SANS 1265-2009 Waxy oil obtained from the synthol process and from other petroleum sources《合成工艺和其它石油资源中得到的蜡油》.pdf

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1、 Collection of SANS standards in electronic format (PDF) 1. Copyright This standard is available to staff members of companies that have subscribed to the complete collection of SANS standards in accordance with a formal copyright agreement. This document may reside on a CENTRAL FILE SERVER or INTRA

2、NET SYSTEM only. Unless specific permission has been granted, this document MAY NOT be sent or given to staff members from other companies or organizations. Doing so would constitute a VIOLATION of SABS copyright rules. 2. Indemnity The South African Bureau of Standards accepts no liability for any

3、damage whatsoever than may result from the use of this material or the information contain therein, irrespective of the cause and quantum thereof. ISBN 978-0-626-23119-4 SANS 1265:2009Edition 1.3Any reference to SABS 1265 is deemedto be a reference to this standard(Government Notice No. 1373 of 8 No

4、vember 2002)SOUTH AFRICAN NATIONAL STANDARD Waxy oil obtained from the synthol process and from other petroleum sources Amdt 2 Published by SABS Standards Division 1 Dr Lategan Road Groenkloof Private Bag X191 Pretoria 0001Tel: +27 12 428 7911 Fax: +27 12 344 1568 www.sabs.co.za SABS SANS 1265:2009

5、Edition 1.3 Table of changes Change No. Date Scope Amdt 1 1989 Amended to change the method of sampling. Amdt 2 1991 Amended to change the title and to allow for a type of oil obtained from other petroleum sources. Amdt 3 2009 Amended to change the designation of SABS standards to SANS standards, an

6、d to update referenced standards. Acknowledgement The SABS Standards Division wishes to acknowledge the valuable assistance derived from publications of the following organizations: American Society for Testing and Materials (ASTM) Institute of Petroleum (IP) (UK) Foreword This South African standar

7、d was approved by National Committee SABS SC 218C, Timber preservation Timber preservatives, in accordance with procedures of the SABS Standards Division, in compliance with annex 3 of the WTO/TBT agreement. This document was published in July 2009. This document supersedes SABS 1265:1979 (edition 1

8、). A vertical line in the margin shows where the text has been technically modified by amendment Nos 1, 2 and 3. SANS 1265:2009 Edition 1.3 1 Contents Page Foreword 1 Scope 3 2 Definitions . 3 3 Requirements 3 4 Packing and marking . 4 5 Sampling and compliance with the specification 4 6 Methods of

9、test . 5 6.1 Flash Point, viscosity, pour point, distillation, congealing point of wax, and water and sediment content. 5 6.2 Wax content . 5 Appendix A Applicable standards 7 SANS 1265:2009 Edition 1.3 2 This page is intentionally left blank SANS 1265:2009 Edition 1.3 3 Waxy oil obtained from the s

10、ynthol process and from other petroleum sources Amdt 2 1 Scope 1.1 This specification covers two types of waxy oil, for use in the blending of creosote/oil wood preservative mixtures. Amdt 2 NOTE The test methods referred to in the specification are listed in appendix A. 2 Definitions 2.1 For the pu

11、rposes of this specification the following definitions shall apply: ASTM method test method published by the American Society for Testing and Materials, 1916 Race Street, Philadelphia, Pa. 19103, USA defective container or a test sample of waxy oil that fails, in one or more respects, to comply with

12、 the relevant requirements of the specification IP method test method published by the Institute of Petroleum, 61 New Cavendish Street, London, W1M 8AR, England lot that quantity of waxy oil bearing the same batch identification, from one manufacturer, submitted at any one time for inspection and te

13、sting 3 Requirements 3.1 Type The waxy oil shall be of type I or type II, as follows: a) type I is obtained from the synthol process; and b) type II is obtained from other petroleum sources. Amdt 2 SANS 1265:2009 Edition 1.3 4 3.2 Physical requirements The waxy oil shall comply with the requirements

14、 given in table 1. Amdt 2 Table 1 Physical requirements 1 2 3 Requirement Property Type I Type II Test method Flash point, C, min. . 120 120 ASTM D 92a-IP 36 Viscosity at 100 C, mm2/sa.2, 5 - 5, 0 2, 5 - 7, 5 ASTM D 445-IP 71 Pour point, C, max. . 27 40 ASTM D 97-IP 15 Distillation Distillate up to

15、355 C (corrected to a barometric pressure of 101,33 kPa), % by mass, max. 50 50 ASTM D 1160 Wax content, % by mass, min. . 10 60 See 6.2 Congealing point of wax, C, min. 55 40 ASTM D 938-IP 76 Water and sediment content, % by volume, max 1,0 0,5 ASTM D 1796 a 1 mm2/s=1cSt. Amdt 2; amdt 34 Packing an

16、d marking 4.1 Packing The condition of each drum and tanker into which the waxy oil is filled shall be such as to have no detrimental effect on the quality of the product during normal transportation and storage. 4.2 Marking The following information shall appear in legible and indelible marking on

