GOST R EN 14331-2010 Liquid petroleum products Separation and characterization of fatty acid methyl esters (FAME) from middle distillates by method of liquid chromatography and gas.pdf

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1、 143312010 (FAME) EN 14331:2004Liquid petroleum products Separation and characterization of fatty acid methylesters (FAME) from middle distillates Liquid chromatography (LC)/gaschromatography (GC) method(IDT) 27 2002 . 184- , 1.02004 . 1 31 - , - ( ) , 42 3 27 2010 . 1112-4 14331:2004 - . (FAME) - .

2、 (LC) (GC) (N14331:2004 Liquid petroleum products Separation and characterisation of fatty acid methyl esters(FAME) from middle distillates Liquid chromatography (L)/gas chromatography (GC) method). - 1.52004 ( 3.5). - - , 5 , - . - () . , , 2012 , - - II 1433120101 12 13 14 .25 .26 .27 .28 29 310 3

3、11 .312 .3 () 4 () FAME 5 () .6 () ( ) .7 .8III 143312010 (FAME) Liquid petroleum products. Separation and characterization of fatty acid methyl esters (FAME) from middle distillates bymethod of liquid chromatography and gas chromatography 201207011 (FAME) (LC) (GC). FAME , - 14 24. FAME 1618. . FAM

4、E, - 5 % . (% .) - (% .) .2 - 1): 3170 . (EN ISO 3171, Petroleumliquids Manual sampling) 3171 . (EN ISO 3171, Petroleum liquids Automatic pipeline sampling) 5508 . - (EN ISO 5508, Animal and vegetable fats and oils Analysis by gaschromatography of methyl esters of fatty acids)3 :- FAME - ;- FAME .1)

5、 . - , .1 143312010 4 4.1 , . . ., (HPLC).4.2 , . . ., (HPLC).5 5.1 .5.2 25 10 , - 700 55 105 .5.3 20 3.6 , 3170 3171.7 7.1 (5.2) 0,100 3 - 2 . , 10 3 (4.1). ( ) 3 3/. . (5.2) FAME, 10 3 (4.2). FAME 5 % ., , FAME, 5%.7.2 5508 . , . , / , , 24:024:1 ., FAME , , , .8 , FAME, - , , = 100AAic83,(1) Ai ,

6、 i- ;c83A , 14 24.2 1433120109 FAME 0,1 % .10 , FAME.10.1 () , , , -1,.10.2 , , 1, . 1 (16:0) 0,5 0,8 (18:1) 0,6 2,8 (18:3) 0,4 1,811 .1 ( C) , , , - . , , , , , FAME.12 :) ;b) ;c) ( 9);d) , , ;e) .3 143312010 () .1 , :Carbowax 20M, DBwax CPwax: 30 ; : 0,32 ; : 0,25 .2 , , - : : 20100 3/, ;: 250 .3

7、-, , : 3080 .4 , : 200 .5 - , : 250 .6 , .4 143312010 () FAME .1 -, . , , , 24:024:1 (3 ), 1. :16:0 ;16:1 ;18:0 ;18:1 ;18:2 ;18:3 ;20:0 ;20:1 ;22:0 ;22:1 ;24:0 ;24:1 .1 FAME, 5 143312010 () .1 , 2 * 16:039,347,5 2,57,0 5,07,6 16:1c163 0,050,6 c163 0,050,6 c163 0,050,3 18:03,56,0 0,83,0 2,76,5 18:136

8、,044,0 51,070,0 14,039,4 18:29,012,0 15,030,0 48,374,0 18:3c163 0,050,5 5,014,0 c163 0,050,3 20:0c163 0,051,0 0,21,2 0,10,5 20:1c163 0,050,4 0,14,3 c163 0,050,3 22:0c163 0,050,2 c163 0,050,6 0,31,5 22:1c163 0,05 c163 0,052,0 c163 0,050,3 24:0c163 0,05 c163 0,050,3 c163 0,050,6* .6 143312010 () ( ) .

9、1 3170 NEQ 251785 . 3171 NEQ 251785 . 5508 * . - . -. - :NEQ .7 1433120101 EN 14103:2003, Fat and oil derivatives Fatty acid methyl esters (FAME) Determination of ester andlinolenic acid methyl ester contents ( 14103:2003 . (FAME). )*2 CODEX STAN 210, 1999 Revision 1 (2001), Named vegetable oils, volumes, codex alimentarius, jointFAO/WHO Food Standards Programme. Food and Agriculture Organization of the United Nations. Italy(http:/www.codexalimentarius.nt)* 141032008. 662.753.1:006.354 75.080 29 020975.160.20 : , , , - (FAME), (LC), (GC)