EN 12659-1999 en Lead and Lead Alloys - Lead《铅和铅合金 铅》.pdf

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1、STD=BSI BS EN 12b59-ENGL 1777 IIFI Lb2qbbS 0617214 717 W BRITISH STANDARD Lead and lead alloys - Lead The European Standard EN 126591999 has the status of a British Standard ICs 77.1“.(iO NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGH LAW BS EN 12659: 1999 STD*BSI BS EN LZbSS-tING

2、L 1497 W 3b24bb7 0837235 855 BS EN 126591999 been prepared under the direction of the Engineenng Amd.No. Date Sedor Committee. wac published under the authonty of the Standards Committee and comes into effect on 15 December 1999 O BSI 12-1999 National foreword Comments This British Standard is the E

3、nglish language version of EN 126591999. It supersedes BS 334: 1982 which is withdram. The UK participation in its preparation was entrusted to Technical Committee NFE22, Lead and lead alloys, which has the responsibility to: - aid enquirers to understand the text; - present to the responsible Europ

4、ean committee any enquiries on the - monitor related international and European developments and promulgate interpretation, or proposals for change, and keep the UK interests informed; them in the UK. A lit of organizations represented on this coininittee can be obtained on request to its secret: Cr

5、oss-reerences The British Standarcis which implement international or European publications referred to in thii document may be found in the BSI Standards Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Find facility of the BSI Standards Electron

6、ic Catalogue. A British Standard does not purport to include all the necessary provisions of a contract. Users of British Standards are responsible for their correct application Compliance with a British Standard does not of itself confer immunity from legal obligations. Summary of pages This docume

7、nt comprises a front cover, an inside front cover, the EN title page, pages 2 to 11 and a back cover. The BSI copyright notice displayed in this document indicates when the document was last issued. ISBN O 580 35148 3 STDDBSI BS EN L2b59-ENGL 1977 9 Lb24bb9 OBL72Lb 791 EUROPEAN STANDARD EN 12659 NOR

8、ME EUROPENNE EUROPISCHE NORM September 1999 ICs 77.120.60 English version Lead and lead alloys - Lead Plomb et alliages de plomb - Plomb Blei und Bleilegerungen - Blei This European Standard was approved by CEN on 19 August 1999. CEN members are bound to comply with the CENICENELEC Internal Regulati

9、ons which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any CEN member. This Europ

10、ean Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official versions. CEN members are the natio

11、nal standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland. Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMlTTEE FOR STANDARDIZATION COMITE EUROPEN DE NORMALISATION EUROPISCHES K

12、OMITEE FR NORMUNG Central Secretariat: rue de Stassart, 36 8-1050 Brussels Q 1999 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 12659:1999 E STD-BSI BS EN 12659-ENGL 1999 II 1b24bb9 OBL72Li b28 Page 2 EN 1 2659: 1 999 Contents Fo

13、reword 3 1 2 3 4 4.1 4.2 5 6 6.1 6.2 6.3 7 7.1 7.2 7.3 8 8.1 8.2 8.3 9 9.1 9.2 10 Scope 4 Normative references 4 Terms and definitions 4 Designation 4 Material number . 4 Product 5 Ordering information . 5 Chemical composition . 6 Shape and size . 6 Surface condition . 6 Sampling and analysis 6 Samp

14、ling . 6 Analysis 6 Rounding of the results of analysis . 6 Documentation . 7 General 7 Certificate of analysis 7 Declaration of conformity . 7 Marking and labelling 7 Marking . 7 Requirements . 6 Labelling . 7 Safety 7 Annex A (normative) European numbering system for lead and lead alloys 9 Al Intr

15、oduction 9 A.2 General 9 A.3 Details of the system . 9 A4 Allocation and administration of material numbers . 10 Bibliography 11 O BSI 12-1999 STD.BSI BS EN 32b59-ENGL 1977 3b2LibbS 08372118 5b4 Page 3 EN 12659 999 Foreword This European Standard has been prepared by Technical Committee CENTTC 306 “

16、Lead and lead alloys“, the Secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by March 2000, and conflicting national standards shall be withdrawn at the latest by

17、 March 2000. According to the CENICENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands

18、, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom. Within its programme of work, Technical Committee CENTTC 306 requested CENTTC 306MIG 1 “Lead“ to prepare the following standard : EN 12659, Lead and lead alloys - lead. O BSI 12-1999 STD-BSI BS EN LZb59-ENGL 1999 I Lb24bb7 08L72L

