GOST 32533-2013 Hexamethylene diamine Determination in air《己二胺 空气中的测定》.pdf

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1、 , () INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ISC) 32533 2013 2014 325332013 II , - 1.0 92 . - 1.2 2009 . - , . , , , 1 - ( - ) - , , - ( ) 2 3 , 14 2013 . 44-2013, 24) : ( 3166) 004 97 3166) 004 97 - AM KG RU TJ UZ 4 22 - 2013 . 820- 325332013 - 1 2014 . 5 - , . ( ) - -

2、 . , , 2014 - , - 325332013 1 Hexamethylene diamine. Determination in air 20140801 1 - ( ) 0,02 3 - ( ) . 2 : 12.1.00588 . 12.1.0192009 . . 177074 . , , , - . 311778 . . 311877 . . 416676 . . 432877 . . 670972 . 2533682 . , - 2922791 ( 835-181) . . 1. - , 1 , - . ( ), - ( ) . , , , , . 3 ( 2 = k ) %

3、 15 = U . 15 % 95 , 0 = P . 325332013 2 4 4.1 , , . 4.2 - ( ) ( - ). - . 4.3 -d 4 . - , - . 4.4 , ) -d 4 , . - . 4.5 . 4.6 , - . 5 , 5.1 , Pharmacia LKB HPLC Pump 2248 (Pharmacia, Uppsala, Sweden), c /200 (Carnegie, Stockholm, Sweden), VICI C6W (Valco Instruments, Houston, TX, USA): 20 , 5 ( ). Mill

4、ipore Waters (Milford, MA, USA) Nova Pak C 18 , 150 3,9 , 5 . VG-Quattro (Waters, VG-Biotech, Altrincham, Chesh- ire, UK) (thermospray). 53228. 50 100 . 5 29227 0,03 . 2-10 2-500 1770 0,1 5,0 . 25 250 1770 0,04 0,15 - , . . 5.2 , ., 2. -d 4(H 2 NCD 2 (CH 2 ) 4 CD 2 NH 2 ) (MSD isotopes, Merck Frost Canada, Montreal, Canada). ( 99,0%, Aldrich),