ASTM B760-2007(2013) Standard Specification for Tungsten Plate Sheet and Foil《钨制厚板材、薄板材和箔的标准规格》.pdf

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1、Designation: B760 07 (Reapproved 2013)Standard Specification forTungsten Plate, Sheet, and Foil1This standard is issued under the fixed designation B760; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A

2、number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This specification covers wrought unalloyed tungstenplate, sheet, and foil.1.2 The values stated in inch-pound units are to be regarded

3、as standard. The values given in parentheses are mathematicalconversions to SI units that are provided for information onlyand are not considered standard.1.3 The following precautionary caveat pertains only to thetest method portions of this specification: This standard doesnot purport to address a

4、ll of the safety concerns, if any,associated with its use. It is the responsibility of the user of thisstandard to establish appropriate safety and health practicesand determine the applicability of regulatory limitations priorto use.2. Referenced Documents2.1 ASTM Standards:2E29 Practice for Using

5、Significant Digits in Test Data toDetermine Conformance with Specifications3. Terminology3.1 Lot Definitions:3.1.1 ingot, nno definition required.3.1.2 A manufacturing lot shall consist of a material of thesame size, shape, condition, and finish produced from the ingotor powder blend by the same rol

6、ling reduction schedule and thesame heat treatment parameters. Unless otherwise agreedbetween manufacturer and purchaser, a lot shall be limited tothe product of an 8 h period for final continuous anneal, or toa single furnace load for final batch anneal.3.1.3 A chemical analysis lot shall consist o

7、f a singlepowder blend in the case of products manufactured frompressed and sintered powder metallurgy shapes, or a singleingot in the case of products manufactured from ingot.3.2 Product Forms:3.2.1 foil, na flat product less than 0.005 in. (0.13 mm) inthickness.3.2.2 plate, na flat product 0.188 i

8、n. (4.75 mm) or more inthickness.3.2.3 sheet, na flat product from .005 in. (0.13 mm) to0.187 in. (4.75 mm) in thickness.4. Ordering Information4.1 Orders for material under this specification shall includethe following information:4.1.1 Material identification and metallurigical condition(Section 7

9、),4.1.2 Product form (Section 3),4.1.3 Chemical requirements (Table 1),4.1.4 Tolerances (Section 9, Table 2, and Fig. 1),4.1.5 Workmanship and quality level requirements (Section10),4.1.6 Packaging (Section 14),4.1.7 Marking (Section 14),4.1.8 Certification and reports (Section 13), and4.1.9 Disposi

10、tion of rejected material (Section 12).5. Materials and Manufacture5.1 The various tungsten flat products covered by thisspecification shall be formed with the conventional rolling,forging, or extrusion equipment, normally found in primaryferrous and nonferrous plants.5.2 The ingot metal is consolid

11、ated employing either thepowder metallurgy or vacuum-arc-casting process.6. Chemical Composition6.1 The tungsten ingots or billets for conversion to finishedproducts covered by this specification shall conform to therequirements of the chemical composition prescribed in Table1.6.2 Heat Analysis:6.2.

12、1 Heat analysis is an analysis made by the manufacturerof the metal on a representative sample of powder from a singlepowder blend in the case of material made from pressed and1This specification is under the jurisdiction of ASTM Committee B10 onReactive and Refractory Metals and Alloys and is the d

13、irect responsibility ofSubcommittee B10.04 on Molybdenum and Tungsten.Current edition approved May 1, 2013. Published May 2013. Originallyapproved in 1986. Last previous edition approved in 2007 as B760 07. DOI:10.1520/B0760-07R13.2For referenced ASTM standards, visit the ASTM website, www.astm.org,

14、 orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States1sintered powder

15、billets, or on a representative sample of a castingot or intermediate product from that ingot in the case ofmaterial made from cast ingot.6.2.2 Chemical lot analysis shall be as specified in Table 1,with the exception of oxygen which shall be reported forinformation only, and not be required to meet

