EN ISO 10426-2-2003 en Petroleum and natural gas industries - Cements and materials for well cementing - Part 2 Testing of well cements (Incorporating corrigendum July 2007 Incorpo.pdf

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1、BRITISH STANDARDBS EN ISO 10426-2:2003Incorporating amendment no. 1 and corrigendum no. 1Petroleum and natural gas industries Cements and materials for well cementing Part 2: Testing of well cementsThe European Standard EN ISO 10426-2:2003, incorporating amendment A1:2005, has the status of a Britis

2、h StandardICS 75.020; 91.100.10 g49g50g3g38g50g51g60g44g49g42g3g58g44g55g43g50g56g55g3g37g54g44g3g51g40g53g48g44g54g54g44g50g49g3g40g59g38g40g51g55g3g36g54g3g51g40g53g48g44g55g55g40g39g3g37g60g3g38g50g51g60g53g44g42g43g55g3g47g36g58BS EN ISO 10426-2:2003This British Standard was published under the

3、authority of the Standards Policy and Strategy Committee on 16 January 2004 BSI 2007ISBN 978 0 580 60341 9National forewordThis British Standard is the UK implementation of EN ISO 10426-2:2003, incorporating amendment A1:2005 and corrigendum July 2007. It is identical with ISO 10426-2:2003, incorpor

4、ating amendment 1:2005 and corrigendum June 2006.The start and finish of text introduced or altered by corrigendum is indicated in the text by tags . Text altered by ISO corrigendum June 2006 is indicated in the text by .The start and finish of text introduced or altered by ISO amendment is indicate

5、d in the text by tags !“. Tags indicating changes to ISO text carry the number of the ISO amendment. For example, text altered by ISO amendment 1 is indicated by !“.The UK participation in its preparation was entrusted by Technical Committee PSE/17, Materials and equipment for petroleum, petrochemic

6、al and natural gas industries, to Subcommittee PSE/17/-/3, Drilling and completion fluids and well cements.A list of organizations represented on this subcommittee can be obtained on request to its secretary.For additional explanatory information please see the National Annex NA at the end of this s

7、tandard.This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application.Compliance with a British Standard cannot confer immunity from legal obligations.Amendments issued since publicationAmd. No. Date Comments15965 March 200

8、6 See national foreword17384 Corrigendum No. 131 October 2007 See national forewordEUROPEAN STANDARDNORME EUROPENNEEUROPISCHE NORMICS 75.020; 91.100.10English versionPetroleum and natural gas industries - Cements and materialsfor well cementing - Part 2: Testing of well cementsIndustries du ptrole e

9、t du gaz naturel - Ciments etmatriaux pour la cimentation des puits - Partie 2: EssaisCEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists a

10、nd bibliographical references concerning such nationalstandards may be obtained on application to the Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility

11、 of a CEN member into its own language and notified to the Management Centre has the same status as the officialversions.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: rue de Stassart, 36 B-1050 Brussels 2003 CEN All rights of exp

12、loitation in any form and by any means reservedworldwide for CEN national Members.EN ISO 10426-2 October 2003 +A1September 2005 (ISO 10426-2:2003)de ciments pour puits (ISO 10426-2:2003) Erdl- und Erdgasindustrie - Zemente und Materialien frdie Zementation von Tiefbohrungen - Teil 2: Prfungen frBohr

13、loch-Zemente (ISO 10426-2:2003)Ref. No. EN ISO 10426-2:2003 EThis European Standard was approved by CEN on 1 October 2003. CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy,

14、Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. Incorporating corrigendum July 2007ForewordThis document (EN ISO 10426-2:2003) has been prepared by Technical Committee ISO/TC 67“Materials, equipment and o

15、ffshore structures for petroleum and natural gas industries“ incollaboration with Technical Committee CEN/TC 12 “Materials, equipment and offshorestructures for petroleum and natural gas industries“, the secretariat of which is held by AFNOR.This European Standard shall be given the status of a nati

