ASTM B834-1995(2009) Standard Specification for Pressure Consolidated Powder Metallurgy Iron-Nickel-Chromium-Molybdenum (UNS N08367) and Nickel-Chromium-Molybdenum-Columbium (Nb) (.pdf

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1、Designation: B 834 95 (Reapproved 2009)Standard Specification forPressure Consolidated Powder Metallurgy Iron-Nickel-Chromium-Molybdenum (UNS N08367) and Nickel-Chromium-Molybdenum-Columbium (Nb) (UNS N06625)Alloy Pipe Flanges, Fittings, Valves, and Parts1This standard is issued under the fixed desi

2、gnation B 834; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision

3、or reapproval.1. Scope1.1 This specification covers pressure consolidated powdermetallurgy iron-nickel-chromium-molybdenum (UNSN08367) and nickel-chromium-molybdenumcolumbium (Nb)(UNS N06625) pipe flanges, fittings, valves, and parts intendedfor general corrosion or heat-resisting service.1.2 The va

4、lues stated in inch-pound units are to be regardedas standard. The values given in parentheses are mathematicalconversions to SI units that are provided for information onlyand are not considered standard.1.3 The following safety hazards caveat pertains only to testmethods portions, Sections 7.3 and

5、 13, of this specification:This standard does not purport to address all of the safetyconcerns, if any, associated with its use. It is the responsibilityof the user of this standard to become familiar with all hazardsincluding those identified in the appropriate Material SafetyData Sheet (MSDS) for

6、this product/material as provided bythe manufacturer, to establish appropriate safety and healthpractices, and to determine the applicability of regulatorylimitations prior to use.2. Referenced Documents2.1 ASTM Standards:2E8 Test Methods for Tension Testing of Metallic MaterialsE 1473 Test Methods

7、for Chemical Analysis of Nickel,Cobalt, and High-Temperature AlloysG28 Test Methods for Detecting Susceptibility to Inter-granular Corrosion in Wrought, Nickel-Rich, Chromium-Bearing AlloysG48 Test Methods for Pitting and Crevice Corrosion Re-sistance of Stainless Steels and Related Alloys by Use of

8、Ferric Chloride Solution2.2 Manufacturers Standardization Society of the Valveand Fittings Industry Standard:3SP-25 Standard Marking System for Valves, Fittings,Flanges, and Unions2.3 ASME/ANSI Standard:4ASME/ANSI B16.5 Pipe Flanges and Flanged Fittings3. Terminology3.1 Definitions of Terms Specific

9、 to This Standard:3.1.1 can, nthe container used to encapsulate the powderduring the pressure consolidation process; it is removed fromthe final part.3.1.2 compact, nthe consolidated powder from one can; itmay be used to make one or more parts.3.1.3 fill pin, nthe part of the compact in the spout us

10、ed tofill the can; it is not usually integral to the part produced.3.1.4 part, na single item coming from a compact, eitherprior to or after machining.3.1.5 powder blend, na homogeneous mixture of powderfrom one or more heats; it is limited to the amount that can bemixed in the same blender at one t

11、ime.3.1.6 rough part, nthe part prior to final machining.4. Ordering Information4.1 Orders for material under this specification shouldinclude the following information:4.1.1 Quantity (weight or number of pieces),4.1.2 Name of material or UNS number,4.1.3 Microstructure examination, if required (5.1

12、.4),4.1.4 ASTM designation and year of issue,4.1.5 Inspection (14.1),4.1.6 Whether rough part or finish machined (7.2.2),4.1.7 Supplementary requirements, when applicable, and4.1.8 If possible, the intended end use.1This specification is under the jurisdiction of ASTM Committee B02 onNonferrous Meta

13、ls and Alloys and is the direct responsibility of SubcommitteeB02.07 on Refined Nickel and Cobalt and Their Alloys.Current edition approved Oct. 1, 2009. Published October 2009. Originallyapproved in 1993. Last previous edition approved in 2003 as B 834 95 (2003).2For referenced ASTM standards, visi

14、t the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.3Available from Manufacturers Standardization Society of the Valve and FittingsIndustry (MSS), 12

15、7 Park St., NE, Vienna, VA 22180-4602, http:/www.mss-.4Available from American Society of Mechanical Engineers (ASME), ASMEInternational Headquarters, Three Park Ave., New York, NY 10016-5990, http:/www.asme.org.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA

16、 19428-2959, United States.5. Materials and Manufacture5.1 Manufacturing Practice:5.1.1 Compacts shall be manufactured by placing a singlepowder blend into a can, evacuating the can, and sealing it. Thecan material shall be selected to ensure that it has no deleteri-ous effect on the final product.

