EN ISO 1518-2-2011 en Paints and varnishes - Determination of scratch resistance - Part 2 Variable-loading method《涂料和清漆 抗划性的测定 可变载荷方法》.pdf

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1、raising standards worldwideNO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAWBSI Standards PublicationBS EN ISO 1518-2:2011Paints and varnishes Determination of scratch r e s i s t a n c ePart 2: Variable-loading method (ISO 1518-2:2011)Incorporating corrigendum November 2011BS E

2、N ISO 1518-2:2011 BRITISH STANDARDNational forewordThis British Standard is the UK implementation of EN ISO 1518-2:2011. It supersedes BS EN ISO 12137-2:2006, which is withdrawn.The UK participation in its preparation was entrusted to T e c h n i c a l C o m m i t t e e S T I / 1 0 , T e s t m e t h

3、 o d s f o r p a i n t s .A list of organizations represented on this committee can be obtained on request to its secretary.This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application.ISBN 978 0 580 77326 6ICS 87.040 Comp

4、liance with a British Standard cannot confer immunity from legal obligations.This British Standard was published under the authority of the Standards Policy and Strategy Committee on 30 November 2011.Amendments/corrigenda issued since publicationDate T e x t a f f e c t e d31 Janury 2012 Implementat

5、ion of CEN Correction Notice 9 November 2011: Correction of the supersedingnote in the EN Foreword and title page The British Standards Institution 2012EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 1518-2 October 2011 ICS 87.040 Supersedes EN ISO 12137-2:2006English Version Paints and var

6、nishes - Determination of scratch resistance - Part 2: Variable-loading method (ISO 1518-2:2011) Peintures et vernis - Dtermination de la rsistance la rayure - Partie 2: Mthode charge variable (ISO 1518-2:2011) Beschichtungsstoffe - Bestimmung der Kratzbestndigkeit -Teil 2: Verfahren mit kontinuierl

7、ich ansteigender Last (ISO 1518-2:2011) This European Standard was approved by CEN on 14 October 2011. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.

8、Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by tra

9、nslation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finl

10、and, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES K

11、OMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2011 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 1518-2:2011: EForeword This document (EN ISO 1518-2:2011) has been prepared by Technical Committee ISO/

12、TC 35 “Paints and varnishes“ in collaboration with Technical Committee CEN/TC 139 “Paints and varnishes” the secretariat of which is held by DIN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by Ap

13、ril 2012, and conflicting national standards shall be withdrawn at the latest by April 2012. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent r

14、ights. This document supersedes EN ISO 12137-2:2006. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finlan

15、d, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 1518-2:2011 has been approved by CEN as a EN I

16、SO 1518-2:2011 without any modification. BS EN ISO 1518-2:2011 EN ISO 1518-2:2011 (E)iiiForeword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out

17、through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO coll

18、aborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International St

19、andards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements

20、of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 1518-2 was prepared by Technical Committee ISO/TC 35, Paints and varnishes, Subcommittee SC 9, General test methods for paints and varnishes. It cancels and repl

21、aces ISO 12137-2:1997, which has been technically revised. The main changes are the following: a) The number of the standard has been changed from ISO 12137-2 to ISO 1518-2 in order to group the scratch-resistance tests under the same number (ISO 1518). b) A definition of scratch has been introduced

22、. c) The supplementary test conditions (formerly Annex A) have been integrated in the test report. d) The text has been editorially revised and the normative references have been updated. ISO 1518 consists of the following parts, under the general title Paints and varnishes Determination of scratch

23、resistance: Part 1: Constant-loading method Part 2: Variable-loading method BS EN ISO 1518-2:2011 EN ISO 1518-2:2011 (E) ISO 2011 BS EN ISO 1518-2:2011 EN ISO 1518-2:2011 (E)INTERNATIONAL STANDARD 1Paints and varnishes Determination of scratch resistance Part 2: Variable-loading method 1 Scope This

24、part of ISO 1518 specifies a method for determining, using a pointed stylus loaded with a continuously increasing load, the scratch resistance of a single coating of a paint, varnish or related product, or the upper layer of a multicoat system. This test has been found to be useful in comparing the

25、scratch resistance of different coatings. It is most useful in providing relative ratings for a series of coated panels exhibiting significant differences in scratch resistance. Neither this part of ISO 1518 nor ISO 1518-1 specifies a method using a curved stylus, which is specified in ISO 12137. Th

26、e choice between the three methods will depend on the particular practical problem. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of th

27、e referenced document (including any amendments) applies. ISO 1513, Paints and varnishes Examination and preparation of test samples ISO 1514, Paints and varnishes Standard panels for testing ISO 2808, Paints and varnishes Determination of film thickness ISO 15528, Paints, varnishes and raw material

28、s for paints and varnishes Sampling 3 Terms and definitions For the purposes of this document, the following terms and definitions apply. 3.1 scratch, n cut or gouge through the surface of a coating, made by contact with a sharp object 4 Principle The product or system under test is applied at unifo

29、rm thickness to flat panels of uniform surface texture. After drying/curing, the scratch resistance is determined using an automatic instrument which pushes the panels beneath a pointed stylus mounted so that it presses down perpendicularly on the surface of the test panel. The load on the test pane

