KS I ISO 11369-2008 Water quality-Determination of selected plant treatment agents-Method using high performance liquid chromatography with UV detection after solid-liquid extracti.pdf
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1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS I ISO 11369 ( ) KS I ISO 11369:2008 2008 8 7 http:/www.kats.go.krKS I ISO 11369:2008 : ( ) ( ) ( ) : (http:/www.standard.go.kr) : : 1998 12 24 : 2008 8 7 2008-0411 : : ( 02-509-7266) (http:/www.kats.go.kr). 10 5 , . KS I ISO 11369:2008 ( ) Water quality D
2、etermination of selected plant treatment agents Method using high performance liquid chromatography with UV detection after solid-liquid extraction 1997 1 ISO 11369, Water quality Determination of selected plant treatment agents Method using high performance liquid chromatography with UV detection a
3、fter solid-liquid extraction . 1 (HPLC) . 0.1 g/L ( ) . 0.05 g/L ( 1 ). . 1 (1992) . A . KS I ISO 11369:2008 2 1 CAS ab C8H14CIN5215.7 001912 24 9 T C10H13CIN2O 212.7 015545 48 9 H c9H13CIN6240.7 021725 46 2 T dC6H9CIN5186.6 006190 65 4 T C9H10Cl2N2O 233.1 000330 54 1 H c12H20N4O2252.3 051235 04 2 T
4、 C12H18N2O 206.3 034123 59 6 H C9H10CI2N2O2249.1 000330 55 2 H C14H16CIN2O3277.8 067129 08 2 A C10H11N3OS 221.3 018691 97 9 H cC9H11BrN2O2259.1 003060 89 7 H C15H22CINO2283.8 051218 45 2 A c10H13CIN2O2228.7 19937 59 8 H C9H11CIN2O2214.6 1746 81 2 H cC9H15CIN5228.7 00728 69 3 T C7H12CIN5201.7 000122
5、34 9 T C9H16CIN5229.7 005915 41 3 T aCAS : b T: , H: , A: c . d 2 2.1 RP( ) C 18 . . . 1 . . . . 2.2 HPLC . . 3 . . KS I ISO 11369:2008 3 KS M ISO 5667 1, ( ) KS M ISO 5667 2, 2: KS M ISO 5667 3, 3: KS M ISO 8466 1, (1 ) 4 RP C l8(RP ) , (HPLC) . 5 5.1 , ( HPLC ) , . 5.2 . 5.3 HPLC (6.13 ) . 5.4 c(H
6、3PO4) 1 mol/L 5.5 c(NaOH) 1 mol/L 5.6 RP C 18 . 2.1 . , 2.1 . 5.7 (CH3OH), (CH3CN) (C3H6O) . . 5.8 (reference standards)( 1 ) . 5.9 (5.8 ) 50 mg( ) 100 mL (5.7 ) . KS I ISO 11369:2008 4 (simazine) . 4 . 1 . . 5.10 (stock solution) (5.9 ) 1 mL 100 mL (5.7) . 4 . 1 . 5.11 (reference solutions) (5.10)
7、5 , i 20 ng/mL200 ng/mL . HPLC . 4 . 1 . 5.12 20 mmol/L (CH3COONH4), (CH3COONa) ( ) 0.45 m . . 2 . 6 6.1 . , (PTFE) . 6.2 9 mm, 8 cm RP C 18 6.3 PTFE 1 000 mL 2 000 mL . 6.4 10 mL 1 000 mL . KS I ISO 11369:2008 5 6.5 12 mL . 6.6 6.7 PTFE . 6.8 1 mL, 10 mL 100 mL . 6.9 HPLC , 25 L, 50 L, 100 L, 250 L
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