16、onal standard, either by publication ofan identical text or by endorsement, at the latest by April 2004, and conflicting nationalstandards shall be withdrawn at the latest by April 2004.According to the CEN/CENELEC Internal Regulations, the national standards organizations ofthe following countries

17、are bound to implement this European Standard: Austria, Belgium, CzechRepublic, Denmark, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy,Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland andthe United Kingdom.NOTE FROM CMC The foreword is susce

18、ptible to be amended on reception of the Germanlanguage version. The confirmed or amended foreword, and when appropriate, the normativeannex ZA for the references to international publications with their relevant Europeanpublications will be circulated with the German version.Endorsement noticeThe t

19、ext of ISO 10426-2:2003 has been approved by CEN as EN ISO 10426-2:2003 without anymodifications.EN ISO 104262:2003Foreword to amendment A1 This document (EN ISO 10426-2:2003/A1:2005) has been prepared by Technical Committee ISO/TC 67 “Materials, equipment and offshore structures for petroleum and n

20、atural gas industries“ in collaboration with Technical Committee CEN/TC 12 “Materials, equipment and offshore structures for petroleum and natural gas industries“, the secretariat of which is held by AFNOR.This European Standard shall be given the status of a national standard, either by publication

21、 of an identical text or by endorsement, at the latest by March 2006, and conflicting national standards shall be withdrawn at the latest by March 2006. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this Euro

22、pean Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. Endorsement n

23、otice The text of ISO 10426-2:2003 has been approved by CEN as EN ISO 10426-2:2003/A1:2005 without any modifications. Reference numberISO 10426-2:2003(E)NINRETOITALANADNATSDRISO162402-tide tsriFino-300251-01Petroleum and natural gas industries Cements and materials for well cementing Part 2: Testing

24、 of well cements Industries du ptrole et du gaz naturel Ciments et matriaux pour la cimentation des puits Partie 2: Essais de ciment pour puits INTERNATIONALSTANDARDISO10426-2First edition2003-10-15EN ISO 104262:2003iiiiiContents PageForeword viIntroduction vii1 Scope 12 Normative references . 13 Te

25、rms, definitions and symbols 13.1 Terms and definitions. 13.2 Symbols . 74 Sampling 84.1 General. 84.2 Sampling cement at field location. 84.3 Sampling cement blends at field location 84.4 Sampling dry cement additives at field location . 84.5 Sampling liquid cement additives at field location .84.6

26、 Sampling mixing water. 84.7 Shipping and storage . 104.8 Sample preparation prior to testing 104.9 Sample disposal 105 Preparation of slurry. 105.1 General. 105.2 Apparatus. 105.3 Procedure. 126 Determination of slurry density. 146.1 Preferred apparatus 146.2 Calibration 146.3 Procedure. 146.4 Alte

27、rnative apparatus and procedure . 167 Well-simulation compressive strength tests 167.1 General. 167.2 Sampling 167.3 Preparation of slurry. 177.4 Apparatus. 177.5 Procedure. 187.6 Determination of cement compressive strength at the top of long cement columns . 208 Non-destructive sonic testing of ce

28、ment . 268.1 General. 268.2 Apparatus. 268.3 Sampling 268.4 Preparation of slurry. 268.5 Procedure. 268.6 Curing time 268.7 Curing schedules 268.8 Data reporting 279 Well-simulation thickening-time tests 279.1 General. 279.2 Apparatus and material 279.3 Calibration 289.4 Test procedure 30EN ISO 1042

29、62:2003iv9.5 Determination of test schedule3210 Static fluid-loss tests 3810.1 General .3810.2 Apparatus.3810.3 Safety3910.4 Mixing procedure.3910.5 Conditioning procedures3910.6 Procedures for testing at temperatures u 88 qC (190 qF)3910.7 Procedures for testing at temperatures ! 88 qC (190 qF).401

30、0.8 Filling the static fluid-loss cell.4210.9 Fluid loss test 4310.10 Test completion and clean-up4311 Permeability tests4511.1 General .4511.2 Apparatus.4511.3 Sample preparation.4611.4 Liquid permeability (cement permeameter)4611.5 Alternative procedure (core permeameter) for liquid permeability47