30、l is increased continuously until the coating is scratched. EN ISO 1518-2:2011 (E)BS EN ISO 1518-2:2011 ISO 2011 2 5 Apparatus 5.1 Instrument for determining scratch resistance. A suitable instrument1)is shown in Figure 1. It consists principally of a counterbalanced beam with, mounted at one end, a

31、 pointed stylus. The test panel is placed on a sliding table which is motor-driven to move under the stylus at a speed of 10 mm/s. A continuous-loading weight mounted over the beam acts on the beam in such a way that, as the test panel passes under the stylus, the load on the stylus is continuously

32、increased. The stylus-loading range can be varied by changing the continuous-loading weight (weights giving loading ranges of 0 g to 50 g, 0 g to 100 g and 0 g to 200 g are available, for instance). Mounted over the stylus itself is a small scale pan on which weights can be placed to expand the styl

33、us-loading range (adding a weight of 100 g, for instance, changes a 0 g to 200 g loading range to one of 100 g to 300 g). 1) This apparatus is available from Shinto Scientific Co., Ltd, 27 Kanda-higashikonyacho, Chiyoda-ku, Tokyo 101-0034, Japan. This information is given for the convenience of user

34、s of this part of ISO 1518 and does not constitute endorsement by ISO of the apparatus shown. Other types of scratch tester may be used if they can be shown to give similar relative ratings. BS EN ISO 1518-2:2011 EN ISO 1518-2:2011 (E) ISO 2011 3Key 1 cylindrical counterweight 2 continuous-loading w

35、eight 3 scale pan 4 sliding table 5 stylus Figure 1 Scratch instrument with pointed stylus 5.2 Stylus, preferably tipped with a conical sapphire or diamond, the point of which is rounded to a radius of (0,03 0,005) mm (see Figure 2). BS EN ISO 1518-2:2011 EN ISO 1518-2:2011 (E) ISO 2011 4 Dimensions

36、 in millimetres Key 1 conical sapphire or diamond 2 stylus Figure 2 Stylus tipped with conical sapphire or diamond 5.3 Microscope, preferably with a magnification range extending up to 100, required to examine the stylus. It may also be used to inspect the scratched coating. 6 Sampling Take a repres

37、entative sample of the product to be tested (or of each product in the case of a multicoat system), as specified in ISO 15528. Examine and prepare each sample for testing, as specified in ISO 1513. 7 Test panels 7.1 Substrate Select the substrate from one of those specified in ISO 1514 and, where po

38、ssible, in accordance with the desired practical application. The panels shall be plane and free from distortion, with a maximum thickness of about 12 mm, and 100 mm to 400 mm wide and long. 7.2 Preparation and coating Prepare each test panel in accordance with ISO 1514 and then coat it by the speci

39、fied method with the product or system under test. BS EN ISO 1518-2:2011 EN ISO 1518-2:2011 (E) ISO 2011 57.3 Drying and conditioning Dry (or stove) and age, if applicable, each coated test panel according to the instructions given for the product or system under test. Before testing, condition the

40、coated panels at (23 2) C and a relative humidity of (50 5) % for a minimum period of 16 h. The coated panels shall be stored and handled so as to avoid contamination by fingerprints and dust. NOTE Fingerprints, dust or other contamination on the surface will result in a lower accuracy. 7.4 Thicknes

41、s of coating Determine the thickness, in micrometres, of the dried coating by one of the procedures specified in ISO 2808. 8 Procedure 8.1 Test conditions Carry out the test at (23 2) C and a relative humidity of (50 5) %. 8.2 Preparation for the test Place the instrument on a stable and level surfa

42、ce. Level the instrument in accordance with the manufacturers instructions. Examine the stylus under the microscope, preferably at a magnification of 100, in accordance with the instrument operation manual, to ensure that it is undamaged. Clean the stylus, if necessary, with a clean cloth or lint-fr

43、ee paper. 8.3 Determination Place a test panel up against the stop on the sliding table. Secure the panel in place by turning the securing screws evenly about one turn at a time. Secure the stylus in the vertical position. Adjust the counterweights so that, when the tip of the stylus is just touchin

44、g the surface of the test panel, the load on the stylus is zero. Adjust the height of the stylus to the thickness of the test panel, with the beam released and the stylus resting on the test panel. Load the stylus at the lowest weight range to be tested, e.g. 0 g to 50 g. Start the instrument at a r

45、ate of about 10 mm/s. The instrument shown in Figure 1 will stop automatically when the sliding table has moved 100 mm. Inspect the coating for scratching under a suitable magnification or with the naked eye. BS EN ISO 1518-2:2011 EN ISO 1518-2:2011 (E) ISO 2011 6 If no scratching occurs, increase t

46、he stylus-loading range, e.g. 0 g to 100 g, and continue in test areas that do not overlap until scratching does occur. When scratching has occurred, determine which type of defect is involved. The defects are defined as follows: a) Plastic deformation: the permanent indentation of the surface with

47、or without any surface blemish or cohesive fracture. b) Surface blemish: a superficial surface effect caused by a difference in the scattering of light between the line of test and the adjacent surface. c) Surface scratch: a continuous cut or gouge through the surface. d) Cohesive fracture: the pres

48、ence of a visible surface break or rupture. e) Combinations of the above. NOTE In some cases, one of these types of defect might be of particular importance. Repeat the determination at least twice (i.e. for a total of at least three determinations) on the same panel at the stylus-loading range at which scratching occurs. For each of the determinations,