BS 5551-2 2-1984 Fertilizers - Sampling - Presentation of sampling reports《肥料 第2部分 取样 第2节 取样报告表述方法》.pdf

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1、BRITISH STANDARD BS 5551-2.2: 1984 ISO 5306:1983 Fertilizers Part 2: Sampling Section 2.2 Presentation of sampling reports ISO title: Fertilizers Presentation of sampling reports UDC 631.8:543.05:620.113:001.818BS5551-2.2:1984 This British Standard, having been prepared under the directionof the Che

2、micals Standards Committee, was published under the authority ofthe Board of BSI and comes intoeffect on 31 August 1984 BSI 10-1999 The following BSI references relate to the work on this standard: Committee reference CIC/37 Draft for comment 82/52646 DC ISBN 0 580 13954 9 Committees responsible for

3、 this British Standard The preparation of this British Standard was entrusted by the Chemicals Standards Committee (CIC/-) to Technical Committee CIC/37 upon which the following bodies were represented: Association of Public Analysts British Agrochemicals Association Department of Trade and Industry

4、 (Laboratory of the Government Chemist) Fertiliser Manufacturers Association Ltd. Institute of Trading Standards Administration Ministry of Agriculture, Fisheries and Food Amendments issued since publication Amd. No. Date of issue CommentsBS5551-2.2:1984 BSI 10-1999 i Contents Page Committees respon

5、sible inside front cover National foreword ii 0 Introduction 1 1 Scope and field of application 1 2 Essential information 1 3 Additional information 1 Annex A Typical sampling report 2 Publications referred to Inside back coverBS5551-2.2:1984 ii BSI 10-1999 National foreword This British Standard ha

6、s been prepared under the direction of the Chemicals Standards Committee in order to standardize terminology and labelling, sampling and methods of physical and chemical testing for fertilizers. For some years the United Kingdom has participated in the standardization of methods of sampling fertiliz

7、ers through Subcommittee2, Sampling, of Technical Committee134, Fertilizers and soil conditioners, of the International Organization for Standardization (ISO). As international agreement is reached on the methods, it is proposed to publish them as Sections of BS5551. The standard is to be published

8、in four Parts, each Part being subdivided into Sections and, where appropriate, Subsections. The four Parts are: Part 1: Terminology and labelling; Part 2: Sampling; Part 3: Physical properties; Part 4: Chemical analysis. This Section of Part2 is identical with ISO5306:1983 “Fertilizers Presentation

9、 of sampling reports”. Terminology and conventions. The text of the International Standard has been approved as suitable for publication as a British Standard without deviation. Some terminology and certain conventions are not identical with those used in British Standards; attention is drawn especi

10、ally to the following. Wherever the words “International Standard” appear, referring to this standard, they should be read as “British Standard”. A British Standard does not purport to include all the necessary provisions of a contract. Users of British Standards are responsible for their correct ap

11、plication. Compliance with a British Standard does not of itself confer immunity from legal obligations. Summary of pages This document comprises a front cover, an inside front cover, pages i and ii, pages1 to 8, an inside back cover and a back cover. This standard has been updated (see copyright da

12、te) and may have had amendments incorporated. This will be indicated in the amendment table on the inside front cover.BS5551-2.2:1984 BSI 10-1999 1 0 Introduction In many cases, sampling is carried out in accordance with legal requirements, and, in these cases, a legal sampling report has to be comp

13、leted. For all other cases, or for cases where it is considered that insufficient information is provided by the legal sampling report, the information specified in this International Standard should be given. A sampling report should be made out for each sample taken. If the sample is divided into

14、a number of equivalent portions, a copy of the sampling report should accompany each portion. 1 Scope and field of application This International Standard specifies the information to be given in sampling reports for consignments of fertilizers. An example of a typical sampling report is given in th

15、e Annex A. 2 Essential information The following essential information shall always be given in the sampling report. a) The name of the sampler and the department or organization to which he belongs. b) The name, description or designation associated with the fertilizer, and whether it is in bulk or

16、 in packages. c) Any declared information on the composition or the fineness of grind of the fertilizer, and, if available, a copy of any labels attached to the original packages containing the product. d) Any lot or consignment numbers for the complete identification of the lot, and, if possible, t

17、he date of manufacture or delivery. e) The quantity of fertilizer sampled (i.e. the lot in terms of mass and/or the number of packages) and its relation to the total amount present. f) If the fertilizer was in packages, the nature of the packages and the method of sealing. g) The sampling plan adopt

18、ed and the number of increments taken. (If sampling was carried out in accordance with an International Standard or other standard, its reference shall be given.) h) Any relevant observations made during the sampling procedure, including assessment of the condition of the fertilizer. j) The date, ti

19、me and postal address of the place of sampling, including, where appropriate, the name of any vessel or the registration number of any vehicle from which the sample was taken. k) The identification mark or reference number given to the sample by the sampler. m) The method of sealing the sample conta

20、iners, with a description of any seals. n) The names and addresses of the parties to the relevant transaction, for example manufacturer, importer or vendor and purchaser or holder of the sampled fertilizer. p) The destinations of the laboratory samples and information for the analysts. q) The signat

21、ure of the sampler and name and signature of any independent witness or person from whom any of the information given in the report was obtained. 3 Additional information The sampler may, if he so wishes, or shall, if instructed by the client, Annex A any other information not required by clause2. I

