ASTM D6834 - 02(2008) Standard Test Method for Determining Product Leakage from a Package with a Mechanical Pump Dispenser (Withdrawn 2017).pdf

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1、Designation: D6834 02 (Reapproved 2008)Standard Test Method forDetermining Product Leakage from a Package with aMechanical Pump Dispenser1This standard is issued under the fixed designation D6834; the number immediately following the designation indicates the year oforiginal adoption or, in the case

2、 of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method covers the evaluation of the ability ofa pump dispenser to seal when the pa

3、ckaging is held undervacuum. Furthermore, it evaluates the seal between the pumpdispenser and the neck container/closure integrity.1.2 The values stated in SI units are to be regarded asstandard. The values given in parentheses are mathematicalconversions to inch-pound units that are provided for in

4、forma-tion only and are not considered standard.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of reg

5、ulatory limitations prior to use.See 4.3 for a specific warning statement.2. Referenced Documents2.1 ASTM Standards:2D999 Test Methods for Vibration Testing of Shipping Con-tainersD3198 Test Method for Application and Removal Torque ofThreaded or Lug-Style Closures (Withdrawn 2016)33. Significance a

6、nd Use3.1 This test method is suitable for establishing specifica-tions of product leakage for both the pump dispenser and thefinal package. The test is performed at two levels of vacuum, alow and a high level, in order to avoid going directly fromatmospheric pressure to 200 mbar, which can sometime

7、s causepump components that had not been fully seated, to seat.3.1.1 Method A, Product Leakage Test without VibrationTesting of a Mechanical Pump Dispenser Package, is usedwhen a pre-conditioning of the package in a simulated shippingsituation is not desired.3.1.2 Method B, Product Leakage Test with

8、 Vibration Test-ing of a Mechanical Pump Dispenser Package, is used when apre-conditioning of the package in a simulated shippingsituation is desired. The dynamics and stresses of shipping cancreate conditions where the package may be more likely toleak.4. Apparatus4.1 Vacuum Chamber, with a minimum

9、 capacity of 200mbar (147 mm Hg).4.2 Absorbent Paper.NOTE 1Alcoholsensitive paper may be useful in verifying the pointsof leakage for alcohol based products since it is permanently stained withalcohol upon contact.4.3 WarningAppropriate handling consideration shouldbe given to flammable, toxic, caus

10、tic, or other potentiallyhazardous materials used in this determination.5. Sampling5.1 Select an appropriate number of dry, unused pumpdispensers at random for the precision and accuracy desired. Anumber of ten or more samples is recommended, but aminimum of three is acceptable.6. Conditioning6.1 If

11、 possible, condition the test specimen at 23 6 3C (736 5.4F) for not less than 4 h. If the test specimens are notconditioned at the recommended temperature, this should benoted in the test report discussed in 9.1.7. Test Specimen and Sample7.1 For each test specimen select a container to which thepu

12、mp dispenser will be attached during the test. The actualbottle for final package is recommended for testing.1This test method is under the jurisdiction ofASTM Committee F02 on FlexibleBarrier Packaging and is the direct responsibility of Subcommittee F02.40 onPackage Integrity.Current edition appro

13、ved Oct. 1, 2008. Published November 2008. Originallyapproved in 2002. Last previous edition approved in 2002 as D6834 02. DOI:10.1520/D6834-02R08.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandard

14、s volume information, refer to the standards Document Summary page onthe ASTM website.3The last approved version of this historical standard is referenced onwww.astm.org.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United StatesNOTICE: This stan

15、dard has either been superseded and replaced by a new version or withdrawn.Contact ASTM International (www.astm.org) for the latest information18. ProceduresMETHOD APRODUCT LEAKAGE TEST WITHOUTVIBRATION TESTING OF A MECHANICAL PUMPDISPENSER PACKAGE8.1 Fill each container with the liquid to be tested

16、 at theactual level of the final package target weight.8.2 Attach the pump dispenser securely to the container. Formechanical pump dispenser packages using a threaded orlug-style closure, follow Test Method D3198 for the propermethod of closure application. Take care not to actuate thepump dispenser

