DIN EN 1464-2010 Adhesives - Determination of peel resistance of adhesive bonds - Floating roller method German version EN 1464 2010《粘合剂 粘结的抗剥离性测定 浮辊法 德文版本EN 1464-2010》.pdf

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1、June 2010 Translation by DIN-Sprachendienst.English price group 8No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 83

2、.180!$iL“1700441www.din.deDDIN EN 1464Adhesives Determination of peel resistance of adhesive bonds Floating roller methodEnglish translation of DIN EN 1464:2010-06Klebstoffe Bestimmung des Schlwiderstandes von Klebungen RollenschlversuchEnglische bersetzung von DIN EN 1464:2010-06Adhsifs Dterminatio

3、n de la rsistance au pelage des assemblages Mthode des galets mobilesTraduction anglaise de DIN EN 1464:2010-06SupersedesDIN EN 1464:1995-01,DIN EN 1967:2003-02 andDIN EN 1967 Corrigendum1:2004-10www.beuth.deDocument comprises pagesIn case of doubt, the German-language original shall be considered a

4、uthoritative.1106.10 DIN EN 1464:2010-06 A comma is used as the decimal marker. National foreword This standard has been prepared by Technical Committee CEN/TC 193 “Adhesives” (Secretariat: AENOR, Spain). The responsible German body involved in its preparation was the Normenausschuss Materialprfung

5、(Materials Testing Standards Committee), Working Committee NA 062-04-55 AA Prfung von Konstruktions-klebstoffen, -klebeverbindungen und Kernverbunden. Amendments This standard differs from DIN EN 1464:1995-01, DIN EN 1967:2003-02 and DIN EN 1967 Corrigendum 1:2004-10 as follows: a) The title of the

6、standard has been changed. b) An environmental statement has been included (see clause 1). c) The wet peel test (formerly specified in DIN EN 1967:2003-02) has been included (see 7.2). d) For adherends made of metal, the thickness has been amended (see 5.3). e) When making the autographic recording

7、of force versus crosshead movement (force versus distance peeled), the first 25 mm of peel are to be disregarded (see 7.1 “Dry peel test”). f) Details regarding the failure type have been amended. Previous editions DIN 53289: 1975-05, 1979-09 DIN V ENV 1967: 1995-09 DIN EN 1967: 2003-02 DIN EN 1967

8、Corrigendum 1: 2004-10 DIN EN 1464: 1995-01 2 EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 1464 February 2010 ICS 83.180 Supersedes EN 1464:1994, EN 1967:2002English Version Adhesives - Determination of peel resistance of adhesive bonds - Floating roller method Adhsifs - Dtermination de la r

9、sistance au pelage des assemblages - Mthode des galets mobiles Klebstoffe - Bestimmung des Schlwiderstandes von Klebungen - Rollenschlversuch This European Standard was approved by CEN on 28 December 2009. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the

10、conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN member. This European Standard exists in

11、 three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions. CEN members are the national standards bodies

12、 of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingd

13、om. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2010 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 1464:2010: EEN 1464:

14、2010 (E) 2 Contents Page Foreword 31 Scope 42 Normative references 43 Terms and definitions .44 Apparatus .55 Test specimens 66 Conditioning and testing atmosphere .77 Procedure .77.1 Dry peel test .77.2 Wet peel test .88 Expression of results 89 Test report 8DIN EN 1464:2010-06 EN 1464:2010 (E) 3 F

15、oreword This document (EN 1464:2010) has been prepared by Technical Committee CEN/TC 193 “Adhesives”, the secretariat of which is held by AENOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by Aug

16、ust 2010, and conflicting national standards shall be withdrawn at the latest by August 2010. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent

17、rights. This document supersedes EN 1464:1994 and EN 1967:2002. This document has been prepared under a mandate given to CEN by the European Commission and the European Free Trade Association, and supports essential requirements of EC Directive(s). According to the CEN/CENELEC Internal Regulations,