17、The entire assembly shall beheated and placed under sufficient pressure for a sufficientperiod of time to ensure that the final consolidated part is fullydense. The compact may represent one part or a number ofparts may be machined from it.5.1.2 The powder shall be produced by vacuum meltingfollowed

18、 by gas atomization.5.1.3 When powder from more than one heat is used tomake a blend, the heats shall be thoroughly mixed to ensurehomogeneity.5.1.4 When specified on the order, a section of the compactmay be sectioned and the microstructure examined to showporosity and other internal imperfections.

19、 This is usuallyperformed on the fill pin. In such cases, the section location andthe question of acceptable and unacceptable microstructureshall be agreed upon by the manufacturer and the purchaser.5.2 Heat Treatment:5.2.1 Alloy N06625 shall be supplied in the solution an-nealed condition. At the o

20、ption of the producer, the anneal maybe a separate operation following consolidation or may be partof the consolidation process. In either case, the temperatureshall be 1800F minimum.5.2.2 Alloy N08367 shall be supplied in the solution an-nealed condition.5.2.2.1 The heat treatment shall consist of

21、heating to aminimum temperature of 2025F and quenching in water orrapidly cooling by other means.6. Chemical Composition6.1 The material shall conform to the requirements forchemical composition prescribed in Table 1.6.2 If a product (check) analysis is performed by thepurchaser, the material shall

22、conform to the product (check)analysis variations prescribed in Table 2.7. Mechanical and Other Requirements7.1 Mechanical PropertiesThe material shall conform tothe requirements for mechanical properties prescribed in Table3 at room temperature.7.2 Hydrostatic TestsAfter machining, valve bodies, fi

23、t-tings, and other pressure-containing parts shall be tested to thehydrostatic shell-test pressures prescribed in ASME/ANSIB16.5 for the applicable steel rating for which the compact isdesigned, and shall show no leaks. Parts ordered under thesespecifications for working pressures other than those l

24、isted inthe American National Standard ratings shall be tested to suchpressures as may be agreed upon between the manufacturer andpurchaser.7.2.1 No hydrostatic test is required for welding neck orother flanges.7.2.2 The compact manufacturer is not required to performpressure tests on rough parts th

25、at are to be finish machined byothers. The fabricator of the finished part is not required topressure test parts that are designed to be pressure containingonly after assembly by welding into a larger structure. How-ever, the manufacturer of such parts is responsible as requiredin 15.1 for the satis

26、factory performance of the parts under thefinal test required in 7.2.7.3 DensityThe density shall be determined using samplesuspended from a scale and weighed in air and water usingArchimedes principle. The equipment used shall have accu-racy sufficient for the test. The measured value shall not be

27、lessthan 0.3047 lb/in.3(8.452 gm/cm3) for UNS N06625 and0.2904 lb/in.3(8.055 gm/cm3) for UNS N08367. (See Note 1.)NOTE 1The density is a function of alloy variations. Because of this,density differences may be the result of either alloy content or differencesin micro-porosity.7.4 Microstructure Exam

28、inationExaminations shall showsound and reasonably uniform material, free from injuriousTABLE 1 Chemical RequirementsElementComposition,%UNS N06625 UNS N08367Carbon, max 0.10 0.030Manganese, max 0.50 2.00Silicon, max 0.50 1.00Phosphorus, max 0.015 0.040Sulfur, max 0.015 0.030Chromium 20.00 to 23.00

29、20.00 to 22.00Molybdenum 8.00 to 10.00 6.00 to 7.00Nickel 58.0 minA23.50 to 25.50Iron 5.00 max balanceACobalt (when specified) 1.00 max .Columbium (Nb) 3.15 to 4.15 .Aluminum 0.50 max .Titanium 0.40 max .Nitrogen . 0.18 to 0.25Copper . 0.75 maxAElement shall be determined arithmetically by differenc

30、e.TABLE 2 Product Analysis ToleranceElementTolerance, Over the Maximum Limit or Under theMinimum Limit, %UNS N06625 UNS N08367Carbon, max 0.01 0.005Manganese, max 0.03 0.04Silicon, max 0.03 0.05Phosphorus, max 0.005 0.005Sulfur, max 0.003 0.005Chromium 0.25 0.25Molybdenum 0.15 0.15Nickel 0.35 0.25Ir

