ASTM E1096-1986(2006) Standard Specification for Laboratory Glass Separatory Funnels《实验室玻璃分液漏斗》.pdf

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1、Designation: E 1096 86 (Reapproved 2006)Standard Specification forLaboratory Glass Separatory Funnels1This standard is issued under the fixed designation E 1096; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revi

2、sion. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.INTRODUCTIONSeparatory funnels are used in laboratories primarily for liquid extractions, and are intended tofacilitate the separation of

3、two immiscible liquids of different densities into separate layers. Somefunnels are used to add reagent solution into a reaction vessel. They are, therefore, often provided witha tapered ground joint at the bottom of the delivery stem for joining to vessels having similarly taperedground necks. They

4、 may also be provided with pressure equalizing side arms.1. Scope1.1 This specification provides standard dimensional re-quirements for glass separatory funnels for general laboratoryuse.2. Referenced Documents2.1 ASTM Standards:2E 438 Specification for Glasses in Laboratory ApparatusE 671 Specifica

5、tion for Maximum Permissible Thermal Re-sidual Stress in Annealed Glass Laboratory ApparatusE 675 Specification for Interchangeable Taper-GroundStopcocks And StoppersE 676 Specification for Interchangeable Taper-GroundJointsE 694 Specification for Laboratory Glass Volumetric Appa-ratusE911 Specifica

6、tion for Glass Stopcocks with Polytetrafluo-roethylene (PTFE) Plugs3. Classification3.1 Separatory funnels shall be in the following types andsizes:3.1.1 Type 1ACylindrical shape with open top.3.1.1.1 Sizes60, 125, and 250 cm33.1.2 Type 1BCylindrical with stopper finish top.3.1.2.1 Sizes60, 125, 250

7、, 500, and 1000 cm3.3.1.3 Type 1CCylindrical with stopper finish top, gradu-ated.3.1.3.1 Sizes125, 250, 500, and 1000 cm3.3.1.4 Type 2Globe shape with stopper finish top.3.1.4.1 Sizes60, 125, 250, 500, 1000, 2000, and 4000cm3.3.1.5 Type 3Globe shape, “French,” with stopper finishtop.3.1.5.1 Sizes125

8、, 250, 500, and 1000 cm3.3.1.6 Type 4Pear shape, Squibb, with stopper finish top.3.1.6.1 Sizes20, 60, 125, 250, 500, 1000, 2000, and 4000cm3.NOTE 1The term millilitre (mL) is commonly used as a special namefor the cubic centimetre (cm3) and similarly the litre (L) for 1000 cubiccentimetres, in accor

9、dance with the International System of Units (SI).4. Materials and Annealing4.1 Separatory funnels shall be made of borosilicate glassconforming to the requirement of Type 1, Class A of Specifi-cation E 438.4.2 Maximum residual thermal stress shall be such as toconform to Specification E 671.5. Desi

10、gn5.1 Type 1 cylindrical separatory funnels shall have straightsides and comply with the dimensions given in Table 1. (Type1A stem length shall comply with Table 2.) See Fig. 1, Type1A; 1B; and 1C.5.2 Type 2 globe-shaped separatory funnels shall be roughlyglobular in shape and have dimensions comply

11、ing with thosegiven in Table 2. See Fig. 2, Type 2.5.3 Type 3 separatory funnels shall be like Type 2, however,a straight-walled portion shall be between the globe and thestopcock assembly and shall meet the dimensions listed in1This specification is under the jurisdiction of ASTM Committee E41 onLa

12、boratory Apparatus and is the direct responsibility of Subcommittee E41.01 onApparatus.Current edition approved Nov. 1, 2006. Published December 2006. Originallyapproved in 1986. Last previous edition approved in 2001 as E 1096 86 (2001)e12For referenced ASTM standards, visit the ASTM website, www.a

13、stm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.Table 2

14、, except for stem length which shall have a maximumlength of 40 mm. See Fig. 2, Type 3.5.4 Type 4 Squibb separatory funnels shall be pear-shapedor conical-shaped and meet the requirements of Table 3. SeeFig. 2, Type 4.5.5 Type 1 and 4 separatory funnels may be supplied with ataper-ground joint below

15、 the stopcock, (see Specification E 676and Fig. 1C. Type 1 funnels with this feature may also havepressure equalizing tubes placed at the back or opposite side ofthe funnel when it is in the position of normal use with thehandle of the stopcock on the right. See Fig. 1B).5.6 All types except Type 1A

16、 shall have stoppers or betaper-ground to receive stoppers in accordance with Specifica-tions E 675 or E 676. Stoppers of suitable inert plastic materialmay be permitted as an alternative to glass but must alsocomply with Specification E 675. All stoppers shall bear a sizeidentification.5.7 All type