18、the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Neth

19、erlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. DIN EN 1464:2010-06 EN 1464:2010 (E) 4 1 Scope This European Standard specifies a floating roller method for the determination of the peel resistance of adhesive bonds between one rigid

20、 adherend and one flexible adherend when tested under specified conditions of preparation and testing. NOTE The use the floating roller produces more constant numerical data than other peel methods, but it should not be expected that the flexible adherend will conform to the surface of the roller. S

21、AFETY STATEMENT Persons using this document should be familiar with the normal laboratory practice, if applicable. This document does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate safety and health pr

22、actices and to ensure compliance with any regulatory conditions. ENVIRONMENTAL STATEMENT It is understood that some of the material permitted in this standard may have negative environmental impact. As technological advantages lead to acceptable alternatives for these materials, they will be elimina

23、ted from this standard to the extent possible. At the end of the test, the user of the standard should take care to carry out an appropriate disposal of the wastes, according to local regulation. 2 Normative references The following referenced documents are indispensable for the application of this

24、document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 923:2005, Adhesives Terms and definitions EN ISO 291, Plastics - Standard atmospheres for conditioning and testing (ISO 291:200

25、8) EN ISO 10365, Adhesives - Designation of main failure patterns (ISO 10365:1992) 3 Terms and definitions For the purposes of this document, the terms and definitions given in EN 923:2005 and the following apply. 3.1 peel resistance average force per unit test specimen width, measured along the bon

26、d line, required to separate progressively the two members of a bonded test specimen under specified conditions of test NOTE It is expressed in newtons per millimetre of width (N/mm). 3.2 wet-peel resistance peel resistance after application of water containing a wetting agent DIN EN 1464:2010-06 EN

27、 1464:2010 (E) 5 4 Apparatus 4.1 Tensile testing machine1), capable of maintaining a pre-determined constant crosshead rate to be reported in the test report (preferred rate: 100 mm/min). It shall be provided with a suitable self-aligning grip to hold the test specimen. The jaws of this grip shall f

28、irmly engage the outer 25 mm of the end of the flexible adherend. The grip and attachments shall be so constructed that they will move into alignment with the test specimen as soon as the force is applied, so that the flexible member of the test specimen will coincide with the direction of the appli

29、ed pull through the centre line of the grip assembly. The machine shall be autographic, giving a chart that can be read in terms of millimetres of crosshead movement as one coordinate and applied force as the other coordinate. All equipment shall be calibrated regularly. It is recommended that equip

30、ment should be essentially free of inertial forces during use. The machine shall permit the measurement and recording of the applied force with an accuracy of 1 %. 4.2 Peel test fixture, for supporting the test specimen (see Figure 1). The fixture shall be attached to one of the cross-arms of testin

31、g machine (4.1). The 25 mm diameter rollers on the test fixture shall roll freely. The angle determined by the rollers and the use of dual roller bearings are critical and the rollers shall therefore be carefully maintained. 1) See for instance ISO 5893:2002, Rubber and plastics test equipment Tensi

32、le, flexural and compression types (constant rate of traverse) Specification. DIN EN 1464:2010-06 EN 1464:2010 (E) 6 Dimensions in millimetres Key 1 Rigid adherend 2 Peeling zone 3 Flexible adherend 4 Mild steel 5 Dual roller bearing type Figure 1 Peel test fixture for supporting test specimens 5 Te

33、st specimens 5.1 Test specimens of the dimensions shown in Figure 2 may be prepared individually or cut from bonded panels. Laminated test panels, or individual test specimens, shall consist of two adherends properly prepared and bonded together. 5.2 The adherends and the surface treatment shall be

34、in accordance with the intended application and process. The adhesive shall be applied in accordance with the manufacturers recommendations to obtain an optimum bond with minimum of variations. NOTE Direct comparison of different adhesives can be made only when test specimen construction, adherend m

35、aterials and dimension and test conditions are identical. DIN EN 1464:2010-06 EN 1464:2010 (E) 7 5.3 The thickness of the flexible adherend shall be (0,5 0,02) mm and that of the rigid adherend shall be (2,5 0,1) mm in the case of metals, or thicker if other adherends are used in order the reduce th

