DIN EN 13075-2-2017 Bitumen and bituminous binders - Determination of breaking behaviour - Part 2 Determination of fines mixing time of cationic bituminous emulsions German version.pdf

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1、February 2017 English price group 9No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 75.140; 91.100.50!%ann“2627575ww

2、w.din.deDIN EN 13075-2Bitumen and bituminous binders Determination of breaking behaviour Part 2: Determination of fines mixing time of cationic bituminous emulsions;English version EN 130752:2016,English translation of DIN EN 13075-2:2017-02Bitumen und bitumenhaltige Bindemittel Bestimmung des Brech

3、verhaltens Teil 2: Bestimmung der Mischzeit von Feinanteilen in kationischen Bitumenemulsionen;Englische Fassung EN 130752:2016,Englische bersetzung von DIN EN 13075-2:2017-02Bitumes et liants bitumineux Dtermination du comportement la rupture Partie 2: Dtermination de la dure de miscibilit des fine

4、s dans les mulsions cationiques de bitume;Version anglaise EN 130752:2016,Traduction anglaise de DIN EN 13075-2:2017-02SupersedesDIN EN 130752:200907www.beuth.deDTranslation by DIN-Sprachendienst.In case of doubt, the German-language original shall be considered authoritative.Document comprises 13 p

5、ages 02.17 2 A comma is used as the decimal marker. National foreword This document (EN 13075-2:2016) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders” (Secretariat: AFNOR, France). The responsible German bodies involved in its preparation were DIN-Normenausschuss Materialprfu

6、ng (DIN Standards Committee Materials Testing) and DIN-Normenausschuss Bauwesen (DIN Standards Committee Building and Civil Engineering), Joint Committee NA 062-03-32 GA Bitumen; Prfverfahren und Anforderungen fr die Bindemittel. Amendments This standard differs from DIN EN 13075-2:2009-07 as follow

7、s: a) there are now three reference fillers - Forshammer, Sikaisol and Caolin Q92; the document has been amended in this regard and the characteristics of other fillers have been included; b) indications concerning precision have been deleted as a European interlaboratory test has not been conducted

8、. Previous editions DIN EN 13075-2: 2002-10, 2009-07 DIN EN 13075-2 Corrigendum 1: 2007-09 DIN EN 13075-2:2017-02EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 13075-2 November 2016 ICS 75.140; 91.100.50 Supersedes EN 13075-2:2009English Version Bitumen and bituminous binders - Determination o

9、f breaking behaviour - Part 2: Determination of fines mixing time of cationic bituminous emulsions Bitumes et liants bitumineux - Dtermination du comportement la rupture - Partie 2 : Dtermination de la dure de miscibilit des fines dans les mulsions cationiques de bitume Bitumen und bitumenhaltige Bi

10、ndemittel - Bestimmung des Brechverhaltens - Teil 2: Bestimmung der Mischzeit von Feinanteilen in kationischen Bitumenemulsionen This European Standard was approved by CEN on 27 August 2016. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for

11、giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three

12、official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodie

13、s of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spa

14、in, Sweden, Switzerland, Turkey andUnited Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2016 CEN All rights of exploitation in any form and by any means reserved worldwide

15、 for CEN national Members. Ref. No. EN 13075-2:2016 EEN 13075-2:2016 (E) 2 Contents Page European foreword . 3 1 Scope 4 2 Normative references 4 3 Terms and definitions . 4 4 Principle . 4 5 Reagents and materials . 4 6 Apparatus . 5 7 Sampling . 5 8 Procedure. 5 9 Expression of results 6 10 Precis

16、ion . 6 11 Test report . 6 Annex A (normative) Characteristics of the reference fillers 7 A.1 Characteristics of the Forshammer filler . 7 A.2 Characteristics of the Sikaisol filler 8 A.3 Characteristics of the Caolin Q92 filler 9 Bibliography . 11 DIN EN 13075-2:2017-02 EN 13075-2:2016 (E) 3 Europe

17、an foreword This document (EN 13075-2:2016) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at t

18、he latest by May 2017, and conflicting national standards shall be withdrawn at the latest by May 2017. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN shall not be held responsible for identifying any or all such patent right