16、 the requirementsof Table 1.6.3 Check Analysis:6.3.1 Check analysis is an analysis made by the purchaser orthe manufacturer of the metal after it has been processed intofinished mill forms, and is either for the purpose of verifyingthe composition of a heat or lot, or to determine variations inthe c

17、omposition within a heat or lot.6.3.2 Check analysis tolerances do not broaden the specifiedheat analysis requirements but cover variations between labo-ratories in the measurement of chemical content.6.3.3 Check analysis limits shall be as specified in Table 1.6.3.4 The manufacturer shall not ship

18、material that isoutside the limits specified in Table 1.7. Metallurgical Condition7.1 Plate, sheet and foil shall be furnished in one of thefollowing conditions as designated on the purchase order:Form Metallurgical ConditionPlate hot-rolledhot-rolled, stress-relievedSheet hot-rolledhot-rolled, stre

19、ss-relievedcold-rolledcold-rolled, stress-relievedFoil cold-rolledcold-rolled, stress-relieved7.2 Other conditions can be specified as agreed upon be-tween the purchaser and the manufacturer at the time ofpurchase.8. Significance of Numerical Limits8.1 For the purpose of determining compliance with

20、thespecified limits for requirements of the properties listed in thefollowing table, an observed value or a calculated value shallbe rounded as indicated in accordance with the roundingmethods of Practice E29.Property Rounded Unit for Observedor Calculated ValueChemical composition, and tolerances(w

21、hen expressed as decimals)nearest unit in the last right-hand placeof figures of the specified limitTensile strength and yield strength nearest 1000 psi (10 MPa)Elongation nearest 1 %9. Permissible Variations in Dimensions9.1 The thickness tolerances on tungsten products coveredby this specification

22、 shall be as specified in Table 2.9.2 The width tolerances shall be as agreed upon betweenthe manufacturer and the purchaser. In general, shearingtolerance will be 6116 in. (61.6 mm) and slitting tolerance willbe 6132 in. (60.8 mm).9.3 The length and camber tolerances shall be as agreedupon between

23、the manufacturer and the purchaser. In general,length and camber tolerances will show a maximum deviationof +116 in., 0/ft (1.6 mm/m) of length.9.4 Flatness tolerances on tungsten flat products shall be asfollows:Thickness, in.(mm) Flatness Deviation,max,%0.0050.187 (0.134.75) 40.1880.625 (4.7515.9)

24、 59.4.1 Determine flatness deviation (Fig. 1) as follows:Flatness deviation, % 5 H/L! 3100where:H = maximum vertical distance between a flat referencesurface and the lower surface of the flat product, andL = minimum horizontal distance between the highest pointof the flat product where H is determin

25、ed, and the pointof contact of the lower surface of the flat product witha flat reference surface.10. Workmanship, Finish, and Appearance10.1 Cracks, seams, slivers, blisters, burrs, and other inju-rious imperfections shall not exceed standards of acceptabilityagreed upon by the manufacturer and the

26、 purchaser.10.2 Tungsten plate, sheet, and foil shall be free of injuriousinternal and external imperfections of a nature that willinterfere with the purpose for which it was intended.10.3 Methods of testing for these defects and standards ofacceptability shall be as agreed upon between the manufact

27、urerand the purchaser.10.4 Material may be supplied with as-rolled, as-cleaned,as-machined, or as-ground finish.10.5 The manufacturer shall be permitted to remove surfaceimperfections provided such removal does not reduce thedimensions below the minimum permitted by the tolerances forthat dimension.