19、9 4TO Page 4 EN 12659:1999 1 Scope This European Standard specifies the designation, chemical composition, sampling and analysis, marking and labelling and other requirements for lead. 2 Normative references This European Standard incorporates, by dated or undated references, provisions from other p

20、ublications. These normative references are cited at the appropriate places in the text and the publications are listed hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply to this European Standard only when incorporated in it by amendment or rev

21、ision. For undated references the latest edition of the publication referred to applies. EN 1 2402, Lead and lead alloys - Methods of sampling for analysis. IS0 1 1 O1 4-1, Safety data sheet for chemical products - Part I , Content and order of sections. NOTE For the chemical analysis, prestandards

22、in preparation by CENITC 306/WG 3, see bibliography. 3 Terms and definitions For the purposes of this European Standard, the following definitions apply: 3.1 cast product of one furnace or crucible melt NOTE All the ingots from the single cast have the same identifying mark 3.2 ingot cast product in

23、tended for remelting and/or processing 3.3 jumbo very large ingot with a mass generally much more than 50 kg 3.4 bundle collection of ingots taken from a single cast and secured if necessary, for the purposes of handling, shipment and storage. 4 Designation 4.1 Material number The material is design

24、ated by number (see table 1). This material number designation is in accordance with the system given in annex A (normative). O BSI 12-1999 STD-BSI BS EN 12b59-ENGL 1777 lb24bb7 0817220 112 II Page 5 EN 12659 999 4.2 Product The product designation for products to this standard shall consist of : -

25、- - material number (see 4.1). The derivation of a product designation is shown in the following example. denomination (Lead ingot or Lead jumbo) ; number of this European Standard (EN 12659) ; EXAMPLE Lead ingot EN 12659 - PB990R Denomination Number of this European Standard Material number 5 Order

26、ing information In order to facilitate the enquiry, order and confirmation of order procedures between the purchaser and the supplier, the purchaser shall state on his enquiry and/his order the following information : a) quantity of product required (mass) ; b) product designation (see 4.2) ; c) nom

27、inal mass of an ingot (in kilograms) and of a jumbo or a bundle (in tonnes). In addition, the purchaser shall also state on the enquiry and the order if any of the following is required : d) colour coding see 9.1 d) ; e) EXAMPLE certificate of analysis (see 8.2), andior declaration of conformity (se

28、e 8.3). Ordering details for 100 t lead ingots conforming to EN 12659, in material number PB990R, nominal ingot mass 50 kg, nominal mass of a bundle 1 t, with colour coding blue : 100 t Lead ingot EN 12659 - PB990R - nominal ingot mass 50 kg - nominal bundle mass 1 t - colour coding blue O BSI 12-1

29、999 STD-BSI BS EN L2b57-ENGL 1999 II Lb29bbS 0817221 059 I Page 6 EN 12659:1999 6 Requirements 6.1 Chemical composition The composition of the lead shall conform to the requirements given in table 1. 6.2 Shape and size The shape and size of ingots and jumbos shall be at the discretion of the supplie

30、r, unless otherwise agreed between the purchaser and the supplier. 6.3 Surface condition The surface condition of the ingots and jumbos shall be such that it does not affect the composition and is not detrimental to the use of the ingots. 7 Sampling and analysis 7.1 Sampling Sampling shall be carrie

31、d out in accordance with EN 12402. 7.2 Analysis When analysis is carried out by the supplier to verify conformity of a cast, the analytical methods used shall be at his discretion. NOTE When optical emission spectrometry is used, the method should conform to ENV 12908. In case of dispute concerning

32、the results of analysis, the relevant methods of analysis of the prENVs in preparation (see bibliography) to be used to control the compositional conformity of a consignment, apply. NOTE Due to the nature of samples prepared, only chemical analyses are feasible. 7.3 Rounding of the results of analys

33、is The values obtained shall be rounded to the same number of decimal places as used to express the specified limit in table 1. The following rules shall be used for rounding a) if the figure immediately after the last figure to be retained is less than 5, the last figure to be retained shall be kep

34、t unchanged ; b) if the figure immediately after the last figure to be retained is equal to or greater than 5, the last figure to be retained shall be increased by one. OBSI 12-1999 Page 7 EN 1 2659:1999 8 Documentation 8.1 General The supplier shall provide with each consignment the following minim

35、um documentation, including a certificate of analysis in accordance with 8.2 and/or, if requested by the purchaser, a declaration of conformity in accordance with 8.3 : a) name and address ; b) material number ; c) mass of supplied product ; d) certificate of analysis (see 8.2). Other information ca