36、e deformation of the rigid adherend. 5.4 If the test specimens are cut from the bonded panels (see Figure 2) it shall not be deleterious to the bond. The width shall be either: a) 25 mm (the preferred width); or b) any other convenient width, provided that the test equipment is suitably adapted and

37、the width is stated in the test report. NOTE The method of cutting the test specimens is dependent upon the adherend and adhesive compositions. Milling and band-sawing are two methods commonly used for this purpose. 5.5 The unbounded end of the flexible adherend shall be bent perpendicular to the ri

38、gid adherend for clamping in the grip of the testing machine. 5.6 The number of specimens to be tested shall be as specified in the material specification or, if not so specified, shall be not less than five. Dimensions in millimetres Key a) angled b) not angled 1 direction of rolling s1thickness of

39、 the rigid adherend s2thickness of the flexible adherend Figure 2 Test specimen 6 Conditioning and testing atmosphere The test specimens shall be conditioned and tested in one of the standard laboratory atmospheres specified in EN ISO 291. 7 Procedure 7.1 Dry peel test Insert the test specimen into

40、the peel test fixture (4.2) as shown in Figure 1, with the unbounded end of the flexible adherend gripped in the jaw of the testing machine (4.1). Peel the specimen at a constant crosshead separation rate of (100 5) mm/min, unless otherwise specified. If the rigid adherend bends or is distorted DIN

41、EN 1464:2010-06 EN 1464:2010 (E) 8 during the test, it is recommended that the specimen be redesigned with a rigid adherend stiff enough to ensure even peeling. During the peel test, make an autographic recording of force versus crosshead movement (force versus distance peeled) over a length of a le

42、ast 115 mm of the bond line disregarding the first 25 mm of peel. Disregard the results if failure occurs outside the peeling zone as defined in Figure 1. 7.2 Wet peel test Insert the test specimen into the peel test fixture (4.2) as shown in Figure 1, with the unbounded end of the flexible adherend

43、 gripped in the jaw of the testing machine (4.1). Peel the specimen at a constant crosshead separation rate of (100 5) mm/min, unless otherwise specified. If the rigid adherend bends or is distorted during the test, it is recommended that the specimen be redesigned with a rigid adherend stiff enough

44、 to ensure even peeling. Stop the crosshead after peeling about 75 mm of the bonded length. Then apply several drops of water containing a wetting agent (for example 0,5 % to 1,0 % of a detergent) to the crack opening. After the application of this liquid the peeling process shall be immediately com

45、menced. The test shall be continued until the complete sample is peeled. An autographic recording of force versus crosshead movement (force versus distance peeled) shall be made. Disregard the results if failure occurs outside the peeling zone as defined in Figure 1. 8 Expression of results Determin

46、e from the autographic curve, for at least 115 mm of peeling (disregarding the first 25 mm and the last 25 mm), the average peeling resistance, in newtons per millimetre (N/mm) of the test specimen width, required to separate the adherends. The average force may be determined from the curve by one o

47、f the following methods: a) a planimeter; b) a gravimetric method, as follows: Cut out the area of the chard paper surrounded by the curve and the base line (abscissa) and weigh it. Determine the area by dividing its mass by the previously determine mass per surface area of the chart paper. Divide t

48、he area thus found by the length of the base line (corresponding to 80 mm peeling length), to obtain the average height of the curve (and hence the average peeling force); c) by drawing the best straight line through the peeling curve using a straight edge; d) by any other method such as computer as

49、sisted. Also record the maximum and minimum forces for each individual specimen. 9 Test report The test report shall include the following information: a) a reference to this European Standard; DIN EN 1464:2010-06 EN 1464:2010 (E) 9 b) identification of the adhesive tested, including type, source, manufacturers code number, batch or lot number, form, etc.; c) identification of adherends, including material, thickness, width and surface preparation; d) description of the bonding process, in