28、11. Sampling and Test Methods11.1 Care shall be exercised to ensure that the sampleselected for testing is representative of the material and formand that it is not contaminated by the sampling procedure. Ifthere is any question relating to the sampling technique or theanalysis of the sample, the me

29、thods of sampling and analysisshall be as agreed upon between the purchaser and themanufacturer.11.2 Test Methods:11.2.1 Chemistry:TABLE 1 Chemical Composition/Check AnalysisElementComposition,max, %Permissible Variations inCheck Analysis, %C 0.010 0.002OA0.010 + 10 % relativeN 0.010 + 0.0005Fe 0.01

30、0 + 0.001Ni 0.010 + 0.001Si 0.010 + 0.001AIf chemical analysis is performed on a sample from the powder blend used tomake the finished product, oxygen will be reported for information only.B760 07 (2013)211.2.1.1 Analyses shall be made using the manufacturersstandard methods.11.2.1.2 The chemical co

31、mposition enumerated in thisspecification shall in case of disagreement, be determined inaccordance with the methods approved for referee purposes byASTM International. Where such methods are not available,methods of analysis as mutually agreed upon by the manufac-turer and the purchaser shall be em

32、ployed.12. Rejection and Referee12.1 Material that fails to conform to the requirements ofthis specification or to authorized modifications may be re-jected. Rejection for failure of the material to meet therequirements of this specification shall be reported to themanufacturer within 30 calendar da

33、ys from the receipt of thematerial by the purchaser.12.2 Unless otherwise specified, rejected material may bereturned to the manufacturer at the manufacturers expense,unless the purchaser receives, within four weeks of the noticeof rejection, other instructions for disposition.12.3 In the event of d

34、isagreement between the manufacturerand the purchaser on the conformance of the material to therequirements of the specification or any special test specifiedby the purchaser, a mutually acceptable referee shall performthe tests in question. The results of the referees testing shall beused in determ

35、ining conformance of the material to thisspecification.13. Certification13.1 If requested, the manufacturer shall supply at leastthree copies of a report of the heat analysis of each melt orpowder lot represented in the shipment, and reports of theresult of tests of each size of each heat or powder

36、lot todetermine properties.13.2 The report shall include the purchase order number,heat or powder lot number, this specification number, type andmetallurgical condition, nominal thickness, and quantity andnumber of items covered by the shipment.14. Packaging and Package Marking14.1 IdentificationUnl

37、ess otherwise specified, each plateor sheet shall be legibly and conspicuously marked or taggedwith the number of this specification, material type andmetallurgical condition, heat or lot number, manufacturersidentification, and the nominal thickness gage in inches. Allmarkings must withstand ordina

38、ry handling and shall becapable of removal with standard cleaning solvents. Themarking shall have no deleterious effect on the material or itsperformance.TABLE 2 Permissible Thickness VariationsSpecified Width,in. (mm)Specified Thickness,in. (mm)Thickness Tolerance,Ain. (mm)12 (305) and under 0.005

39、to 0.010 (0.130.25) 0.001 (0.0254)over 0.010 to 0.020 (0.250.51) 0.002 (0.051)over 0.020 (0.51) 10 %Over 12 to 24 (305610), over 0.010 to 0.025 (0.250.64) 0.0025 (0.064)over 0.025 (0.64) 10 %ATolerances for foil shall be as agreed upon between the producer and the purchaser.Flatness Deviation, % = (

40、H/L) x 100H = maximum distance between flat surface and lower surface of sheet.L = minimum distance between highest point on sheet and point of contact with flat surface.FIG. 1 Plate and Sheet Flatness TolerancesB760 07 (2013)314.1.1 Coiled sheet and foil shall be similarly marked at theoutside end

41、of each coil.14.2 All material shall be packaged in such a manner as toassure safe delivery to its destination when properly trans-ported by any common carrier.14.3 The package shall be so marked as to indicate thenature of any special handling required.14.4 Each bundle, box, or coil shall be legibl

42、y and conspicu-ously marked or tagged with the following information:14.4.1 Purchase order or contract number,14.4.2 Name of material,14.4.3 Grade,14.4.4 Size,14.4.5 Lot, heat, or ingot number,14.4.6 Metallurgical condition,14.4.7 Gross, net and tare weights, and14.4.8 ASTM specification number.15.

43、Keywords15.1 foil; plate; sheet; tungstenASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and th

44、e riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision o

45、f this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you should

46、make your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).B760 07 (2013)4