17、 during this step.8.3 Line the vacuum chamber shelves with the absorbentpaper. The paper should be absent of stains so that it is easierto identify any leakage during the test.8.4 Lay one or more containers on their side in the vacuumchamber.NOTE 2Packages should be oriented such that possible leaka

18、ge pointsare visible when the vacuum chamber door is closed.8.5 With the door of the vacuum chamber closed, start thepump and bring the vacuum level to a maximum of 850 mbar(absolute pressure, equal to 163 mbar).8.5.1 Hold this level of vacuum for a minimum of 3 min andobserve for signs of leakage.

19、If leakage is observed, stop thetest, and identify the leakage points and report findings inSection 9.8.5.2 If no leakage has occurred, increase the level ofvacuum to 200 mbar (absolute pressure, equal to 813 mbar).8.5.3 Hold this level of vacuum for a minimum of 3 min andobserve for signs of leakag

20、e. If leakage is observed, stop thetest, and identify the leakage points and report findings inSection 9.8.6 If leakage occurs, carefully disassemble the pump unitsfrom the container and identify possible causes for the leakage(for example: damaged seal surface, poorly molded neck-finishon the conta

21、iner, and so forth.). Report findings in Section 9.METHOD BPRODUCT LEAKAGE TEST WITHVIBRATION TESTING OF A MECHANICAL PUMPDISPENSER PACKAGE8.7 Fill each container with the liquid to be tested at theactual level of the final package target weight.8.8 Attach the pump dispenser securely to the containe

22、r. Formechanical pump dispenser packages using a threaded orlug-style closure, follow Test Methods D3198 for the propermethod of closure application. Take care not to actuate thepump dispenser during this step.8.9 Place the filled containers in an appropriate carton sothat they will remain firmly in

23、 place during vibration.8.10 Proceed as directed according to Method D999 for 20min each on bottom, top, and one side.8.11 Remove the specimens from the carton. Examine allspecimens for visible leakage without removing or disturbingthe closure. Report the location of any leakage in Section 9.8.12 Li

24、ne the vacuum chamber shelves with the absorbentpaper. The paper should be absent of stains so that it is easierto identify any leakage.8.13 Lay one or more containers on their side in the vacuumchamber.NOTE 3Packages should be oriented such that possible leakage pointsare visible when the vacuum ch

25、amber door is closed.8.14 Packages should be oriented such that possible leakagepoints are visible when the vacuum chamber door is closed.8.15 With the door of the vacuum chamber closed, start thepump and bring the vacuum level to a maximum of 850 mbar(absolute pressure).8.15.1 Hold this level of va

26、cuum for a minimum of 3 minand observe for signs of leakage. If leakage is observed, stopthe test, and identify the leakage points and report findings inSection 9.8.15.2 If no leakage has occurred, increase the level ofvacuum to 200 mbar (absolute pressure).8.15.3 Hold this level of vacuum for a min

27、imum of 3 minand observe for signs of leakage. If leakage is observed, stopthe test, and identify the leakage points and report findings inSection 9.8.16 If leakage occurs, carefully disassemble the pumpcomponents from the container and identify possible causes forthe leakage (for example: damaged s

28、eal surface, poorly moldedneck-finish on the container, and so forth.). Report findings inSection 9.9. Report9.1 Report the following information:9.1.1 Product description, container and type and model ofthe pump dispenser being tested,9.1.2 Number of defective packages,9.1.3 Number of packages,9.1.

29、4 Leakage location on each package,9.1.5 Reason or possible reason for the leakage to occur foreach location cited, and9.1.6 The method followed, A or B.10. Precision and Bias10.1 No statement is made about either the precision or biasof these methods since results merely state whether or not therei

30、s conformance to the criteria specified in the procedure.11. Keywords11.1 container leakage; mechanical pump dispenser leak-age; vacuum leakage testD6834 02 (2008)2ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this

31、standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be r

32、eviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of therespon

33、sible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West

34、 Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 02 (2008)3