ASTM E1094-2004(2015) 1902 Standard Specification for Pharmaceutical Glass Graduates《制药用玻璃量杯的标准规格》.pdf

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1、Designation: E1094 04 (Reapproved 2015)Standard Specification forPharmaceutical Glass Graduates1This standard is issued under the fixed designation E1094; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A

2、 number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This specification covers glass graduates suitable forlaboratory, pharmaceutical, and other uses, in both conical andcylindrical shape

3、s.2. Referenced Documents2.1 ASTM Standards:2E438 Specification for Glasses in Laboratory ApparatusE671 Specification for Maximum Permissible Thermal Re-sidual Stress in Annealed Glass Laboratory ApparatusE694 Specification for Laboratory Glass Volumetric Appa-ratusE920 Specification for Commerciall

4、y Packaged LaboratoryApparatusE921 Specification for Export Packaged Laboratory Appa-ratusE1133 Practice for Performance Testing of Packaged Labo-ratory Apparatus for United States Government Procure-mentsE1157 Specification for Sampling and Testing of ReusableLaboratory Glassware2.2 Other Document:

5、NIST Handbook 44, Section 4.44 Graduates33. Classification3.1 Graduates shall be in the following types and sizes:3.1.1 Type 1Graduated in metric scale only.3.1.1.1 Sizes5, 10, 25, 50, 100, 250, 500, and 1000 mL.3.1.2 Type 2Graduated in both metric and inch-poundscales.3.1.2.1 Sizes5 mLand 60 minims

6、, 10 mLand 120 minims,15 mL and 4 fluid drams, 25 mL and 8 fluid drams, 50 mL and2 fluid oz, 100 mL and 4 fluid oz, 250 mL and 8 fluid oz, 500mL and 16 fluid oz, and 1000 mL and 32 fluid oz.NOTE 1The term millilitre (mL) is commonly used as a special namefor the cubic centimetre (cm3) in accordance

7、with the International Systemof Units (SI). (The inch-pound fluid ounce is equivalent to 29.5735 mL,hence, the fluid dram is equivalent to 3.6967 mL and the minim isequivalent to 0.0616 mL).4. Material and Annealing4.1 Graduates shall be made of borosilicate glass conform-ing to the requirements of

8、Type 1, Class A of SpecificationE438.4.2 Maximum residual thermal stress shall be such as toconform to Specification E671.5. Design5.1 StyleGraduates having a capacity of more than 15 mL(4 fluid drams) may be either conical or cylindrical. Thosehaving a capacity of 15 mL or less shall be cylindrical

9、.5.2 DimensionsThe inside measurement from the bottomof the graduate to the top capacity graduation shall be not lessthan five times the inside diameter on a cylindrical graduateand two times on a conical graduate. The inside measurementfrom the bottom of the graduate to the point representing onefo

10、urth of the capacity shall not be less than the inside diameterat that point.5.3 Pour-Out SpoutAll graduates shall have a pour-outspout that ensures delivery of an unbroken stream of liquidwithout wetting the outside wall of the graduate.5.4 BaseThe base shall be perpendicular to the verticalaxis of

11、 the graduate. The base shall be large enough so that theempty graduate will stand on a surface 15 from the horizontal.6. Graduations6.1 Each graduate shall have clear graduation markingsperpendicular to the vertical axis of the graduate and parallel toeach other. They shall conform to the requireme

12、nts of Speci-fication E694.6.1.1 No graduation line shall extend less than one fourththe circumference of the graduate. Graduates shall have aninitial interval that is not subdivided, equal to not less than onefifth and not more than one fourth of the capacity of thegraduate. Except for this interva

13、l, the values of all graduated1This specification is under the jurisdiction of ASTM Committee E41 onLaboratory Apparatus and is the direct responsibility of Subcommittee E41.01 onLaboratory Ware and Supplies.Current edition approved June 1, 2015. Published July 2015. Originally approvedin 1991. Last

14、 previous edition approved in 2009 as E1094 04(2009). DOI:10.1520/E1094-04R15.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandardsvolume information, refer to the standards Document Summary page ont

15、he ASTM website.3Available from National Institute of Standards and Technology (NIST),Gaithersburg, MD 20899.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States1intervals shall be the same. Each main graduation line shall bemarked to indi

16、cate its value; intermediate lines shall not bemarked. Numerals shall be uniformly positioned, either di-rectly upon or immediately above the graduation line to whichthey refer. Numerals shall be set in from the ends of the linesa sufficient distance to permit the line ends to be used inmaking a men