19、s. This document supersedes EN 13075-2:2009. In comparison with EN 13075-2:2009, the following significant changes have been made: Clause 5: three reference fillers (Forshammer, Sikaisol and Caolin Q92) may be used; Subclause 6.10 is discarded since this clause is not referenced in the test procedur

20、e (Clause 8) and since requirements on temperature control are already stated in 6. 1 (oven) and 6.7 (temperature bath or climatic chamber); Subclause 6.2 and Clause 8: the conical shaped funnel is no longer required as filler is to be directly added via a spoon from a simple ad hoc container. Claus

21、e 6.2 now defines the different containers needed by the test procedure. Clause 8 is modified accordingly; Clause 10: since no supporting evidence for the values previously stated in the 2009 version could be found, repeatability and reproducibility figures are withdrawn; Annex A: more complete (e.g

22、. particle size distribution envelopes) and more homogeneous description of the three reference fillers. EN 13075 consists of the following parts under the general title “Bitumen and bituminous binders - Determination of breaking behaviour”: Part 1: Determination of breaking value of cationic bitumi

23、nous emulsions, mineral filler method Part 2: Determination of fines mixing time of cationic bituminous emulsions According to the CEN-CENELEC Internal Regulations, the national standards organisations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgar

24、ia, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turk

25、ey and the United Kingdom. DIN EN 13075-2:2017-02 EN 13075-2:2016 (E) 4 1 Scope This European Standard specifies a method for the determination of the fines mixing time of diluted cationic bituminous emulsions, under standardized conditions. WARNING The use of this European Standard can involve haza

26、rdous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of reg

27、ulatory limitations prior to use. 2 Normative references The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the refere

28、nced document (including any amendments) applies. EN 58, Bitumen and bituminous binders - Sampling bituminous binders EN 12594, Bitumen and bituminous binders - Preparation of test samples EN ISO 3696, Water for analytical laboratory use - Specification and test methods (ISO 3696) 3 Terms and defini

29、tions For the purposes of this document, the following term and definition applies. 3.1 fines mixing time time in seconds for the mixability of a mixture of mineral filler and bitumen emulsion without noticeable breaking effect under the conditions specified in this European Standard 4 Principle A s

30、pecified quantity of filler is added at a uniform rate, with stirring, to a specified quantity of bitumen emulsion diluted with water. Stirring is continued until the mixture becomes pasty and forms lumps that do not adhere to the walls of the pan. This, combined with a noticeable increase in stirri

31、ng power indicates the end of mixability. The time to reach this point (breaking status) is the fines mixing time. 5 Reagents and materials Use only reagents of recognized analytical grade and water conforming to grade 3 of EN ISO 3696. 5.1 Reference fillers. The Forshammer filler1), the Sikaisol fi

32、ller1)or the Caolin Q92 filler1)shall be used as reference fillers.The characteristics of these fillers are given in Annex A. In the event of dispute, the same filler shall be used by the testing laboratories. 5.2 Cleaning agents, as used conventionally in laboratories. 1) This information is given

33、for the convenience of users of this European Standard and does not constitute an endorsement by CEN of the product named. Equivalent products may be used if they can be shown to lead to the same results, or if a correlation between the products has been established. DIN EN 13075-2:2017-02 EN 13075-

34、2:2016 (E) 5 6 Apparatus Usual laboratory apparatus and glassware, together with the following. 6.1 Oven, capable of maintaining a temperature of (110 5) C. 6.2 Containers of appropriate capacity for storing and holding the quantities of filler required in Clause 8. 6.3 Spatula, nickel or stainless

35、steel, 20 cm long. 6.4 Spatula, spoon shaped for adding filler. 6.5 Stop watch, with an accuracy of 0,2 s or better over a time interval of 500 s. 6.6 Bottles, of approximate capacity 500 ml made of a material that will not react with the emulsion, having tight fitting lids, for storing emulsion sam

36、ples and water. 6.7 Constant temperature bath and/or climatic chamber, capable of maintaining a temperature of (25 1) C. If the bath is used to condition the emulsion sample bottles, it should be equipped with a frame or device to prevent the bottles from moving in the water bath. 6.8 Balance, capab

