SAE AMS 3075F-2000 Compound Corrosion-Preventive Hard Film Hot Application《热敷防腐蚀硬膜化合物》.pdf

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1、_SAE Technical Standards Board Rules providHWKDW7KLVUHSRUWLVSXEOLVKHGE6$(WRDGYDQFHWKHVWDWHRIWHFKQ LFDODQGHQJLQHHULQJVFLHQFHV7KHXVHRIWKLVUHSRUWL sentirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising thereIURPLVWKHVROHUHVSRQVLELOLW

2、RIWKHXVHUSAE reviews each technical report at least every five years at which time it may be revised, reaffirmed, stabilized, or cancelled. SAE invites your written comments and suggestions.Copyright 2016 SAE InternationalAll rights reserved. No part of this publication may be reproduced, stored in

3、a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE.TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada)Tel: +1 724-776-4970 (outside USA)Fax: 724-776-0790Email: Cus

4、tomerServicesae.orgSAE WEB ADDRESS: http:/www.sae.orgSAE values your input. To provide feedbackon this Technical Report, please visithttp:/www.sae.org/technical/standards/AMS3075FAEROSPACEMATERIAL SPECIFICATIONAMS3075REV. FIssued 1943-04Revised 2000-12Reaffirmed 201Superseding AMS3075ECompound, Corr

5、osion-PreventiveHard Film, Hot ApplicationRATIONALEAMS3075F has been reaffirmed to comply with the SAE five-year review policy.1. SCOPE:1.1 Form:This specification covers a stable, nonvolatile, petroleum-base compound in a form suitable for application by dipping at 170 to 210 F (77 to 99 C).1.2 App

6、lication:This compound has been used typically for preservation of metal parts, tools, assemblies, and equipment during shipment and storage where a compound readily removable without component damage is required, but usage is not limited to such applications.1.3 Safety - Hazardous Materials: While

7、the materials, methods, applications, and processes described or referenced in this specification may involve the use of hazardous materials, this specification does not address the hazards which may be involved in such use. It is the sole responsibility of the user to ensure familiarity with the sa

8、fe and proper use of any hazardous materials and to take necessary precautionary measures to ensure the health and safety of all personnel involved.2. APPLICABLE DOCUMENTS:The issue of the following documents in effect on the date of the purchase order form a part of thisspecification to the extent

9、specified herein. The supplier may work to a subsequent revision of adocument unless a specific document issue is specified. When the referenced document has beencanceled and no superseding document has been specified, the last published issue of that documentshall apply.2.1 SAE Publications: Availa

10、ble from SAE, 400 Commonwealth Drive, Warrendale, PA 15096-0001.AMS 3160 Solvent, PetroleumAMS 4037 Aluminum Alloy Sheet and Plate, 4.4Cu - 1.5Mg - 0.60Mn (2024; - T3 Flat Sheet, - T351 Plate), Solution Heat TreatedAMS 5044 Steel Sheet and Strip, 0.15 Carbon, maximum, Half Hard Temper2.2 ASTM Public

11、ations: Available from ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959.ASTM B 117 Operating Salt Spray (Fog) Testing ApparatusASTM D 92 Flash and Fire Points by Cleveland Open CupASTM D 127 Drop Melting Point of Petroleum Wax, Including PetrolatumASTM D 217 Cone Penetration of Lubricat

12、ing GreaseASTM D 1748 Rust Protection by Metal Preservatives in the Humidity Cabinet3. TECHNICAL REQUIREMENTS:3.1 Setting: Compound applied to metal parts shall set to a firm, hard film within 24 hours at 68 to 86 F (20 to 30 C) and, after 120 hours standing, shall not have checked or cracked exposi

13、ng the metal surface underneath.3.1.1 Toxicity: Compound shall not contain materials of known toxicity. The vapor shall not cause discomfort or injury to workmen engaged in application of the compound.3.1.2 Abrasiveness: Compound shall not contain abrasive substances.3.2 Properties: Compound shall c

14、onform to the requirements shown in Table 1 and 3.2.5 through 3.2.14; tests shall be conducted in accordance with specified test methods:TABLE 1 - PropertiesProperty Value Test Method3.2.1 Melting Point 150 to 170 F (66 to 77 C) ASTM D 1273.2.2 Flash Point, minimum 350 F (177 C) ASTM D 923.2.3 Consi

15、stency 30 to 90 ASTM D 2173.2.4 Nonvolatile Matter by weight,minimum 99.0%4.5.1SAE INTERNATIONAL AMS3075F Page 2 of 8_3.2.5 Stability: Compound shall remain homogeneous with age, determined in accordance with 4.5.2.3.2.6 Application and Removability: Compound shall form a continuous, completely prot

16、ective film on metal surfaces under normal conditions of storage in all climates; it shall be readily removed by dipping in, or spraying with, AMS 3160 petroleum solvent or by wiping with cloths saturated with the solvent.3.2.7 Wetting Properties and Low-Temperature Adhesion: Compound shall thorough

