DIN EN ISO 12625-3-2014 Tissue paper and tissue products - Part 3 Determination of thickness bulking thickness apparent bulk density and bulk (ISO 12625-3 2014) German version EN I.pdf

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1、September 2014 Translation by DIN-Sprachendienst.English price group 11No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).

2、ICS 85.080.20!%:Y“2235854www.din.deDDIN EN ISO 12625-3Tissue paper and tissue products Part 3: Determination of thickness, bulking thickness, apparent bulkdensity and bulk (ISO 12625-3:2014);English version EN ISO 12625-3:2014,English translation of DIN EN ISO 12625-3:2014-09Tissue-Papier und Tissue

3、-Produkte Teil 3: Bestimmung der Dicke, der Blattdicke im Stapel, der scheinbaren Stapeldichte unddes spezifischen Volumens (ISO 12625-3:2014);Englische Fassung EN ISO 12625-3:2014,Englische bersetzung von DIN EN ISO 12625-3:2014-09Papier tissue et produits tissues Partie 3: Dtermination de lpaisseu

4、r, de lpaisseur moyenne dune feuille en liasse etde la masse volumique moyenne et de la main (ISO 12625-3:2014);Version anglaise EN ISO 12625-3:2014,Traduction anglaise de DIN EN ISO 12625-3:2014-09SupersedesDIN EN ISO 12625-3:2014-07www.beuth.deDocument comprises 19 pagesIn case of doubt, the Germa

5、n-language original shall be considered authoritative.08.14 DIN EN ISO 12625-3:2014-09 2 A comma is used as the decimal marker. National foreword This document (EN ISO 12625-3:2014) has been prepared by Technical Committee CEN/TC 172 “Pulp, paper and board”, Working Committee WG 8 “Test methods for

6、soft tissue papers“ (Secretariat: DIN, Germany) in collaboration with Technical Committee ISO/TC 6 “Paper, board and pulps”. The responsible German body involved in its preparation was the Normenausschuss Papier, Pappe und Faserstoff (Paper, Board and Pulps Standards Committee), Working Committee NA

7、 074-02-05 AA Prfverfahren fr Tissue-Papier und Tissue-Produkte. The DIN Standards corresponding to the International Standards referred to in this document are as follows: ISO 186 DIN EN ISO 186 ISO 187 DIN EN 20187 ISO 287 DIN EN ISO 287 ISO 534 DIN EN ISO 534 ISO 638 DIN EN ISO 638 ISO 5725-1 DIN

8、 ISO 5725-1 ISO 12625-1 DIN EN ISO 12625-1 ISO 12625-6 DIN EN ISO 12625-6 ISO 15755 DIN EN ISO 15755 Amendments This standard differs from DIN EN ISO 12625-3:2005-09 as follows: a) the title has been changed to include “bulk”; b) accuracy data in Annex A have been adjusted to the existing equipment

9、capabilities and calibration procedures; c) the preparation of test pieces has been described more precisely; Subclauses 7.1 and 7.4 have been reformulated; d) the standard has been editorially revised. Compared with DIN EN ISO 12625-3:2014-07, the following corrections have been made to the German

10、version only and therefore do not affect the English text: a) in Subclause 5.2, the last sentence has been supplemented to include “bei einer Temperatur von 23 C” (at 23 C); b) in Annex A, Table A.4, second row, 6th column, the value has been corrected to read “0,006 69” instead of “0,006 9”. Previo

11、us editions DIN 54540-3: 1989-06 DIN EN 12625-3: 1999-03 DIN EN ISO 12625-3: 2005-09, 2014-07 DIN EN ISO 12625-3:2014-09 3 National Annex NA (informative) Bibliography DIN EN 20187, Paper, board and pulps Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere an

12、d conditioning of samples DIN EN ISO 186, Paper and board Sampling to determine average quality DIN EN ISO 287, Paper and board Determination of moisture content of a lot Oven-drying method DIN EN ISO 534, Paper and board Determination of thickness, density and specific volume DIN EN ISO 638, Paper,