37、le of weighing up to 1 000 g with an accuracy of 0,1 g or better. 6.9 Enamelled or stainless steel dish, of suitable volume, capable of containing 150 g of diluted emulsion and 150 g of filler. 7 Sampling The test material shall be sampled in accordance with EN 58 and shall be prepared in accordance

38、 with EN 12594. 8 Procedure Carry out the procedure under normal laboratory conditions (18 C to 28 C). Dry the quantities of filler, required for the test, in the oven (6.1) at a temperature of (110 5) C until constant mass is reached and let it cool to ambient temperature in a desiccator. Pour a po

39、rtion of emulsion (250 10) g and water (150 10) g into separate bottles (6.6) and secure the lid. Place the required quantity of filler in a closed container (6.2). Place the bottles with the emulsion and the water and the container with the filler in the constant temperature bath or climatic chambe

40、r (6.7) for a minimum of 1,5 h. Transfer (100,0 0,5) g of the emulsion in the dish (6.9) then add (50,0 0,5) g of water while agitating with the spatula (6.3). Transfer (150 1) g of filler in a second container (6.2). Start the stop watch (6.5), and while mixing with the spatula (6.3) at constant ra

41、te of 1 r/s, add filler with the spoon shaped spatula (6.4) from the container (6.2) to the diluted emulsion, by portions of 10 g per 5 s, so that within the 75 s, the overall (150 1) g filler is poured. NOTE To control the portion of filler, the container could be placed on the balance. Continue mi

42、xing and measure the time until the emulsion breaks (see Clause 4). DIN EN 13075-2:2017-02 EN 13075-2:2016 (E) 6 If the bitumen emulsion does not break within 300 s, the test procedure shall be stopped, and the result of the test “ 300 s” shall be reported. It may happen that lumps form as soon as t

43、he filler contacts the diluted emulsion, but the body of the emulsion neither breaks nor reaches the “pasty” stage within 300 s. In such cases, the emulsion is deemed to have not broken. The test procedure shall be stopped and the result of the test “ 300 s formation of lumps” shall be reported. Rep

44、eat the test with a new test portion taken from the same laboratory sample using clean apparatus. 9 Expression of results Express the individual mixing time values (in seconds) to the nearest integer. Express the result as the arithmetic mean of the two individual results of mixing time, to the near

45、est integer. 10 Precision A European round robin test has not been carried out. 11 Test report The test report shall contain at least the following information: a) type and complete identification of the sample under test; b) reference to this European Standard; c) reference to the used filler; d) r

46、esult of the test and individual mixing time values (see Clause 8 and Clause 9); e) any deviation, by agreement or otherwise, from the procedure described; f) date of the test. DIN EN 13075-2:2017-02 EN 13075-2:2016 (E)7 Annex A (normative) Characteristics of the reference fillers A.1 Characteristic

47、s of the Forshammer filler The Forshammer filler is a mixture of: 65 % Feldspath 30 % Quartz 5 % Mica It has following compositional properties (X-ray fluorescence): SiO2: from 74,3 % to 76,8 % Al2O3: from 14,1 % to 14,8 % K2O: from 3,6 % to 4,7 % Na2O: from 4,2 % to 5,2 % The particle size distribu

48、tion envelope, according to EN 933-10 1, is shown in Figure A.1 and defined by: 89 % to 93 % passing the 0,500 mm sieve; 55 % to 59 % passing the 0,250 mm sieve; 22 % to 26 % passing the 0,125 mm sieve; 6 % to 10 % passing the 0,063 mm sieve; 2 % to 6 % passing the 0,032 mm sieve. DIN EN 13075-2:201

49、7-02EN 13075-2:2016 (E) 8 Key X sieves, in m Y % passing, in weight Figure A.1 Gradation of the Forshammer filler A.2 Characteristics of the Sikaisol filler The Sikaisol filler has the following properties: natural fine silica, uncrushed; SiO2content greater than 98 %; density of (2650 20) kg/m3; The particle size distribution envelope is shown in Figure A.2 and defined by: 94 % to 100 % passing th