17、s shall have stopcock assemblies. They shall bedesigned to permit smooth and precise control of outflow andto meet the permissible leakage rate requirements allowed inSpecification E 675. Stopcocks shall be made of glass or fromsuitable inert plastic material such as polytetrafluoroethylene(PTFE) an

18、d must comply with Specification E911, or form aseal by having PTFE plug ends butt against a constriction in theglass shell.5.8 Delivery stems for Types 1B and C, 3, and 4 should havea bore wide enough to avoid formation of a liquid column, thatcould lead to unsatisfactory separation. Type 1A and Ty

19、pe 2FIG. 1 Cylindrical Body FunnelsType 2 Type 3 Type 4FIG. 2 Globe and Squibb-Pear Shaped Body FunnelsTABLE 1 Cylindrical Body FunnelsNominal Capacity,mL 60 125 250 500 1000Body height, max 135 200 225 290 390(mm) (see Fig.1“L1”)Body diameter, 34 44 53 67 79max (mm)Body wall thick- 0.8 0.8 0.9 0.9

20、1.3ness, min (mm)Stem length, max 100 100 100 100 100(mm) (see Fig.1“S1”)Stem diameter, 12 12 12 12 12max (mm)Stem wall thick- 1.5 1.5 1.5 1.5 1.5ness min (mm)Stopcock size 2 2 2 4 4Stopper size 16 22 22 27 27Stem taper- 14/20 24/40 24/40 24/40 .ground jointE 1096 86 (2006)2funnel stems shall confor

21、m to stem dimensions of Table 2.Stem tip shall be at an angle of 30 or 45.6. Graduations6.1 Type 1C separatory funnels shall have a graduated scaleplaced centrally about the vertical axis of the funnel when it isin position of normal use with the handle of the stopcock on theright. See Table 4 for s

22、pecifications. (For graduation patternand figuring see Specification E 694.)6.1.1 The graduation marks may be figured in ascendingorder or in both ascending and descending order.6.1.2 Subdivision and numbering shall conform to Table 4.7. Markings7.1 Each separatory funnel shall be permanently marked

23、with the name or known trademark of the manufacturer, orboth, the nominal capacity, except for graduated cylindricalfunnels, and the symbol cm3, mL, or L.8. Keywords8.1 funnels; glass; separatoryASTM International takes no position respecting the validity of any patent rights asserted in connection

24、with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible te

25、chnical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consider

26、ation at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr

27、Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(

28、www.astm.org).TABLE 2 Globe Shaped Body FunnelsNominal Capacity, (mL) 30 60 125 250 500 1000 2000 4000Body height, max (mm) (see Fig. 2 “L2”) 75 85 110 135 175 215 255 290Body diameter, max (mm) 50 55 70 90 110 140 170 210Body wall thickness, min (mm) 0.8 0.8 0.8 0.9 0.9 1.3 1.3 1.3Straight wall len

29、gth, max (mm) (Type 3 only) (see Fig. 2 “S3”) 110 130 130 130 135 140 165 .Straight wall diameter, max (mm) (Type 3 only) 18 18 18 18 25 35 35 .Stem length, max (mm)A(see Fig. 2“ S2”) 180 180 180 180 180 180 135 135Stem diameter, max (mm) 12 12 12 12 12 12 14 15Stem wall thickness, min (mm) 1.5 1.5

30、1.5 1.5 1.5 1.5 1.5 1.5Stopcock size 2 2 2 2 4 4 6 8Stopper size 16 16 22 22 27 27 38 38AType 3 50 mm max.TABLE 3 Squibb Pear Shaped Body FunnelsNominal Capacity, (mL) 30 60 125 250 500 1000 2000 4000Body height, max (mm) (see Fig. 2 “L4”) 85 140 160 200 225 255 340 480Body diameter, max (mm) 45 60

31、65 80 105 125 155 210Body wall thickness, min (mm) 0.8 0.8 0.8 0.9 0.9 1.0 1.3 1.3Stem length, max (mm) (see Fig. 2 “S4”) 75 75 75 75 75 75 75 75Stem diameter, max (mm) 12 12 12 12 12 12 14 15 or 19AStem wall thickness, min (mm) 1.5 1.5 1.5 1.5 1.5 1.5 1.5 1.5Stopcock size 2 2 2 2 or 4 4 4 6 8 or 10

32、AStopper size 9 or 13 16 22 22 27 27 38 38Stem taper-ground joint . . 14/20,19/22or 24/4024/40 24/40 24/40 . .TABLE 4 Graduated Cylindrical Body FunnelsNominal Capacity(mL)50 100 125 250 500 1000Subdivision (mL) 5 5 1 2 or 5 5 10Numbered at leastat every milli-litre10 10 10 20 or 50 50 100E 1096 86 (2006)3