GOST 32391-2013 Engine oils Test method for determination of volatility by capillary gas chromatography《发动机油 使用毛细管气相色谱法测定挥发性的试验方法》.pdf

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1、 , () INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ISC) 32391 2013 2014 323912013 II , - - 1.092 . 1.22009 . , . , , , 1 - ( ) - , 4 2 3 , ( 5 2013 . 61-) : ( 3166) 00497 ( 3166) 00497 - - AM - BY - KG MD - RU TJ UZ 4 ASTM D 641709 Standard test method for estima-tion of engi

2、ne oil volatility by capillary gas chromatography ( ). ASTM D02 - D02.04.0H - . (en). - 1.52001 ( 3.6). ASTM, - , , , - . . (IDT) 5 22 - 2013. 692- 323912013 1 2015 . 6 323912013 III - , . () - - . , . , 2014 -, - 323912013 _ 1 Engine oils. Test method for determination of volatility by capillary ga

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4、graphy ( - ) ASTM D 4626 Standard practice for calculation of gas chromatographic response factors (- ) ASTM D 5800 Standard test method for evaporation loss of lubricating oils by the Noack method ( ) 1) ASTM ASTM website, www.astm.org ASTM serviceastm.org, ASTM (Website standards Document Summary)

5、. 323912013 2 ASTM E 355 Standard practice for gas chromatography terms and relationships ( ) ASTM E 594 Standard practice for testing flame ionization detectors used in gas or supercritical fluid chromatography ( - , - ) ASTM E 1510 Standard practice for installing fused silica open tubular capilla

6、ry columns in gas chromatographs ( ) 2.2 CEC L-4093 Evaporation loss of lubricating oils (Noack evaporative tester) ( ).2) 3 , 3.1 , ASTM 355, ASTM 594 ASTM 1510, : 3.2.1 (area slice): , . (. 6.5.2) , , - . 3.2.2 c (corrected area slice): , - , - . 3.2.3 c (cumulative corrected area): - , (RT) (, ).

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8、. 323912013 3 (FID). , - (RT) . 4.4 (RT) - (C8C60) . 371 (700 F) , , -. - , 371 , ( ), 371 . 5 5.1 371 (700 F) . 5.2 ASTM D 5800 (CEC L-4093). , , , - ASTM D 5800. ( ), . . 5.3 , - , , ASTM D 2887. 6 6.1 . 6.1.1 , - (, 35 50 ) 400 . 6.1.2 400 20 /. - 0,1 (6 ) (. 7.6). 6.1.3 - ASTM E 594. 6.1.3.1 400 . 6.1.3.2 0,005 / . 6.1.3.3 1 10-11 /. 6.1.3.4 106. 6.1.3.5 , - . ASTM E 1510. 6.1.4 , , - 7.6. . 6.2 0,1 10 23. 6.2.1 . 6.3 0,53 , .