GOST 32014-2012 Food products food raw materials Method of determination of the nitrofuran mytobolites by high performance liquid chromatography - mass spectrometry (HPLC-MS)《食品 食品.pdf

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1、 , - , ()INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION(ISC)320142012, - 1.092 . - 1.22009 . , . -, , , 1 ( ), - ( )2 3 , (- 3 2012 . 54-) : ( 3166) 00497 ( 3166) 00497 KZKGRUTJUZ 4 27 2013 . 239- 1 2014 5 5399220106 -, - . () . , - - , 2013 -, II 3201420121 .12 13 .24 , , , 25

2、.46 .46.1 46.2 - 56.3 56.4 .66.5 76.6 76.7 .87 .87.1 , .87.2 97.3 , 97.4 -/ .107.5 .108 109 .1110 .1110.1 .1110.2 .11 () 12 () 1314III 320142012 , - Food products, food raw materials. Method of determination of the nitrofuran mytobolites by high performance liquidchromatography mass spectrometry (HP

3、LC-MS)1 , , , , , , , - 1,0 1000,0 /.2 :5725-62003 ()-. 6. 12.1.00588 . - 12.1.00776 . . 12.1.01979 . . - 12.2.0852002 , . . - 177074 ( 104283, 478880) . -, , , . 260379 . . 432877 . . 584873 . . 596267 . 655280 . . 670972 . 699577 . -. 76312008 , . - 1386768 . 1426177 . 197922001 . 2230076 . . - 24

4、1042001 . 1 320142012 20140701 2533682 . , 2680986 . , 2922791 ( 835-181) . . 1. 316542012 . 317202012 . - , 1 , - . - (), () . , , , , .3 3.1 ( ), - , - - (-/).3.2 - .3.3 .4 , , ,4.1 , :- - 100 500 (. . .), - 500, 0,2 . . ., ( /);- , , , 50 ;- - - ;- I II 200 500 , 0,1 1,0 24104;- - , 0 14 . - c177

5、0,01 ;- 10100 3, 40200 3, 2001000 3,153 , 2%;- 40 ;- - ;- - 3 150 2500 /;- 10000 / 4 20 , - 15 3 1,5 3;- 20 1 3;2 320142012- 20 280 / - 30 100 ;- - 150 3,5 ;- ;- 12 3, - 50 ;- () 15 50 3 ;- 0,45 ;- () 2 4 3 - ;- 2 3 50 3;- -1-5-0,1, -2-10-14/23 1770;- -1-100-14/23 25336;- 29227;- 2-100-2, 2-1000-2 1

6、770;- 1-25 (100, 500)-1 1770;- ;- - 18 24 . , - .4.2 :- 14261, . .;- 6995, . .;-,.;- 22300, . .;- 2603;- 5962;- ();- - ;- 99,0 %;- 5848, . . ;- 2- () 98 %;- ;- 4328, . . .;-,.;- ;- 6709. 2 (. .) 3 (. . .) 13867.4.3 - :4.3.1 :- 3-2- () 99,0 %, (Vetranal,33347)*;- 3-5-2- (), 99,0 % (Witega, NF003)*;-

7、1- () 99,0 %,(Witega, NF001)*;- () 99,0%,(Vetranal,33656)*;- 3-(2-) -2- (-) 99,0 %, (Witega, NF013)*;* . .3 320142012- 5-3-(2-)-3-2- (-) - 99,0 %, (Witega, NF011)*;- 1-(2-)- (-) 99,0 %, (Witega, NF009)*;- (2-)- (-) 99,0 %, (Witega, NF015)*.4.3.2 :-d4-3-2- (d4-) 99,0 %,(Witega, NF006)*;-d5-3-5-2- (d5

8、-) 99,0 %, (Vetranal, 33881)*;-1,2-N15,13- (1,2-N15,13-) 99,0 %, (Witega, NF008)*;-(13)31-) (13)3-) 99,0 %,(Witega, NF002)*;-d4-3-(2-)-2- (- d4-) 99,0 %, (Witega, NF014)*;-d5-5-3-(2-)-3-2- (- d5-) 99,0 %, (Witega, NF012)*;-(13)31-(2-)- (-(13)3-) 99,0 %, (Witega, NF015)*;-1,2-N15,13-(2-)- (- 1,2-N15,13-) - 99,0 %, (Witega, NF016)*.5 5.1 1- 2- 12.1.007, , 12.1.005.5.2 ,