17、ly wet the surface of test panels, shall form a smooth, unbroken film and shall show satisfactory adhesion, determined in accordance with 4.5.3.3.2.8 Rosin: Compound shall show no evidence of the presence of rosin, determined in accordance with 4.5.4.3.2.9 Acidity: Compound shall show no evidence of

18、 the presence of inorganic acid, determined in accordance with 4.5.5.3.2.10 Lead Solubility: Compound shall not cause a change in weight of a lead specimen of more than 5 milligrams per square inch (0.78 mg/cm2), determined in accordance with 4.5.6.3.2.11 Loss on Heating: Compound shall lose not mor

19、e than 5% in weight when tested as in 4.5.7.3.2.12 Humidity Protection: Panels coated with the compound in accordance with 4.5.8.1, exposed to humid atmosphere for not less than 28 days, shall meet the requirements of 4.5.8.2.3.2.13 Salt Spray Protection: Panels coated with the compound in accordanc

20、e with 4.5.9.1 and exposed to salt spray in accordance with 4.5.9.2 shall protect metal panels from corrosion and pitting for not less than the times shown in Table 2.3.2.14 Corrosion: Compound shall not corrode polished steel, copper, magnesium, aluminum, or cadmium plate when maintained in contact

21、 with those metals for four hours 0.25 at 210 F 2 (99 C 1).TABLE 2 - Salt Spray Corrosion ParametersPanel MaterialProtection TimeDays, minimumSand blasted steel 7Polished steel 7Polished aluminum 28SAE INTERNATIONAL AMS3075F Page 3 of 8_4. QUALITY ASSURANCE PROVISIONS: 4.1 Responsibility for Inspect

22、ion: The vendor of compound shall supply all samples for vendors tests and shall be responsible for the performance of all required tests. Purchaser reserves the right to sample and to perform any confirmatory testing deemed necessary to ensure that the compound conforms to the requirements of this

23、specification.4.2 Classification of Tests: 4.2.1 Acceptance Tests: Melting point (3.2.1), application and removability (3.2.6), wetting properties and low-temperature adhesion (3.2.7), humidity protection (3.2.12), and salt spray protection (3.2.13) are acceptance tests and shall be performed on eac

24、h lot.4.2.2 Periodic Tests: Flash point (3.2.2), consistency (3.2.3), non-volatile matter (3.2.4), stability (3.2.5), rosin (3.2.8), acidity (3.2.9), lead solubility (3.2.10), and loss on heating (3.2.11) are periodic tests, and shall be performed at a frequency selected by the vendor unless frequen

25、cy of testing is specified by purchaser.4.2.3 Preproduction Tests: All technical requirements are preproduction tests and shall be performed prior to or on the first article shipment of compound to a purchaser, when a change in ingredients and/or processing requires reapproval as in 4.4.2, and when

26、purchaser deems confirmatory testing to be required.4.3 Sampling and Testing: Shall be as follows; a lot shall be all compound produced in a single production run from the same batches of raw materials under the same fixed conditions and presented for vendors inspection at one time.4.3.1 Acceptance

27、Tests: Sufficient compound shall be taken at random from each lot to perform all required tests. The number of determinations for each requirement shall be as specified in the applicable test procedure or, if not specified therein, not less than two.4.3.2 Sample quantities for periodic and preproduc

28、tion tests shall be selected at the discretion of the vendor unless otherwise specified by the purchaser.4.4 Approval: Compound shall be assigned a name or other alphanumeric code identification traceable to a specific set of ingredients and raw materials, manufacturing processes and sequences, cont

29、rols and inspection procedures. In the event of any change in ingredients, raw material, manufacturing processes, manufacturing sequences, manufacturing controls or inspection procedures, that name or other coded identification shall also be changed.SAE INTERNATIONAL AMS3075F Page 4 of 8_4.5 Test Me

30、thods: 4.5.1 Nonvolatile Content: Weigh approximately 5 grams of compound to the nearest milligram into a tared evaporating dish. Heat the dish and contents in an oven at 221 to 230 F (105 to 110 C) for 24 hours 0.25. Cool to room temperature, reweigh, and calculate the nonvolatile content using Equ

31、ation 1.(Eq. 1)where:A = weight of residue, gramsB = original weight of sample, grams4.5.2 Stability: A sample of compound shall be placed in a test tube, heated to 220 F 2 (104 C 1), and maintained at that temperature for 60 minutes 5. Tube and compound shall be cooled to room temperature, held for

32、 60 minutes 5, further cooled to -40 F 2 (-40 C 1), and maintained at that temperature for 60 minutes 5. Tube and compound shall be reheated to 220 F 2 (104 C 1) and maintained at that temperature for 60 minutes 5. Compound, after returning to room temperature, shall be examined for homogeneity.4.5.