13、 board and pulps Determination of dry matter content Oven-drying method DIN ISO 5725-1, Accuracy (trueness and precision) of measurement methods and results Part 1: General principles and definitions DIN EN ISO 12625-1, Tissue paper and tissue products Part 1: General guidance on terms DIN EN ISO 12

14、625-6, Tissue paper and tissue products Part 6: Determination of grammage DIN EN ISO 15755, Paper and board Estimation of contraries DIN EN ISO 12625-3:2014-09 4 This page is intentionally blank. EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 12625-3 April 2014 ICS 85.060 Supersedes EN ISO

15、 12625-3:2005 English Version Tissue paper and tissue products Part 3: Determination of thickness, bulking thickness and apparent bulk density and bulk (ISO 12625-3:2014) Papier tissue et produits tissue Partie 3: Dtermination de lpaisseur, de lpaisseur moyenne dune feuille en liasse et de la masse

16、volumique moyenne et de la main (ISO 12625-3:2014) Tissue-Papier und Tissue-Produkte Teil 3: Bestimmung der Dicke, der Blattdicke im Stapel, der scheinbaren Stapeldichte und des spezifischen Volumens (ISO 12625-3:2014) This European Standard was approved by CEN on 15 February 2014. CEN members are b

17、ound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the

18、 CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centr

19、e has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania

20、, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000

21、 Brussels 2014 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 12625-3:2014 E ContentsPageForeword .3Introduction .41 Scope . 52 Normative references 53 Terms and definitions . 54 Principle 65 Apparatus . 65.1 Precision dead-we

22、ight micrometer . 65.2 Gauge blocks . 75.3 Balance and attachments . 76 Conditioning 77 Preparation of test pieces . 77.1 General . 77.2 Single-ply thickness 77.3 Single-ply sheet thickness . 77.4 Bulking thickness 78 Procedure. 89 Calculation 89.1 Single-ply thickness 89.2 Single sheet thickness .

23、89.3 Bulking thickness 89.4 Apparent bulk density 89.5 Bulk (apparent specific bulk volume) . 910 Test report . 9Annex A (informative) Precision 10Annex B (normative) Measurement conditions . 12Annex C (informative) Foot pressure 14Bibliography .15DIN EN ISO 12625-3:2014-09 EN ISO 12625-3:2014 (E) 2

24、Foreword This document (EN ISO 12625-3:2014) has been prepared by Technical Committee ISO/TC 6 “Paper, board and pulps“ in collaboration Technical Committee EN ISO 12625-3:2014 by Technical Committee CEN/TC 172 “Pulp, paper and board” the secretariat of which is held by DIN. This European Standard s

25、hall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by October 2014, and conflicting national standards shall be withdrawn at the latest by October 2014. Attention is drawn to the possibility that some of the elements of this d

26、ocument may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN ISO 12625-3:2005. According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countrie

27、s are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland

28、, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. Endorsement notice The text of ISO 12625-3:2014 has been approved by CEN as EN ISO 12625-3:2014 without any modification. With regard to ISO 12625-3:2005, the following minor changes have been made:a)

29、 title changed; “bulk” added;b) the accuracy data in Annex A were adjusted to the existing equipment capabilities and calibration procedures;,c) preparation of test pieces more precisely described, 7.1 and 7.4 reformulated;d) editorial updating.ISO 12625 consists of the following parts, under the ge

30、neral title Tissue paper and tissue products Part 1: General guidance on terms; Part 3: Determination of thickness, bulking thickness, apparent bulk density and bulk Part 4: Determination of tensile strength, stretch at break and tensile energy absorption; Part 5: Determination of wet tensile streng

31、th; Part 6: Determination of grammage; Part 7: Determination of optical properties Measurement of brightness and colour with D65/10 (outdoor daylight); Part 8: Water-absorption time and water-absorption capacity; basket-immersion test method; Part 9: Determination of ball burst strength; Part 11: De

32、termination of wet ball burst strength; Part 12:Determination of tensile strength of perforated lines Calculation of perforation efficiency; Part 15 Determination of optical properties Measurement of brightness and colour with C/2 (indoor daylight) illuminant; Part 16 Determination of optical proper

