KS H ISO 10504-2008 Starch derivatives-Determination of the composition of glucose syrups fructose syrups and hydrogenated glucose syrups-Method using high-performance liquid chrom.pdf

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1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS H ISO 10504 , KS H ISO 10504:2008 2008 11 7 http:/www.kats.go.krKS H ISO 10504:2008 : ( ) ( ) KT&G ( ) : (http:/www.standard.go.kr) ： ：2003 11 28 ：2008 11 7 2008-0741 ： ： ( 025097266) (http:/www.kats.go.kr). 10 5 , . KS H ISO 10504:2008 , Starch derivativ

2、es Determination of the composition of glucose syrups, fructose syrups and hydrogenated glucose syrupsMethod using high-performance liquid chromatography 1998 1 ISO 10504, Starch derivatives Determination of the composition of glucose syrups, fructose syrups and hydrogenated glucose syrups Method us

3、ing high-performance liquid chromatography , . ISO 10504 ISO/TC 93 . A . 1 , , , , , (HPLC) . , , , , , , . . 2 . . ( ) . KS H ISO 5381, KS M ISO 3696, 3 . . . KS H ISO 10504:2008 2 4 . 4.1 KS M ISO 3696 1 2 . . 0.22 m . . 70 . . 4.2 10 %( ) . 1. . 4.3 . . (5.5) . a) 1) , 4 % (polystyrene divinylben

4、zene), H 2) 200 400 b) 1) , 3 4 % , 2) 200 400 . Bio Rad1) . 5 1) ISO . . KS H ISO 10504:2008 3 5.1 . 0.5 95 5.2 20 L . 5.3 . 5.4 . 9 m 25 m 6 % 8 % (cross-linked sulfonated polystyrene divinylbenzene) . . 5.5 2 . Bio Rad1) 125 0118 . 5.6 (membrane disc filter) . 0.45 m . 0.45 m . 0.22 m . 6 6.1 . 6

5、 % . KS H ISO 10504:2008 4 . 6.2 , (5.5)( ) . . ( , ) . . 0.1 mL , . . . 0.5 mL/min . . (attenuation) . 6.3 6.3.1 KS H ISO 5381 ( A ). (tri-itol) . 6.3.2 (4.2 ) . 3 0.1 % . . . . 6.3.3 . (4.2 ) . A . 6.3.4 2 . , . 6.3.5 . 2 0.2 % . x rx . xxxamr = mx ： x ax ： x 1 . 2 % , . KS H ISO 10504:2008 5 6.4

6、6.4.1 0.45 m . (6.4.2 6.4.3 ). 6.4.2 . . . 6.4.3 25 % 30 % 15 mL 20 mL 1.0 g 1.5 g . 15 . 0.45 m . 5.6 . 6.5 6.3.4 . 2 . . 7 x . cx rxax cx ： x rx ： (6.3.5 ) ax ： x . . . 8 8.1 2 1 (g/100 g) 5 % . KS H ISO 10504:2008 6 1 g/100 g , r g/100 g 95 0.90 0.17 45 1.4 0.70 80 0.36 48 0.39 42 0.43 0.23 9 0.2

7、2 0.55 98 0.81 75 0.19 0.12 8.2 2 2 (g/100 g) 5 % . 2 g/100 g , R g/100 g 95 1.70 0.55 45 4.0 1.20 80 3.50 48 2.10 42 1.0 0.98 9 0.57 1.40 98 1.70 75 0.87 0.21 KS H ISO 10504:2008 7 A ( ) A.1 ： % 99.0 0.5 0.0 0.5 0.2 99.0 0.5 0.3 0.0 0.0 95.0 5.0 4.0 4.0 4.0 88.0 A.2 4.5 g dma 4.455 0 0.022 5 0.000

8、0 0.022 5 2.5 g dma 0.005 0 2.475 0 0.012 5 0.007 5 0.3 g dma 0.000 0 0.000 0 0.285 0 0.015 0 2.6 g dma 0.104 0 0.104 0 0.104 0 2.288 0 9.9 g dma 4.564 2.601 5 0.401 5 2.333 0 % 46.10 26.28 4.06 23.57 adm , 135513 7017 (02)60094114 (02)600948878 http:/ KS H ISO 10504:2008 KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS Starch derivativesDetermination of the composition of glucose syrups, fructose syrups and hydrogenated glucose syrupsMethod using high- performance liquid chromatography ICS 67.180.20 Korean Agency for Technology and Standards http:/www.kats.go.kr