BS EN 12617-2-2005 Products and systems for the protection and repair of concrete structures - Test methods - Shrinkage of crack injection products based on polymer binder volumetr.pdf

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1、BRITISH STANDARDBS EN 12617-2:2004Products and systems for the protection and repair of concrete structures Test methods Part 2: Shrinkage of crack injection products based on polymer binder: volumetric shrinkageThe European Standard EN 12617-2:2004 has the status of a British StandardICS 91.080.40g

2、49g50g3g38g50g51g60g44g49g42g3g58g44g55g43g50g56g55g3g37g54g44g3g51g40g53g48g44g54g54g44g50g49g3g40g59g38g40g51g55g3g36g54g3g51g40g53g48g44g55g55g40g39g3g37g60g3g38g50g51g60g53g44g42g43g55g3g47g36g58BS EN 12617-2:2004This British Standard was published under the authority of the Standards Policy and

3、 Strategy Committee on 9 September 2005 BSI 9 September 2005ISBN 0 580 44409 0National forewordThis British Standard is the official English language version of EN 12617-2:2004.The UK participation in its preparation was entrusted by Technical Committee B/517, Concrete, to Subcommittee B/517/8, Prot

4、ection and repair of concrete structures, which has the responsibility to:A list of organizations represented on this subcommittee can be obtained on request to its secretary.Cross-referencesThe British Standards which implement international or European publications referred to in this document may

5、 be found in the BSI Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue or of British Standards Online.This publication does not purport to include all the necessary provisions of a contract. Users ar

6、e responsible for its correct application.Compliance with a British Standard does not of itself confer immunity from legal obligations. aid enquirers to understand the text; present to the responsible international/European committee any enquiries on the interpretation, or proposals for change, and

7、keep the UK interests informed; monitor related international and European developments and promulgate them in the UK.Summary of pagesThis document comprises a front cover, an inside front cover, the EN title page, pages 2 to 6, an inside back cover and a back cover.The BSI copyright notice displaye

8、d in this document indicates when the document was last issued.Amendments issued since publicationAmd. No. Date CommentsEUROPEAN STANDARDNORME EUROPENNEEUROPISCHE NORMEN 12617-2August 2004ICS 91.080.40English versionProducts and systems for the protection and repair of concretestructures - Test meth

9、ods - Part 2: Shrinkage of crack injectionproducts based on polymer binder: volumetric shrinkageProduits et systmes pour la protection et la rparation desstructures en bton - Mthodes dessai - Partie 2: Retraitdes produits dinjection pour fissures formul avec despolymres : retrait volumtriqueProdukte

10、 und Systeme fr den Schutz und dieInstandsetzung von Betontragwerken - Prfverfahren - Teil2: Schrumpfung von polymeren Rissfllstoffen :Volumetrische SchrumpfungThis European Standard was approved by CEN on 27 February 2004.CEN members are bound to comply with the CEN/CENELEC Internal Regulations whi

11、ch stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Central Secretariat or to any CEN member.This European Standa

12、rd exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the officialversions.CEN members are the national standards

13、 bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France,Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia,Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE F

14、OR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: rue de Stassart, 36 B-1050 Brussels 2004 CEN All rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 12617-2:2004: EEN 12617-2:2004 (E) 2Contents pa

15、geForeword3 1 Scope 4 2 Normative references 4 3 Test principle4 4 General requirements for testing - Apparatus4 5 Test procedure.5 6 Expression of results 5 7 Test report 6 EN 12617-2:2004 (E) 3Foreword This document (EN 12617-2:2004) has been prepared by Technical Committee CEN /TC 104, “Concrete

16、and related products“, the secretariat of which is held by DIN. It has been prepared by Sub-Committee 8 “Products and systems for the protection and repair of concrete structures“ (Secretariat AFNOR). This European Standard shall be given the status of a national standard, either by publication of a

17、n identical text or by endorsement, at the latest by February 2005, and conflicting national standards shall be withdrawn at the latest by February 2005. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this Eur

18、opean Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. EN 12617-2:2

19、004 (E) 41 Scope This document describes a method for determining the volumetric shrinkage of products formulated with thermosetting polymer binders, mainly epoxy and polyester binders, that cure at ambient temperature or below. This method is adapted for crack injection products formulated with pol

20、ymer thermosetting binder. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.