22、f the sampler has been so instructed by the client, the latter shall supply a detailed list of the items of additional information required.BS5551-2.2:1984 2 BSI 10-1999 Annex A Typical sampling report A.1 Participants, place and time A.1.1 Name and address of sampler A.1.2 Postal address of place a

23、nd date and time of sampling A.1.3 Name and address of owner of fertilizer A.1.4 Name and address of owners representative present at the time of sampling A.1.5 Name and address of impartial witness or witnesses present at the time of sampling A.2 Inspection of written documents A.2.1 The sampled go

24、ods were supplied with: A.2.2 Designation of the goods by documents A.2.2.1 Reference to catalogue description: A.2.2.2 Patent symbol (trade name): A.2.2.3 Name of producer, seller or importer of the fertilizer A.2.2.4 Is the designation of the goods in accordance with the contract requirements A.2.

25、3 The lot or delivery unit to which the sampled material belongs is further identified by: Delivery note Invoice Other document (designation): No written documents (the following details concerning designation of the goods, nutrient content, extent of the delivery unit or lot, date of delivery, prod

26、uction or import, depend, therefore, upon information supplied by the owner or his representative) Yes NoBS5551-2.2:1984 BSI 10-1999 3 A.2.4 The sampled goods were dispatched by the producer on (date) A.2.5 The lot was delivered on (date) A.2.6 The sampled lot was imported on (date) A.2.7 The size o

27、f the lot or delivery units was: A.2.8 The stated nutrient contents are: at least in accordance with the catalogue description at least in accordance with the producers, content guarantee in accordance with the invoice A.3 Identification (Check of the identify of the sampled goods with that indicate

28、d in the documents) Identity was shown to be A.4 External inspection of goods A.4.1 The goods arrived in the following form Proven Stamp on bags Probable by Date indications on bags Unlikely Original seals on waggon, tank waggon, truck Other (specify) Impossible to check Solid Liquid Loose Solution

29、Packed in Suspension jute sacks Paper bags Plastics bags Other (specify) BS5551-2.2:1984 4 BSI 10-1999 A.4.2 The sampled goods were on the premises of the A.4.3 Completeness of the sampled lot Producer Dealer Other (specify) At the time of loading or unloading fromto in storage loose in piles loose

30、in compartments packed in stacks and was clearly separated not clearly separated from other lots/goods in a silo in a waggon in a ship in a lorry in a container in a tank waggon in a tank other (specify) The lot was complete according to inspection incomplete but comprised . mass, percentage of insp

31、ected lot, number of packages, other (specify) according to visual appearance according to data supplied by the owner or his representative BS5551-2.2:1984 BSI 10-1999 5 A.4.4 The uniformity of the sampled lot was A.4.5 Deterioration or damage to the goods The deteriorated part of the lot included:

32、(Percentage of the total lot, mass, number of packages, etc.) The deteriorated part was probable unlikely for the following reasons: The colour of the goods was uniform not uniform The particle size distribution of the goods was uniform not uniform The packaging material was uniform not uniform and

33、consisted of Jute Paper Plastics The quality of the packaging material was uniform not uniform The colour of the packaging material was uniform not uniform The sealing of the package(s) was(were) uniform not uniform and consisted of a valve closure seam weld The stamp(s) on the package(s) was(were)

34、uniform not uniform The goods appeared to be undamaged The goods appeared to be deteriorated/damaged by Moisture Heat Contamination by foreign matter Damage to the packaging Contamination from the packaging Mixing with adjoining lots Segregation Hardening Other (specify) sampled separately not sampl

35、ed separatelyBS5551-2.2:1984 6 BSI 10-1999 A.5 Sampling A.5.1 Location of sampling Sampling took place A.5.2 Sampling method The number of increments taken was: The number of units tested was: The amount of the bulk sample (sum of the increments) was (approximately): kg, l. from a conveyor belt at a

36、 dropping or transfer point on the conveyor belt from a bucket conveyor at the outlet of a waggon tank waggon/tank silo other (specify) from a truck from a container Material in from a ship sacks bulk other (specify) Sampling took place from the goods in motion goods at rest mechanically, by means o

37、f an automatic sampling device passing the entire sack contents through a rotary sampler other (specify) manually, by means of piercing the sacks with a sampling spear other (specify) BS5551-2.2:1984 BSI 10-1999 7 A.6 Reduction of the bulk sample and obtaining the final samples A.6.1 Reduction of th

38、e bulk sample and division of the reduced sample into final samples took place by means of A.6.2 (Number) final samples were produced A.7 Sampling regulation(s) The inspection of the written documents, the comparison of the identity of the sampled goods with those given in the documents, checking fo

39、r completeness, uniformity and external condition of the sampled lot, obtaining of increments and the number of increments and obtaining the number of final samples, were in accordance with the following regulation(s) A.8 Particular observations or comments: a rotary sample divider a static divider

40、a manually by coning and quartering a For example a riffler. A.6.3 The final samples were given the seal/sign shown opposite: The above data are to the best of our knowledge as accurate and as complete as possible. (Signature of sampler) (Seal)8 blankBS5551-2.2:1984 BSI 10-1999 Publications referred

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