33、ties Opacity (paper backing) Diffuse reflectance methodDIN EN ISO 12625-3:2014-09 EN ISO 12625-3:2014 (E) 3IntroductionThickness is an important property of tissue paper and tissue products.In the tissue industry, thickness-related parameters, such as the roll diameter of rolled products (kitchen to

34、wel) or the stack height of folded products (paper towels) are often measured. However, the fact that not only end-use tissue products, but also the base tissue paper from which these products are made, is the subject of trade between companies and countries, means that there is a genuine need for a

35、 consistent measure of thickness that can be applied to tissue products at any stage of their manufacture.The thickness of tissue paper and tissue products is known to be dependent on the pressure applied to the material at the time of measurement. Several different loading pressures, pressure-foot

36、diameters and loading speeds have been used within the tissue industry. This part of ISO 12625 has been prepared by harmonizing those standards applicable to tissue and tissue products currently in use. It specifies a single loading pressure, foot diameter and loading speed to be used for all thickn

37、ess measurements of tissue and tissue products.It is expressly stated that the detection of impurities and contraries in tissue paper and tissue products should be applied according to ISO 15755.For the determination of moisture content in tissue paper and tissue products, ISO 287 or ISO 638 should

38、be applied.DIN EN ISO 12625-3:2014-09 EN ISO 12625-3:2014 (E) 41 ScopeThis part of ISO 12625 specifies a test method for the determination of thickness and bulking thickness and the calculation of apparent bulk density and bulk of tissue papers and tissue products under a pressure of 2,0 kPa.NOTE Th

39、is part of ISO 12625 has been developed to provide a consistent test method for the determination of thickness and density of tissue paper and tissue products. Corresponding test methods for paper and board in general are covered in ISO 534.2 Normative referencesThe following documents, in whole or

40、in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.ISO 186, Paper and board Sampling to determin

41、e average qualityISO 187, Paper, board and pulps Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samplesISO 12625-1, Tissue paper and tissue products Part 1: General guidance on termsISO 12625-6, Tissue paper and tissue products Part 6

42、: Determination of grammage3 Terms and definitionsFor the purposes of this document, the terms and definitions given in ISO 12625-1 and the following apply.3.1single-ply thicknessdistance between the two principal surfaces of a single ply of tissue paper measured under the applied static load specif

43、ied in this part of ISO 12625Note 1 to entry: A ply of tissue is an unlaminated tissue, like that made directly from a tissue machine.3.2single sheet thicknessdistance between the two principal surfaces of a single sheet of tissue product measured under the applied static load specified in this part

44、 of ISO 12625Note 1 to entry: A sheet of tissue is a laminated or unlaminated tissue like that present in the finished tissue product.DIN EN ISO 12625-3:2014-09 EN ISO 12625-3:2014 (E) 53.3bulking thicknessthickness of a single sheet of tissue paper or tissue product, calculated from the thickness o

45、f several superimposed sheets, measured under the applied static load specified in this part of ISO 126253.4apparent bulk densitymass per unit volume of tissue paper or tissue product, calculated from its grammage and bulking thicknessNote 1 to entry: The apparent bulk density is expressed in grams

46、per cubic centimetre.3.5bulk apparent specific bulk volumeinverse of densityNote 1 to entry: The bulk is expressed in cubic centimetres per gram.3.6grammagemass of a unit area of tissue paper or tissue product as determined by the procedure in ISO 12625-6Note 1 to entry: to entry The grammage is exp

47、ressed in grams per square metre (g/m2).4 PrincipleMeasurement of the thickness of a test piece of tissue paper sampled during the manufacturing process or of a tissue product supplied as a finished article. The measurement being made as the distance between a fixed reference plate on which the samp

48、le rests and a parallel pressure-foot that exerts a specified load on the area under test.5 Apparatus5.1 Precision dead-weight micrometerThis has two parallel, horizontal faces, flat to within 0,003 mm, between which the test piece is placed. The lower face shall be fixed and the upper face (pressure-foot) moveable in a direction perpendicular to the plane of the fixed face.The upper, circular, pressure-foot shall have a diameter of (35,7 0,1) mm giving a nominal area of 1