21、 EN ISO 2811-2, Paints and varnishes Determination of density Part 2: Immersed body (plummet) method (ISO 2811-2:1997).3 Test principle The total volumetric shrinkage is calculated as the percentage change in density when the polymer system at (21 2) C cures to the final product also at (21 2) C. Th

22、e density after polymerisation (curing) is measured at (21 0,5) C by measuring the buoyancy of the specimen immersed in silicone oil. 4 General requirements for testing - Apparatus 4.1 balance accurate to 0,001 g, a density measuring device, and suitable wire for suspending the specimen in silicone

23、oil; 4.2 thermometer accurate to 0,2 C and graduated at intervals of 0,2 C or finer; 4.3 silicone oil bath of density Qsiat + (21 0,5) C; 4.4 test tube: diameter 20 mm, length 180 mm in polyethylene or glass treated with a silicone release agent; 4.5 stopwatch; 4.6 desiccator; 4.7 temperature contro

24、lled room or enclosure, capable of maintaining the sample at the recommended constant temperature. EN 12617-2:2004 (E) 55 Test procedure 5.1 Determination of the density of the material before polymerisation Since it is difficult to determine the density of resin systems that react at ambient temper

25、ature owing to their high reactivity and the exothermic heat evolved, determine separately the densities of the components of the resin, at (21 0,5) C to EN ISO 2811-2. Calculate the overall density at time 0, QMO, using the following equation: ()()()ABBABABAMOQmQmQQmmQ+= (1) where QAis the density

26、of component A, in gram per millilitre; QBis the density of component B, in gram per millilitre; mAis the mass of component A used for preparation of a specimen, in gram; mBis the mass of component B used for preparation of a specimen, in gram. 5.2 Determination of the density of polymerized (cured)

27、 material Pour (25 5) g of the resin system as specified in 5.1 into the test tube. After allowing the correct time for polymerisation (curing) at (21 2) C, leave to cool in a desiccator. When cool remove the polymerized specimen from the test tube. Weigh the specimen immediately in air: MFSLthen me

28、asure the apparent mass in silicone oil at (21 0,5) C : M(FS + D)si. and weigh the suspension wire used for weighing: MDL in air. Then remove as much as possible of the silicone oil adhering to the specimen, using filter paper, washing with petroleum ether1). Dry the specimen, for one hour, at (110

29、2) C (for epoxy and polyester binders) and place the specimen in a desiccator to cool to (21 2) C. Weigh again, to establish whether a change in apparent mass has occurred during the measurement with the specimen in silicone oil. The change in weight shall not be greater than 0,2 % of the initial we

30、ight MFSL, otherwise another more suitable immersion liquid shall be chosen. 6 Expression of results 6.1 Calculate the density of the cured material, QFS, rounded to the third decimal, using the following equation: ()siDFSDLFSLsiFSLFS+=MMMQMQ (2) where Qsiis the density of silicone oil, in gram per

31、millilitre; MFSLis the mass of the polymerized (cured) resin in air, in gram; M(FS+D)siis the apparent mass of specimen and suspension wire in silicone oil, in gram; MDLis the mass of the suspension wire in air, in gram. 1) Take appropriate precautions by using organic solvents. This document does n

32、ot purport to address the safety problems associated with their use. EN 12617-2:2004 (E) 66.2 Calculate the total volumetric shrinkage, Svol - tot, during the (polymerisation) curing as a percentage rounded to the first decimal using the following equation: 010FSMOFStotvol=QQQS (3) where QFSis the d

33、ensity of the polymerized (cured) product at (21 0,5) C, in gram per millilitre; QMOis the density of the product at (21 0,5) C before polymerization (curing), in gram per millilitre. 7 Test report The test report shall include the following: a) complete identification of the injection product or sy

34、stem tested, including type, source, manufacturers code numbers and history; b) name and address of the testing laboratory and number of the test report; c) reference to this document; d) proportion by weight of the components constituting the product system; e) date and details of preparation of th

35、e specimen of the test; f) time of polymerization; g) test results: density of the components; calculated density before polymerisation; density of the cured material; (individual values and near value); calculated volumetric shrinkage; h) any deviations from this document or any special conditions.

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