31、11.6 Calculating liquid permeability 5011.7 Gas permeability (core permeameter).5011.8 Calculating gas permeability5112 Determination of rheological properties and gel strength using a rotational viscometer 5212.1 General .5212.2 Apparatus.5212.3 Calibration5412.4 Determination of rheological proper

32、ties.5412.5 Determination of gel strength 5612.6 Modelling of the rheological behaviour 5713 Calculation of pressure drop and flow regime for cement slurries in pipes and annuli .6513.1 General .6513.2 Newtonian fluids6713.3 Power Law fluids .7113.4 Bingham Plastic fluids7713.5 Conversion factors871

33、4 Test procedure for arctic cementing slurries.8714.1 General .8714.2 Preparation of cement slurry .8714.3 Fluid fraction8714.4 Thickening time .8714.5 Compressive strength 8714.6 Freeze-thaw cycling at atmospheric pressure .8814.7 Compressive strength cyclic testing.8815 Well-simulation slurry stab

34、ility tests.8815.1 Introduction8815.2 Slurry mixing8915.3 Slurry conditioning8915.4 Free-fluid test with heated static period .8915.5 Free-fluid test with ambient temperature static period .9015.6 Sedimentation test 9016 Compatibility of wellbore fluids.9416.1 General .9416.2 Preparation of test flu

35、ids 9416.3 Rheology 9516.4 Thickening time .9516.5 Compressive strength 9516.6 Solids suspension and static gel strength .95EN ISO 104262:2003v16.7 Fluid loss 9517 Pozzolans. 9817.1 General. 9817.2 Types of pozzolan . 9817.3 Physical and chemical properties . 9817.4 Slurry calculations 9917.5 Bulk v

36、olume of a blend. 100Annex A (normative) Procedure for preparation of large slurry volumes 102Annex B (normative) Calibration procedures for thermocouples, temperature-measuring systems and controllers 104Annex C (informative) Additional information relating to temperature determination 106Annex D (

37、normative) Alternative apparatus for well thickening-time tests . 113Annex E (informative) Cementing schedules 116Bibliography . 171EN ISO 104262:200316.8 Water-wetting capability test (WWCT) 95viForeword ISO (the International Organisation for Standardisation) is a worldwide federation of national

38、standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International

39、 organisations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardisation. International Standards are drafted in accordance with the rules g

40、iven in the ISO/IEC Directives, Part 2. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibi

41、lity that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 10426-2 was prepared by Technical Committee ISO/TC 67, Materials, equipment and offshore structures for petroleum, petrochemical a

42、nd natural gas industries, Subcommittee SC 3, Drilling and completion fluids and well cements.ISO 10426 consists of the following parts, under the general title Petroleum and natural gas industries Cements and materials for well cementing: Part 1: Specification Part 2: Testing of well cements Part 3

43、: Testing of deepwater well cement formulations Part 4: Preparation and testing of foamed cement slurries at atmospheric pressure The following part is under preparation: Part 5: Determination of shrinkage and expansion of well cement formulations at atmospheric pressure EN ISO 104262:2003Foreword t

44、o amendment A1 ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for whi

45、ch a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all m

46、atters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical committees are cir

47、culated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held respon

48、sible for identifying any or all such patent rights. Amendment 1 to ISO 10426-2:2003 was prepared by Technical Committee ISO/TC 67, Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries, Subcommittee SC 3, Drilling and completion fluids and well cements

49、.viiIntroduction This part of ISO 10426 is based on API RP 10B, 22nd edition, December 1997, addendum 1, October 1999. Users of this part of ISO 10426 should be aware that further or differing requirements may be needed for individual applications. This part of ISO 10426 is not intended to inhibit a vendor from offering, or the purchaser from accepting, alternative equipment or engineering solutions for the individual application. This may be particularly applicable where there is innovative or developing technology. Where a