EN ISO 787-9-1995 en General Methods of Test for Pigments and Extenders - Part 9 Determination of pH Value of an Aqueous Suspension《颜料和填充剂的一般试验方法 第9部分 水悬浮液pH值的测定 ISO 787-9-1981》.pdf
《EN ISO 787-9-1995 en General Methods of Test for Pigments and Extenders - Part 9 Determination of pH Value of an Aqueous Suspension《颜料和填充剂的一般试验方法 第9部分 水悬浮液pH值的测定 ISO 787-9-1981》.pdf》由会员分享,可在线阅读,更多相关《EN ISO 787-9-1995 en General Methods of Test for Pigments and Extenders - Part 9 Determination of pH Value of an Aqueous Suspension《颜料和填充剂的一般试验方法 第9部分 水悬浮液pH值的测定 ISO 787-9-1981》.pdf(11页珍藏版)》请在麦多课文档分享上搜索。
1、- CEN EN*IS0*787-9 95 3YOY589 OLLLL29 7LT I A BRITISHSTANDARD General methods of test for pigments and extenders Part 9. Determination of pH value of aqueous suspension The European standard EN Is0 787-9 : 1995 has the status of a British Standard BS EN IS0 787-9 : 1995 CEN EN*IS0*787-9 95 E3 340458
2、9 O11L130 431 F National foreword This revision of Part C4 of BS 3483 has been prepared under the direction of the Pigments. Paints and Varnishes Standads Committee. It is identical with IS0 787/9 General methods of test for pigments and extenders - Part 9 : Determination of pH value of an aqueous s
3、uspension published in 1981 by the International Organization for Standardization (ISO). Ln 1994theEuropeancOmmitteeforsQndardization(CEN)acceptediso7:1981 as European standard ENiS74: 1995. As a comace of impiementhg the European standard this British Stanard is renumbered as BsENISO787-9 and any r
4、eference to EIS 3483 : Part C4 should be read as a reference to BS EN Is0 787-9. This Part of BS 3483 supersedes BS 3483 : Part C4 : 1974 which is withdrawn. Terminology and conventions. The text of the international standard has been approved as suitable for publication as a British Standard withou
5、t deviation. Some terminology and certain conventions are not identical with those used in British Standards; attention is especially drawn to the following. The comma has been used throughout as a decimal marker. In British Standards it is current practice to use a full point on the baseline as the
6、 decimal marker. Wherever the words This part of IS0 787 and International Standard appear, referring to this standard, they should be read as This Part of ES 3483 and British Standard respectively. Cross-reference A I nternstional dandard IS0 842-1 974 Corresponding British Standard BS 4726 : 1971
7、Methods for sampling raw materials for paints and varnishes (Technically equivalent) Additional information. In the last paragraph of clause 6 of IS0 787/9-1981, it is stated that the procedure is to be repeated if the duplicate determinations differ by more than 0.3 unit. In implementing this stand
8、ard in the United Kingdom, it is recommended that, if repeat dererminations are necessary, wherever possible both the sampling (clause 5) and the procedure (clause 6) should be repeated. In paragraph 1 of clause 6, the room temperature is unspecified. It is recommended that the temperature of the te
9、st should be 23 ? 2 “C.“ Compliance with a British Standard does not of itself confer immunity from legal obligations. These changes have been reported to the IS0 in a proposal to amend the text of the international standard. British Standards institution CEN EN*IS0*787-9 95 23 3404589 OLLLL3L 378 f
10、 BS 3483 : Part C4 : 1982 O introduction This document is a part of IS0 787, Generalmethods of test for pigments and extenders. 1 Scope and field of application This patt of IS0 787 specifies a general method of test for determining the pH value of an aqueous suspension of a sam- pie of pigment or e
11、xtender. NOTE - When this general method is applicable to a given pigment or extender, only a cross-reference to it should be included in the Intema- tional Standard relating to that pigment or extender, with a note of any detailed modification which may be needed in view of the special pro- perties
12、 of the material in question. Only when this general method is not applicable to a particular material should a special method for determination of pH value be specified. 2 Reference IS0 842, Raw materials for paints and varnishes - SarnpJing. 3 Reagent Freshly distilled water, boiled before use to
13、remove carbon dioxide, or water otherwise prepared of at least equivalent pu- rity. The water shall be boiled and cooled in a vessel made of chemically resistant glass, immediately before use. It shall be boiled for 5 to 10 min only, in order to avoid an increase of its pH value due to alkali dissol
14、ved from the glass vessel. Because water rapidly absorbs carbon dioxide, the cooled water shall be protected from access to the atmosphere and shall be stored for not more than 30 min. The closed container should be pro- tected by a soda asbestos tube or similar device. 4 Apparatus 4.1 resistant gla
15、ss, fitted with a ground glass or rubber stopper. Before using the container for the first time, boil dilute hydrochloric acid placed in the container and then rinse it thoroughly with distilled water. The rubber stopper shall not have been used for any other purpose. Glass container, of capacity 50
16、 ml, made of chemically 4.2 pH measuring device, capable of measurement to 0.1 unit, calibrated against buffer solutions of known pH value at the temperature of the test. 4.3 Balance, with an appropriate accuracy. 5 Sampling Take a representative sample of the material to be tested as described in I
17、S0 842. 6 Procedure *Carry out the determination in duplicate at room temperature. Prepare a 10 % (rnlrn) suspension of the material under test, using the distilled water (clause 3J, in the glass container (4.1 1. Stopper the container and shake it vigorously for 1 min. Allow it to stand for 5 min,
18、remove the stopper and determine, to the nearest 0.1 unit, the pH value of the suspension. If the material does not disperse easily in water, a wetting agent should be used; in the case of materials not soluble in ethanol, up to 5 mi of ethanol may be used but care should be taken to ensure that the
19、 minimum quantity is used and that it is neutral and free from pyridine. In the case of pigments soluble in ethanol, a neutral non-ionic wetting agent such as 10 ml of a 0,Ol % (mim) solution of an ethylene oxide condensate should be used. The neutrality of the wetting agent should be checked by mak
20、ing a blank determination. If a wetting agent is used, the volume of the water should be reduced so that a 10 % rn/rn) suspension is obtained. The type and quantity of wetting agent used shall be stated in the test report. NOTE - With pigments and extenders of relatively low density, it may be neces
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