DIN EN ISO 1833-9-2011 Textiles - Quantitative chemical analysis - Part 9 Mixtures of acetate and triacetate fibres (method using benzyl alcohol) (ISO 1833-9 2006) German version E.pdf

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1、January 2011 Translation by DIN-Sprachendienst.English price group 7No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS

2、 59.060.20!$lC“1739632www.din.deDDIN EN ISO 1833-9Textiles Quantitative chemical analysis Part 9: Mixtures of acetate and triacetate fibres (method using benzyl alcohol) (ISO 1833-9:2006)English translation of DIN EN ISO 1833-9:2011-01Textilien Quantitative chemische Analysen Teil 9: Mischungen aus

3、Acetat- und Triacetatfasern (Benzylalkohol-Verfahren)(ISO 1833-9:2006)Englische bersetzung von DIN EN ISO 1833-9:2011-01Textiles Analyse chimique quantitative Partie 9: Mlanges de fibres dactate et de triactate (mthode lalcool benzylique)(ISO 1833-9:2006)Traduction anglaise de DIN EN ISO 1833-9:2011

4、-01www.beuth.deDocument comprises pagesIn case of doubt, the German-language original shall be considered authoritative.1002.11 DIN EN ISO 1833-9:2011-01 A comma is used as the decimal marker. National foreword This standard has been prepared by Technical Committee ISO/TC 38 “Textiles” in collaborat

5、ion with Technical Committee CEN/TC 248 “Textile and textile products” (Secretariat: BSI, United Kingdom). The responsible German body involved in its preparation was the Normenausschuss Materialprfung (Materials Testing Standards Committee), Working Committee NA 062-05-12 AA Textilchemische Prfver-

6、fahren und Fasertrennung. The Introduction of ISO 1833-1 is summarized below as a help to users of this standard: In general, the methods described in the various parts of ISO 1833 are based on the selective solution of an individual component. Once a component is dissolved from a test specimen, the

7、 insoluble residue is weighed and the percentage of the soluble component(s) is calculated from loss in mass. ISO 1833-1 gives information that is common to all of these analytical methods for all fibre mixtures, regardless of their composition. This general information should be used when applying

8、the other parts of the ISO 1833 series; each of these parts contains a more detailed description of a method that is applicable for a specific fibre mixture. If one of these methods is based on a principle other than selective solution, this is expressly stated and described in detail in the respect

9、ive part of the standards series. Fibre mixtures used during processing and, to a lesser extent, in finished textiles may contain fats, waxes or dressings which either occur naturally or are added to facilitate processing. Fibre mixtures may also contain salts and other water-soluble matter. Some or

10、 all of these substances can separate during analysis and be erroneously calculated as soluble fibre components. To avoid this error, non-fibrous matter should be removed before analysis. A method of pre-treatment for removing oils, fats, waxes and water-soluble matter is given in ISO 1833-1:2006, A

11、nnex A. In addition, textiles may contain resins or other matter added to bind the fibres or to confer special properties, such as water repellence or crease resistance. Such matter, including dyestuffs in exceptional cases, may interfere with the action of the reagent on the soluble components and/

12、or may be partially or completely removed by the reagents. This type of added matter can thus also cause errors and should be removed before the sample is analysed. If it is impossible to remove such added matter, the methods are no longer applicable. Dye in dyed fibre is considered to be an integra

13、l part of the fibre and is not removed. Most textile fibres contain water, the amount of which depends on the type of fibre and the relative humidity of the ambient air. These analyses are conducted on the basis of dry mass, and a procedure for determining the dry mass of analytical samples and resi

14、dues is given in ISO 1833-1. The result is thus obtained on the basis of the dry mass of the dry fibres only. 2 DIN EN ISO 1833-9:2011-01 Provisions have been made for recalculating results on the basis of a) permissible deviations agreed upon for moisture content1)b) permissible deviations agreed u

15、pon for humidity, as well as for 1) the fibrous matter separated during pre-treatment, and 2) non-fibrous matter (e.g. dressings, processing oils or sizing assistants) which can be considered as being a commonly used commercial article that is part of the fibre. In some methods, the insoluble compon