17、iscus setting.6.1.2 Type 1 graduates shall have main graduation lines thatencircle the graduate at least 90 %. Intermediate lines shallextend at least 50 % of the circumference of the graduate.6.1.3 Type 2 graduates (double scale) shall have a clearspace between the ends of the main graduation lines

18、 of the twoscales. This space shall be approximately 90 % removed fromthe pour-out spout of the graduate and shall comply to therequirements of Table 1.6.2 Graduation Marking Details:6.2.1 Capacities, graduation ranges, values of graduatedintervals, and numbered graduations applicable to single-scal

19、egraduates and to appropriate portions of double-scalegraduates, are shown in Table 2.6.2.2 Permanency of MarkingsGraduation markings shallbe permanent and legible. They shall be applied by etching andfilling with a permanent pigment, by firing a ceramic enamelinto the glass without etching, or by a

20、pplying a stain and firinginto the glass without etching.6.3 Tolerances shall be as shown in Table 3 and in accor-dance with Table 3 of Section 4.44 of NIST Handbook 44.Pharmaceutical graduates are calibrated “to deliver” and at20C. The tolerance applicable at a specific graduation line isdetermined

21、 by the inside diameter of the graduate at the pointin question.7. Markings7.1 Each graduate shall be permanently marked with thename or trademark, or both, of the manufacturer; the letters“TD” or “EX,” or both; the calibration temperature, 20C; andthe units of capacity, such as mL for Type 1 gradua

22、tes, and mLand minims, fluid drams or fluid oz, for Type 2 graduates.8. Sampling8.1 For sampling and testing, refer to Specification E1157.9. Packaging9.1 Select from Specifications E920, E921, and E1133.10. Keywords10.1 glass; graduate; pharmaceuticalTABLE 1 Space Between Ends at Main Graduations o

23、nDouble-Scale GraduatesInside Diameter atGraduation LineSpace Between EndsLess than 40 mm 3 to 6 mm40 to 80 mm 6 to 13 mmOver 80 mm 10 to 16 mmTABLE 2 Graduation Line DetailsDouble-Scale GraduatesCapacityLeast GraduationLineSubdivisionNumbers atEach Even5 mL 1.0 mL 0.5 mL 1 mL10 mL 2.0 mL 1.0 mL 2 m

24、L25 mL 5.0 mL 5.0 mL 5 mL50 mL 10.0 mL 5.0 mL 10 mL100 mL 20.0 mL 10.0 mL 20 mL250 mL 50.0 mL 25.0 mL 50 mL500 mL 100.0 mL 25.0 mL 50 mL1000 mL 200.0 mL 50.0 mL 100 mL60 minims 15.0 minims 5.0 minims 10 minimsA120 minims 30.0 minims 10.0 minims 20 minimsB4 fluid drams 1.0 fluid drams 0.5 fluid drams

25、 1 fluid dram8 fluid drams 2.0 fluid drams 1.0 fluid drams 2 fluid drams2 fluid oz 0.5 fluid oz 0.25 fluid oz 0.5 fluid oz4 fluid oz 1.0 fluid oz 0.5 fluid oz 1 fluid oz8 fluid oz 2.0 fluid oz 0.5 fluid oz 1 fluid oz16 fluid oz 4.0 fluid oz 1.0 fluid oz 2 fluid oz32 fluid oz 8.0 fluid oz 2.0 fluid o

26、z 4 fluid ozAAlso at the first 15-minim graduation.BAlso at the first 30-minim graduation.TABLE 3 Maintenance and Acceptance Tolerances, in Excess andin Deficiency, for GraduatesInside Diameter of GraduateFromTo But NotIncludingTolerance FromTo But NotIncludingTolerancemillimetres milliliters in. mi

27、nims0 16 0.1 0916 216 21 0.29161316 321 26 0.41316 1116 626 31 0.6 1116 1516 1031 36 0.8 1516 1916 1536 41 1.1 1916 11316 2041 46 1.4 11316 2116 3046 51 1.8 2116 2516 4051 56 2.2 2516 2916 5056 61 2.8 2916 21316 6561 66 3.4 21316 3116 8066 71 4.1 3116 3516 9571 76 4.8 3516 3916 11076 81 5.6 3916 313

28、16 13081 86 6.4 3316 4116 15086 91 7.291 96 8.196 101 9.0E1094 04 (2015)2ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity o

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