTM Liquid-in-Glass Thermometers2.2 Other Documents:Motor Fuels, Secti
9、on I, Annex A2, Table 32, Reference Materials and Blending Accessories3Specifications-IP Standard Thermometers, Vol 2, Appendix A4Specifications for IP Standard Reference Liquids, Appendix B4SAE Standard J405 Chemical Composition of SAE Wrought Stainless Steels5BS 871 Specification for abrasive pape
10、rs and cloths41 This test method is under the jurisdiction of ASTM Committee D02 on Petroleum Products Products, Liquid Fuels, and Lubricants and is the direct responsibility ofSubcommittee D02.C0.02 on Corrosion and Water/Air Separability.Current edition approved Nov. 1, 2012Oct. 1, 2014. Published
11、 March 2013November 2014. Originally approved in 1942. Last previous edition approved in 20062012 asD665D665 12.-06. DOI: 10.1520/D0665-12.10.1520/D0665-14.This standard has been developed through the cooperative effort between ASTM International and the Energy Institute, London. The EI and ASTM Int
12、ernational logosimply that the ASTM International and EI standards are technically equivalent, but does not imply that both standards are editorially identical.2 For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at serviceastm.org. For Annual Book of
13、ASTM Standardsvolume information, refer to the standards Document Summary page on the ASTM website.3 See 1996 Annual Book of ASTM Standards, Vol 05.04.4 Annual Book of IP Standard Methods for Analysis and Testing of Petroleum and Related Products, Vol 2.Available from Energy Institute, 61 New Cavend
14、ish St., London,WIG 7AR, U.K.5 1995 SAE Handbook, Vol 1. Available from Society of Automotive Engineers (SAE), 400 Commonwealth Dr., Warrendale, PA 15096-0001.This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been ma
15、de to the previous version. Becauseit may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current versionof the standard as published by ASTM is to be considered the official document.*A
16、Summary of Changes section appears at the end of this standardCopyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States1BS 970 Part 1: Carbon and Carbon Manganese Steels Including Free Cutting Steels43. Terminology3.1 Definitions of Terms Speci
17、fic to This Standard:3.1.1 rust, na special case of corrosion that can be visually observed on the surface of round steel test rods as reddish-browndiscoloration or small black spots.4. Summary of Test Method4.1 A mixture of 300 mL of the oil under test is stirred with 30 mL of distilled water or sy
18、nthetic sea water, as required, at atemperature of 60 C 6 1C1 C with a cylindrical steel test rod completely immersed therein. It is recommended to run the testfor 4 h; however, the test period may, at the discretion of the contracting parties, be for a shorter or longer period. The test rodis obser
19、ved for signs of rusting and, if desired, degree of rusting.NOTE 2Until 1999 it was customary to run the test for 24 h. A round robin with comparisons of different test times showed that no statisticallysignificant differences in rating were found for any sample, between the 44 h and 24 h results.65
20、. Significance and Use5.1 In many instances, such as in the gears of a steam turbine, water can become mixed with the lubricant, and rusting of ferrousparts can occur. This test indicates how well inhibited mineral oils aid in preventing this type of rusting. This test method is alsoused for testing
21、 hydraulic and circulating oils, including heavier-than-water fluids. It is used for specification of new oils andmonitoring of in-service oils.NOTE 3This test method was used as a basis for Test Method D3603. Test Method D3603 is used to test the oil on separate horizontal and verticaltest rod surf
22、aces, and can provide a more discriminating evaluation.6. Apparatus6.1 Oil BathA thermostatically controlled liquid bath capable of maintaining the test sample at a temperature of 6060 C 61C1 C (see Note 4). An oil having a viscosity of approximately ISO VG 32 (see Classification D2422) is suitable
23、for the bath.The bath shall have a cover with holes to accommodate the test beakers.NOTE 4ASTM Thermometer 9C, as prescribed in Specification E1, or IP Thermometer 21C in accordance with IP Standard Thermometers, Volume2, Appendix A, is suitable to indicate the temperature. Alternatively, calibrated
24、 thermocouples may be used.6.2 BeakerA 400-mL, Berzelius-type, tall-form heat-resistant glass beaker without pourout,pour-out, as shown in Fig. 1,approximately 127 mm in height measured from the inside bottom center and approximately 70 mm) in mm inside diametermeasured at the middle.6.3 Beaker Cove
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