16、ents of a mixture may be partially dissolved in the reagent used to dissolve the soluble component(s). Whenever possible, reagents have been chosen that have little or no effect on the insoluble fibres. If a loss in mass is known to occur during the analysis, the result should be corrected; correcti

17、on factors are given for this purpose. These factors have been determined in several laboratories by treating, with the appropriate reagent as specified in the method of analysis, fibres cleaned by pre-treatment. These correction factors apply only to undegraded fibres. If the fibres have been degra

18、ded during processing, different correction factors may be necessary. The methods described in this series apply for single determinations; at least two determinations should be made on separate samples, further determinations can be made where desired. Before the analyses are carried out, all fibre

19、s in the mixture should be identified. For the purposes of confirmation, it is recommended that alternative methods be used in which the component that would have made up the residue when using the standard method is dissolved first, unless this is not technically possible. Where practically possibl

20、e, the components of a mixture are to be manually separated if the method described in ISO 1833-1:2006, Annex B is to be primarily used instead of the chemical analytical methods described in the other parts of ISO 1833. The DIN Standard corresponding to the International Standard referred to in thi

21、s document is as follows: ISO 1833-1 DIN EN ISO 1833-1 1) Commonly used conditioning values shall be used for each fibre, where these are available. 3 DIN EN ISO 1833-9:2011-01 National Annex NA (informative) Bibliography DIN EN ISO 1833-1, Textiles Quantitative chemical analysis Part 1: General pri

22、nciples of testing 4 EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 1833-9 October 2010 ICS 59.060.20 English Version Textiles - Quantitative chemical analysis - Part 9: Mixtures of acetate and triacetate fibres (method using benzyl alcohol) (ISO 1833-9:2006) Textiles - Analyse chimique qu

23、antitative - Partie 9: Mlanges de fibres dactate et de triactate (mthode lalcool benzylique) (ISO 1833-9:2006) Textilien - Quantitative chemische Analysen - Teil 9: Mischungen aus Acetat- und Triacetatfasern (Benzylalkohol-Verfahren) (ISO 1833-9:2006) This European Standard was approved by CEN on 12

24、 September 2010. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may

25、 be obtained on application to the CEN Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CE

26、N Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,

27、Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2010 CEN All rights of exploita

28、tion in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 1833-9:2010: EDIN EN ISO 1833-9:2011-01 EN ISO 1833-9:2010 (E) 2Contents Page Foreword .3 1 Scope.5 2 Normative references.5 3 Principle 5 4 Reagents .5 5 Apparatus5 6 Test Procedure .6 7 Calculation and e

29、xpression of results .6 8 Precision .6 EN ISO 1833 consists of the following parts, under the general title Textiles Quantitative chemical analysis: Part 1: General principles of testing Part 2: Ternary fibre mixtures Part 3: Mixtures of acetate and certain other fibres (method using acetone) Part 4

30、: Mixtures of certain protein and certain other fibres (method using hypochlorite) Part 5: Mixtures of viscose, cupro or modal and cotton fibres (method using sodium zincate) Part 7: Mixtures of polyamide and certain other fibres (method using formic acid) Part 8: Mixtures of acetate and triacetate

31、fibres (method using acetone) Part 9: Mixtures of acetate and triacetate fibres (method using benzyl alcohol) Part 10: Mixtures of triacetate or polylactide and certain other fibres (method using dichloromethane) Part 11: Mixtures of cellulose and polyester fibres (method using sulfuric acid) Part 1

32、2: Mixtures of acrylic, certain modacrylics, certain chlorofibres, certain elastanes and certain other fibres (method using dimethylformamide) Part 13: Mixtures of certain chlorofibres and certain other fibres (method using carbon disulfide/acetone) Foreword The text of ISO 1833-9:2006 has been prep

33、ared by Technical Committee ISO/TC 38 “Textiles” of the International Organization for Standardization (ISO) and has been taken over as EN ISO 1833-9:2010 by Technical Committee CEN/TC 248 “Textiles and textile products”, the secretariat of which is held by BSI. This European Standard shall be given