17、each drum or, when the waxy oil is supplied in tankers, in the relevant consignment documents: a) the manufacturers identification; b) the type of waxy oil. Amdt 2 5 Sampling and compliance with the specification NOTE This section applies to the sampling for inspection and testing before acceptance

18、or rejection of single lots (consignments) in cases where no information about the implementation of quality control or testing during manufacture is available to help in assessing the quality of the lot. It is also used as the procedure for adjudicating in cases of dispute. 5.1 Sampling The relevan

19、t sampling procedure described in ASTM D 4057 or ASTM D 4177, shall be applied (after inspection of the lot for compliance with 4.1 and 4.2) in determining whether a lot complies with the appropriate requirements of the specification. The sample so drawn shall be deemed to represent the waxy oil in

20、the lot. Amdt 1 SANS 1265:2009 Edition 1.3 5 5.2 Compliance with the specification The lot shall be deemed to comply with the requirements of the specification if, after inspection of the lot and testing of the sample taken in accordance with 5.1, no defective is found. 6 Methods of test 6.1 Flash p

21、oint, viscosity, pour point, distillation, congealing point of wax, and water and sediment content Use the applicable methods listed in column 3 of table 1. NOTE The congealing point of wax is determined on the wax residue obtained by the method given in 6.2. 6.2 Wax content 6.2.1 Apparatus a) Buchn

22、er filtering flask. A Buchner flask of suitable capacity and to which the filter may be fitted. b) Filter. A sintered-glass filter of diameter approximately 40 mm, and of porosity No. 2. c) Rotary evaporator, fitted with a round-bottom flask of capacity 250 mL. 6.2.2 Solvents a) Benzene. AR grade be

23、nzene. b) Methyl ethyl ketone. AR grade methyl ethyl ketone. 6.2.3 Procedure a) Using a thoroughly mixed sample, weigh out, to the nearest 0,01 g, 10 g 0,5 g of a type I waxy oil or 5 g 0,5 g of a type II waxy oil, as relevant. Place the weighed specimen in a clean dry glass beaker, add 150 mL of th

24、e methyl ethyl ketone and heat the mixture to boiling point on a hot plate. b) Remove the beaker from the hot plate, allow it to cool in an ice-and-water mixture for at least 30 min, and then, with the aid of a freezing-mixture (or by other suitable means), cool the beaker and its contents to 0 C 2

25、C. NOTE Ensure that the mixture is not cooled to below -2 C and that its temperature is maintained at 0 C 2 C throughout the filtering procedure described in (c) below. c) Cool the filter by filling it, 1 min to 2 min before filtration, with the methyl ethyl ketone that has been pre-cooled to 0 C. F

26、it the filter to the Buchner flask, remove the methyl ethyl ketone from the filter by applying suction to the flask, and immediately afterwards, under conditions of slightly reduced pressure, pass the contents of the beaker through the filter. NOTE The filtration period should normally not exceed 2

27、min. d) Using a suitable volume of the benzene (pre-heated to a suitable temperature) to dissolve the waxy residue, wash the residue on the filter, quantitatively, through the filter into the tared flask of the rotary evaporator (6.2.1(c). SANS 1265:2009 Edition 1.3 6 e) Connect the flask to the rot

28、ary evaporator, and evaporate the solvent under reduced pressure and on a heated water bath. Dry the residue to constant mass at 100 C 5 C. f) From the mass of the residue (determined to the nearest 0,01 g) and the mass of the test sample, calculate the wax content of the sample to the nearest 0,1 %

29、. NOTE Retain the wax residue for the test to determine the congealing point. SANS 1265:2009 Edition 1.3 7 Appendix A Applicable standards Reference is made to the latest issues of the following test methods: ASTM D 92a, Standard test method for flash and fire points by Cleveland open cup tester. Am

30、dt 3 ASTM D 97, Standard test method for pour point of petroleum products. ASTM D 270, Methods of sampling petroleum and petroleum products. Amdt 1 ASTM D 445, Standard test method for kinematic viscosity of transparent and opaque liquids (and calculation of dynamic viscosity). ASTM D 938, Standard

31、test method for congealing point of petroleum, waxes, including petrolatum. ASTM D 1160, Standard test method for distillation of petroleum products at reduced pressure. ASTM D 1796, Standard test method for water and sediment in fuel oils by the centrifuge method (laboratory procedure). ASTM D 4057

32、, Standard practice for manual sampling of petroleum and petroleum products. Amdt 1 ASTM D 4177, Standard practice for automatic sampling of petroleum and petroleum products.Amdt 1 IP 15, Petroleum products Determination of pour point. IP 36, Determination of open flash and fire points Cleveland. IP

33、 71-1, Petroleum products Part 1:Transparent and opaque liquids Determination of kinematic viscosity and calculation of dynamic viscosity. IP 71-2, Petroleum products Part 2:Glass capillary kinematic viscometers Specifications and operating instructions. IP 75, Water and sediment in fuel oils by cen

34、trifuge. Amdt 3 IP 76, Determination of congealing points of waxes and petrolatum. SABS This page has been left blank intentionally SABS Standards Division The objective of the SABS Standards Division is to develop, promote and maintain South African National Standards. This objective is incorporate

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