GOST R 55312-2012 Propolis Method for determination of flavonoids composition《蜂胶 类黄酮成分的测定方法》.pdf

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1、 553122012 1 - ( -)2 432 3 29 2012 . 1580-4 1.02012 ( 8). ( 1 ) , -.()- . , - (gost.ru) , 2014 , - - II 553122012 Propolis. Method for determination of flavonoid compositions 201401011 - .2 : 5725-12002 ( ) . 1. 12.1.0192009 . . 516522000 . 520012002 . 532282008 . 1. . 12.1.00491 . . 12.4.00983 . .

2、. 12.4.10383 . , . 177074 ( 104283, 478880) ., , , . 670972 . 1202676 . 1491983 , . - 2533682 . , 2888690 . 2922791 ( 835-181) . . 1. - - , 1 , 1 553122012 , . (), - () . , , , , .3 5725-1, 52001.4 4.1 28886 ( 3.1).4.2 , . - 3 .5 , , , - . . 408420 .6 6.1 12.1.019.6.2 12.1.004 12.4.009.6.3 12.4.103.

3、6.4 , - , - .7 , , 7.1 - c1770,001 53228.7.2 , - 390420 .7.3 , , 1 .7.4 , 14919.7.5 2-25-1, 2-50-1, 2-100-1 1770.7.6 -1-100-14/23, -1-250-14/23 25336.7.7 -36-60 -36-80 25336.7.8 1- 100-1000 ,15 31- .7.9 2-1-1-1, 2-2-25, 2-2-5 29227.7.10 .7.11 1-100 1770.7.12 12026.7.13 51652, 96 %.7.14 6709.7.15 6-

4、AlCl3c215 6H2O, 99 %, Fluka, 7784-13-6.7.16 , .2 553122012 , -.8 8.1 5 % 60 %- 250 3 25336 (5,000 c177 0,001) , (50,0 c177 0,5) 60 %- , (100,00 c177 0,01) 60 %- . .8.2 (0,050 c177 0,001) , 50 3 1770, 40 360 %- , 50 60 . , 60 %- .8.3 25 3 1770 0,2 (0,4; 0,6; 0,8, 1,0 1,2) 3 6.7.2.2 1 /3; 4 3 - 6.7.2.

5、1 ( ), 60 %- - . 30 ( ) 390420 1 . -, 25 3 , . .9 9.1 (1,000 c177 0,001) 10 3 25336, (30,0 c177 0,5) 360 %- , - 30 , - . 100 3, . , - (30,0 c177 0,1) 360 %- . , (20 c177 3) (100,00 c177 0,01) 360 %- .9.2 25 3 (5,00 c177 0,01) 3 6.7.2.4. ( ) (4,0 c177 0,1) 3 6.7.2.1, 60 %- . 30 ( ) 390420 1 . , , - 2

6、5 3.10 10.1 ( ) 1,%,-X1= C c215 100 c215 100 c215 m c215 5, (1) 25 3, , ;3 553122012100 , 3;100 , %;m , , ;5 , , 3.10.2 - , , , |X1 X2| c163 r, (2)12 , - , %;r , 1,%.10.3 , , |X1 X2| c163 R, (3)12 , -, %;R , 1, %. 1 , - = 0,95 r,%R,% ( ) c177c100,% - ( - ) 0,1 10 2 8 610.4 ( ) , , (c177c68) %, = 0,95, c68 , %, c68 = c100c215c215 0,01 c68 = c100c215c215 0,01, (4) c100 1, %.10.5 .4 553122012 638.178:006.354 65.140 52 : , , , -5 553122012 . . . . 20.06.2014. 04.07.2014. 60 c180 8418. . . . 0,93. .-. . 0,60. 106 . . 2509. , 123995 , ., 4.www.gostinfo.ru infogostinfo.ru