34、 the status of a national standard, either by publication of an identical text or by endorsement, at the latest by April 2011, and conflicting national standards shall be withdrawn at the latest by April 2011. Attention is drawn to the possibility that some of the elements of this document may be th

35、e subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. Part 14: Mixtures of acetate and certain chlorofibres (method using acetic acid) Part 15: Mixtures of jute and certain animal fibres (method by determining nitrogen content) Pa

36、rt 16: Mixtures of polypropylene fibres and certain other fibres (method using xylene) Part 17: Mixtures of chlorofibres (homopolymers of vinyl chloride) and certain other fibres (method using sulfuric acid) Part 18: Mixtures of silk and wool or hair (method using sulfuric acid) Part 6: Mixtures of

37、viscose or certain types of cupro or modal or lyocell and cotton fibres (method using formic acid and zinc chloride) DIN EN ISO 1833-9:2011-01 EN ISO 1833-9:2010 (E) 3 Part 19: Mixtures of cellulose fibres and asbestos (method by heating) Part 21: Mixtures of chlorofibres, certain modacrylics, certa

38、in elastanes, acetates, triacetates and certain other fibres (method using cyclohexanone) The following parts are under preparation: Part 22: Mixtures of viscose or certain types of cupro or modal or lyocell and flax fibres (method using formic acid and zinc chlorate) Part 23: Mixtures of polyethyle

39、ne and polypropylene (method using cyclohexanone) Part 24: Mixtures of polyester and some other fibres (method using phenol and tetrachloroethane) Part 20: Mixtures of elastane and certain other fibres (method using dimethylacetamide) According to the CEN/CENELEC Internal Regulations, the national s

40、tandards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norwa

41、y, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 1833-9:2006 has been approved by CEN as EN ISO 1833-9:2010 without any modification. DIN EN ISO 1833-9:2011-01 EN ISO 1833-9:2010 (E) 41 Scope This part of ISO 1833

42、 specifies a method, using benzyl alcohol, to determine the percentage of acetate, after removal of non-fibrous matter, in textiles made of binary mixtures of acetate and triacetate fibres. 2 Normative references The following referenced documents are indispensable for the application of this docume

43、nt. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 1833-1, Textiles Quantitative chemical analysis Part 1: General principles of testing 3 Principle The acetate fibre is dissolved out

44、 from a known dry mass of the mixture, with benzyl alcohol. The residue is collected, washed, dried and weighed; its corrected mass is expressed as a percentage of the dry mass of mixture. The percentage of acetate is found by the difference. 4 Reagents Use the reagents described in ISO 1833-1 toget

45、her with those given in 4.1 and 4.2. 4.1 Benzyl alcohol. 4.2 Ethanol. 5 Apparatus Use the apparatus described in ISO 1833-1 together with those given in 5.1, 5.2 and 5.3. 5.1 Conical flask, minimum capacity 200 ml, glass-stoppered. 5.2 Mechanical shaker. 5.3 Heating apparatus, suitable for maintaini

46、ng the temperature of the flask at (52 2) C (for example water bath with thermostat). DIN EN ISO 1833-9:2011-01 EN ISO 1833-9:2010 (E) 56 Test procedure Follow the general procedure given in ISO 1833-1, and then proceed as follows. To the specimen contained in the conical flask, add 100 ml of benzyl

47、 alcohol per gram of specimen. Insert the stopper and shake the flask vigorously on the mechanical shaker so that it plunges into the water bath, kept at a temperature of (52 2) C. Shake the flask for (20 1) min at this temperature. Filter the contents of the flask through the weighed filter crucibl

48、e. Replace the residue in the flask by means of forceps, add to the flask a fresh portion of benzyl alcohol and shake as before at a temperature of (52 2) C for (20 1) min. Filter the contents of the flask through the same weighed filter crucible and repeat the cycle a third time with a third 100 ml portion of benzyl alcohol. Pour the liquid and the residue into the same weighed filter crucible; wash any fibres from the flask into the crucible with an extra quanti