33、3 Wetting Properties and Low-Temperature Adhesion: Two polished and alkaline-cleaned panels of AMS 5044 steel, or equivalent, nominally 1/16 x 4 x 2 inches (1.6 x 102 x 51 mm), shall be immersed for one minute in compound at 205 to 210 F (96 to 99 C), withdrawn, cooled to room temperature, and suspe

34、nded vertically in an atmosphere of not more than 60% relative humidity at 77 F 7 (25 C 4) for 24 hours 0.5. Panels shall be cooled to 0 F 2 (-18 C 1), and maintained at that temperature for 60 minutes 5. While at 0 F 2 (-18 C 1), four parallel scratches about 1/8 inch (3.2 mm) apart and 1 inch (25

35、mm) long shall be made in the compound film with a pointed knife blade; four similar scratches which intersect the first four at right angles shall also be made. There shall be no flaking of the film within the area bounded by the scratches.4.5.4 Rosin: Add 10 grams of compound to 25 mL of 95% ethyl

36、 alcohol and heat the mixture to boiling. One or two drops of the solution of compound in alcohol shall be placed on a porcelain spotplate with three or four drops of acetic anhydride. Add one drop of chemically pure sulfuric acid. A rose-violet coloration, or a flash of purple produced when the aci

37、d meets the anhydride, indicates the presence of rosin.4.5.5 Acidity (Inorganic Acid): A 25 to 50-gram sample of compound shall be introduced into a 250 mL separatory funnel followed by 100 mL of boiling distilled water. The funnel shall be shaken vigorously and, after compound and water have separa

38、ted, the water layer shall be drained into a 500 mL casserole. Compound in the funnel shall be washed twice more by vigorously shaking with 50 mL portions of boiling distilled water. After each washing and separation, the water layer shall be drained into the casserole. One drop of 1% solution of ph

39、enolphthalein shall be added to the 200 mL of accumulated water and the water boiled. A change in color to pink indicates the solution is alkaline. If addition of phenolphthalein causes no change in color, two drops of 0.1% solution of methyl orange shall be added. A change to red or pink indicates

40、the presence of inorganic acid.Nonvolatile Content, % A 100B-=SAE INTERNATIONAL AMS3075F Page 5 of 8_4.5.6 Lead Solubility: A polished specimen of lead sheet, nominally 1/16 x 1 x 1 inch (1.6 x 25 x 25 mm), shall be accurately weighed and immersed for four hours 0.25 in 50 grams 1.0 of compound main

41、tained at 205 to 210 F (96 to 99 C). Specimen shall be removed, cleaned with solvent, and reweighed. Change in weight per square inch (per cm2) shall be calculated. 4.5.7 Loss on Heating: Two polished and alkaline-cleaned panels of AMS 5044 steel, or equivalent, nominally 1/16 x 4 x 2 inches (1.6 x

42、102 x 51 mm), shall be weighed to the nearest milligram. Panels shall be immersed for one minute in compound at 205 to 210 F (96 to 99 C), withdrawn, cooled to room temperature, and suspended vertically in an atmosphere of not more than 60% relative humidity at 77 F 7 (25 C 4) for 24 hours 0.25. Pan

43、els shall be weighed to determine the weight of the coating and then suspended for four hours 0.25 in a circulating air oven at 135 F 2 (57 C 1). After heating, panels shall be carefully removed from the oven, cooled to room temperature, and reweighed. The percentage loss in weight shall be calculat

44、ed. 4.5.8 Humidity Protection: 4.5.8.1 Two freshly sand-blasted panels and two polished and alkaline-cleaned panels of AMS 5044 steel, or equivalent, and two polished panels of AMS 4037 aluminum sheet, each panel nominally 1/16 x 4 x 2 inches (1.6 x 102 x 513 mm), shall be immersed for one minute in

45、 compound at 205 to 210 F (96 to 99 C), withdrawn, and suspended vertically in an atmosphere of not more than 60% relative humidity at 77 F 7 (25 C 4) for 24 hours 0.25.4.5.8.2 After conditioning as in 4.5.8.1, all panels shall be suspended vertically in humid atmosphere for 28 days in accordance wi

46、th ASTM D 1748. Upon completion of the exposure, panels shall be removed from the cabinet, cleaned with solvent, and examined for visible corrosion or pitting of any surface. If corrosion occurs, but no greater than three spots not larger than 0.040 inch (1 mm) in diameter, the compound may be retes

47、ted. If, on retesting, no corrosion spots occur, the compound shall be acceptable. In any case, corrosion within 1/8 inch (3.2 mm) of an edge shall be disregarded.4.5.9 Salt Spray Protection: 4.5.9.1 Two freshly sand-blasted panels, two polished and alkaline-cleaned panels of AMS 5044 steel, or equivalent, and two p