ASTM D1429-2003 Standard Test Methods for Specific Gravity of Water and Brine《水和卤水比重的标准试验方法》.pdf
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1、Designation: D 1429 03Standard Test Methods forSpecific Gravity of Water and Brine1This standard is issued under the fixed designation D 1429; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in p
2、arentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.1. Scope*1.1 These test methods cover the determination of thespecific gravity of water and brine free of separable oil, asfollows:SectionsTest Method APycno
3、meter 7 to 11, 21Test Method BBalance 12 to 16, 21Test Method CErlenmeyer Flask 17 to 21Test Method DHydrometer 22 to 271.2 Test Methods A and B are applicable to clear waters orthose containing only a moderate amount of particulate matter.Test Method B is preferred for samples of sea water or brine
4、sand is more sensitive than Test Method D which has the samegeneral application. Test Method C is intended for samples ofwater containing mud or sludge.1.3 It is the users responsibility to ensure the validity ofthese test methods for waters of untested matrices.1.4 The test method was tested at 22C
5、 over a range, showninTables 1-4, of 1.0252 through 1.2299; all data were correctedto 15.6C (60F).1.5 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health
6、 practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:D 1066 Practice for Sampling Steam2D 1129 Terminology Relating to Water2D 1193 Specification for Reagent Water2D 2777 Practice for Determination of Precision and Bias ofApplic
7、able Methods of Committee D19 on Water2D 3370 Practices for Sampling Water from Closed Con-duits2D 5847 Practice for Writing Quality Control Specificationsfor Standard Test Methods for Water Analysis3E1 Specification for ASTM Thermometers43. Terminology3.1 Definitions:3.1.1 brinewater that contains
8、dissolved matter at anapproximate concentration of more than 30 000 mg/L.3.1.2 For definitions of terms used in these test methods,refer to Terminology D 1129.4. Significance and Use4.1 Specific gravity is an important property of fluids beingrelated to density and viscosity. Knowing the specific gr
9、avitywill allow determination of a fluids characteristics comparedto a standard, usually water, at a specified temperature. Thiswill allow the user to determine if the test fluid will be heavieror lighter than the standard fluid.5. Reagents5.1 Purity of WaterUnless otherwise indicated, referenceto w
10、ater shall be understood to mean reagent water conformingto Specification D 1193, Type I. Other reagent water types maybe used provided it is first ascertained that the water is ofsufficiently high purity to permit its use without adverselyaffecting the precision and bias of the test method. Type II
11、Iwater was specified at the time of round robin testing of thistest method.6. Sampling6.1 Collect the samples in accordance with PracticesD 3370 and Practice D 1066.6.2 In view of the lack of a standard test method forsampling mud or sludge, no instructions are given for samplingthis type of materia
12、l.TEST METHOD APYCNOMETER7. Summary of Test Method7.1 The sample is introduced into a pycnometer, stabilizedat the desired temperature, and weighed. The specific gravity iscalculated from this weight and the previously determinedweight of reagent water that is required to fill the pycnometerat the s
13、ame temperature.1These test methods are under the jurisdiction of ASTM Committee D19 onWater, and are the direct responsibility of Subcommittee D19.05 on InorganicConstituents in Water.Current edition approved Aug. 10, 2003. Published September 2003. Originallyapproved in 1956. Last previous edition
14、 approved in 1999 as D 1429 95 (1999).2Annual Book of ASTM Standards, Vol 11.01.3Annual Book of ASTM Standards, Vol 11.02.4Annual Book of ASTM Standards, Vol 14.03.1*A Summary of Changes section appears at the end of this standard.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, Wes
15、t Conshohocken, PA 19428-2959, United States.8. Apparatus8.1 BathConstant-temperature bath designed to maintaina temperature of 15.6 6 1C (60 6 1.8F). If any othertemperature must be used due to local conditions, appropriatecorrections shall be made.8.2 PycnometerCylindrical or conical glass vessel
16、care-fully ground to receive an accurately fitting 24/12 standardtaper glass stopper provided with a hole approximately 1.0 to2.0 mm in diameter, centrally located in reference to thevertical axis.The top surface of the stopper shall be smooth andsubstantially plane, and the lower surface shall be c
17、oncave inorder to allow all air to escape through the bore. The height ofthe concave section shall be approximately 5 mm at the center.The stoppered pycnometer shall have a capacity of about 24 to30 mL, and shall weigh not more than 40 g. Suitable pycnom-eters are shown in Fig. 1.8.3 ThermometerAnAS
18、TM Gravity Thermometer havinga range from 20 to + 102C or 5 to + 215F, as specified,and conforming to the requirements for Thermometer 12C or12F, respectively, as prescribed in Specification E1.9. Procedure9.1 Weigh a clean, dry, calibrated pycnometer, completewith stopper, on an analytical balance,
19、 and record this weightto the nearest 0.1 mg, as P.9.2 Remove the stopper and fill the pycnometer with re-cently boiled reagent water that has been cooled to roomtemperature, to within several millimetres of the top. Removethe air bubbles. Immerse the unstoppered pycnometer up to theneck in a consta
20、nt-temperature bath maintained at 15.6 6 1C(60 6 1.8F). Allow the pycnometer to remain in the bath fora period of time sufficient to establish temperature equilibrium.Twenty minutes is usually sufficient.9.3 After temperature equilibrium has been established, andbefore removing from the bath, firmly
21、 insert the stopper andremove the excess water from the top of the stopper, takingcare to leave the capillary filled. Remove the stopperedpycnometer from the bath and wipe it dry. Immediately weighthe pycnometer, and record this weight to the nearest 0.1 mg,as W.9.4 Empty the reagent water from the
22、pycnometer and dry,or rinse with the sample to be tested.9.5 Using the sample to be tested, repeat the procedure inaccordance with 9.2 and 9.3, recording the weight of thepycnometer containing the sample under test as S.10. Calculation10.1 Calculate the specific gravity of the sample as follows:Spec
23、ific gravity 5 S2P!/W2P!where:P = weight of the empty pycnometer,FIG. 1 Suitable PycnometersTABLE 1 Determination of Bias, Pycnometer MethodCalculated SpecificGravitySpecific GravityExperimentallyDetermined6 %BiasStatisticallySignificant(95 % ConfidenceLevel)1.0247 1.0262 0.049 yes1.0648 1.0665 + 0.
24、16 yes1.1100 1.1119 + 0.17 yes1.2299 1.2235 0.52 yesTABLE 2 Determination of Bias, Balance MethodCalculated SpecificGravitySpecific GravityExperimentallyDetermined6 %BiasStatisticallySignificant(95 % ConfidenceLevel)1.0247 1.0264 0.166 yes1.0648 1.0657 + 0.084 yes1.1100 1.1126 + 0.234 yes1.2299 1.22
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