31、on 0.07 .Cobalt (when specified) 0.03 .Columbium (Nb) 0.15 .Aluminum 0.05 .Titanium 0.03 .Nitrogen . 0.01Copper . 0.04TABLE 3 Mechanical Property RequirementsAlloyTensile Strength Yield Strength Elongation,min%ksi MPa ksi MPaN06625N083671109575865550453453103030B 834 95 (2009)2porosity, voids, laps,

32、 cracks, segregations, and similar objec-tionable defects. The etching can be performed after theconsolidation or final heat treatment. If the sample fails to meetthe requirements of this section, all parts from that compactshall be rejected.8. Dimensions and Permissible Variations8.1 The parts shal

33、l conform to the sizes and shapes specifiedby the purchaser.9. Workmanship, Finish and Appearance9.1 The parts shall be uniform in quality and condition, andshall be free from injurious imperfections.10. Sampling10.1 LotA lot is defined as follows:10.1.1 A lot for chemical analysis shall consist of

34、onepowder blend.10.1.2 A lot for mechanical properties shall consist offinished parts with the same dimensions made from the samepowder blend consolidated in the same hot isostatic press usingthe same pressure, temperature, and time parameters andheat-treated in the same final heat-treatment charge.

35、10.1.3 A lot for density shall be all parts from the samecompact.10.2 Test Material Selection:10.2.1 Chemical AnalysisRepresentative samples shall betaken after powder blending or during subsequent processing.10.2.1.1 Check Analysis shall be wholly the responsibilityof the purchaser.10.2.2 Mechanica

36、l PropertiesTest specimens shall betaken from compacts in the final heat-treated condition fromlocations in that lot in order to be representative of that lot.10.2.3 DensityTest specimens shall be taken from the fillpin of each compact after consolidation or after final heat-treatment.11. Number of

37、Tests11.1 Chemical AnalysisOne test per lot.11.2 Mechanical PropertiesOne test per lot.11.3 DensityOne test per lot.12. Specimen Preparation12.1 The tension test specimens taken from the compactshall be machined to the form and dimensions of the standard2-in. (50.8-mm) gage length tension test speci

38、men shown inFig. 8 of Test Methods E8, except as specified in 12.2.12.2 In the case of small sections from which a standard testspecimen (specified in 12.1) cannot be taken, the tension testspecimen shall be as large as feasible and its dimensions shallbe proportional to those shown in Fig. 8 of Tes

39、t Methods E8.The gage length for measuring elongation shall be four timesthe diameter of the specimen.12.3 For the purpose of tests, extra compacts or test barsshall be provided as necessary. The test specimen, if cut froma flange, shall be cut tangentially from the flange portionapproximately midwa

40、y between the inner and outer surfacesand approximately midway between the front and back faces.Test bar compacts made separately must be processed in thesame manner as the parts.13. Test Methods13.1 The chemical composition and mechanical propertiesof the material as enumerated in this specificatio

41、n shall, in thecase of disagreement, be determined in accordance with thefollowing test methods:Test ASTM Test MethodsChemical analysis E 1473Tension E814. Inspection14.1 If specified, source inspection of the material by thepurchaser at the manufacturers plant shall be made as agreedupon between th

42、e manufacturer and the purchaser as part of thepurchase contract.15. Rejection and Rehearing15.1 Material tested by the purchaser that fails to conform tothe requirements of this specification may be rejected. Rejec-tion should be reported to the supplier promptly and in writing.In case of dissatisf

43、action with the results of the test, theproducer or supplier may make claim for a rehearing.16. Certification16.1 When specified in the purchase order or contract, aproducers or suppliers certification shall be furnished to thepurchaser stating that the material was manufactured, sampled,tested, and

44、 inspected in accordance with this specification andhas been found to meet its requirements. When specified in thepurchase order or contract, a report of the test results shall befurnished.17. Product Marking17.1 Identification marks consisting of the manufacturerssymbol or name, designation of serv

45、ice rating, specificationnumber, grade of material, and size shall be stamped legibly oneach part in accordance with MSS SP-25, and in such positionas not to injure the usefulness of the part.18. Keywords18.1 compact; iron-nickel-chromium-molybdenum; nickel-chromium-molybdenum-columbium; powder part

46、s; pressureconsolidated powder metallurgy; UNS N06625; UNS N08367B 834 95 (2009)3SUPPLEMENTARY REQUIREMENTSThe following supplementary requirements shall be applied when specified by the purchaser in theinquiry, contract, or order.S1. Corrosion TestsS1.1 UNS N06625 shall be tested in accordance with

47、 TestMethods G28 and UNS N08367 in accordance with TestMethods G48. Acceptance criteria shall be a matter of agree-ment between the manufacturer and purchaser.ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this stand

48、ard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be review

49、ed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International