36、n also be included, if agreed between the purchaser and the supplier. 8.2 Certificate of analysis This is a document which certifies the chemical composition of each cast. The chemical composition shall be reported as the average of the results obtained on the samples taken during moulding unless ot

37、herwise agreed between purchaser and supplier. Other information can also be included, if agreed between the purchaser and the supplier. 8.3 Declaration of conformity If a declaration of conformity is required, the content shall be agreed between the purchaser and the supplier. 9 Marking and labelli

38、ng 9.1 Marking Each ingot shall be clearly and permanently marked with the following minimum information : a) name or identification mark of the manufacturer (usually cast into the product) ; b) cast identity. In addition, if agreed between the supplier and the purchaser : c) material number or shor

39、t designation (see table 1) ; d) any additional marking (for example, purchaser, coiour coding). 9.2 Labelling If required, labelling shall be agreed between the purchaser and the supplier 10 Safety Any risks involved in handling and use of lead are detailed in the suppliers safety data sheet. This

40、data sheet shall conform to IS0 1101 4-1. O BSI 12-1999 STD-BSI BS EN 12b59-ENGL 1999 Lb24bbS 0837223 92% 8 O O 0- Page 9 EN 12659:1999 Annex A (normative) European numbering system for lead and lead alloys A. 1 Introduction The numbering system described in this annex is based on annex A to ISO/TR

41、7003 in which a unique number is allocated to a lead material (lead or lead alloy) in order to categorize it. A.2 General This annex establishes a numbering system for identifying lead and lead alloys and the responsibility for the allocation and administration of numbers for individual lead materia

42、ls. The system is applicable to lead materials standardized in European Standards prepared by CEN/TC 306. A.3 Details of the system A.3.1 General The number shall be composed of alphabetic (upper case Latin letters) and numeric (Arabic) characters. The system shall provide only one number for each m

43、aterial. A number assigned to an individual materiai shall not be re-assigned to another material even if the first mentioned material has been withdrawn. A.3.2 Structure of numbers A.3.2.1 Complete number The number shall consist of six characters. A.3.2.2 Position of characters The position of cha

44、racters shall be as follows : 1 2 3 4 5 6 k3.2.2.1 Positions 1 and 2 The characters for the first two positions shall be the letters “PB“ to designate lead material. A.3.2.2.2 Positions 3 to 5 The characters for the third, fourth and fifth positions shall form a number in the range O01 to 999, see t

45、able A. 1. O BSI 12-1999 Page 10 EN 12659:1999 A.3.2.2.3 Position 6 Material group Position 3,4 and 5 (a number in the range) Cable alloys O01 too99 Battery alloys Sb I 3 Oh 100 to 199 Sb3% 200 to 299 Ca 300 to 399 Sn 400 to 499 Miscellaneous (all alloys) 800 to 899 Pure lead 900 to 999 The characte

46、r for the 6th position shall be a letter designating one of the material groups given in table A.l. Position 6 (letter designating material group) K A M R A.3.2.2.4 Examples - PB001K - PB810M A.4 Allocation and administration of material numbers NOTE 1 CENTC 306 is responsible for the allocation and

47、 administration of materia1 numbers. NOTE 2 of numbers have been allocated to the various battery alloys in the case their inclusion is required in the future. At present no lead alloys for battery applications are standardized in European Standards. However, ranges O BSI 12-1999 Page 11 EN 12659:19

48、99 Bibliography ENV 12908, Lead and lead a/loys - Analysis by Optical Emission Spectrometry (013) with spark excitation. ISOTTR 7003, Unified format for the designation of metals. 1) prENV XXX , Lead and lead alloys - Analysis by flame Atomic Absorption Spectrometry (FAAS) or Induction Coupled Plasm

49、a Emission spectrometry (ICP-ES) without separation of the matrix (WI 00306009). prENV XXX , Lead and lead a/oys - Analysis by flame Atomic Absorption Spectrometry FAAS) after separation of the matrix (WI 00306070). prENV XXX (ICP-ES) after separation of the matrix (WlOO306011). 1) 1) , Lead and lead alloys - Analysis by Induction Coupling Plasma Emission Spectrometry prENV XXX ), Lead and lead a/oys - Analysis by flame Atomic Absorption Spectrometry (FAAS) or Induction Coupled Plasma Emission Spectrometry (ICP -ES) after separation of the matrix by co-precipitation