EN 17033-2018 en Plastics - Biodegradable mulch films for use in agriculture and horticulture - Requirements and test methods.pdf

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1、BSI Standards PublicationWB11885_BSI_StandardCovs_2013_AW.indd 1 15/05/2013 15:06Plastics Biodegradable mulch films for use in agriculture and horticulture Requirements and test methodsBS EN 17033:2018EUROPEANSTANDARDNORME EUROPENNE EUROPISCHE NORMEN 17033 January 2018ICS 83.140.10EnglishVersionPlas

2、tics - Biodegradable mulch films for use in agricultureand horticulture - Requirements and test methodsPlastiques - Films de paillage biodgradablesthermoplastiques pour utilisation en agriculture et horticulture - Exigences et mthodes dessaiKunststoffe - Biologisch abbaubare Mulchfolien fr denEinsat

3、z in Landwirtschaft und Gartenbau - Anforderungen und PrfverfahrenThis European Standard was approved by CEN on 13 November 2017.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving thisEuropean Standard the status of a national standard

4、 without any alteration.Up-to-date lists and bibliographical referencesconcerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any oth

5、er language made bytranslation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC ManagementCentre has the same status as the officialversions.CEN members are the nationalstandards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denm

6、ark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom.EUROPEAN CO

7、MMITTEE FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGCEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels 2018 CEN All rights of exploitation in any form and by any means reservedworldwide for CENnational Members.Ref. No. EN 17033:2018 ENational fore

8、wordThis British Standard is the UK implementation of EN 17033:2018.The UK participation in its preparation was entrusted to Technical Committee PRI/75, Plastics and rubber film and sheets.A list of organizations represented on this committee can be obtained on request to its secretary.This publicat

9、ion does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. The British Standards Institution 2018 Published by BSI Standards Limited 2018ISBN 978 0 580 94365 2ICS 83.140.10Compliance with a British Standard cannot confer immunity fr

10、om legal obligations. This British Standard was published under the authority of the Standards Policy and Strategy Committee on 28 February 2018.Amendments/corrigenda issued since publicationDate Text affectedBRITISH STANDARDBS EN 17033:2018EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 17033

11、January 2018 ICS 83.140.10 English Version Plastics - Biodegradable mulch films for use in agriculture and horticulture - Requirements and test methods Plastiques - Films de paillage biodgradables thermoplastiques pour utilisation en agriculture et horticulture - Exigences et mthodes dessai Kunststo

12、ffe - Biologisch abbaubare Mulchfolien fr den Einsatz in Landwirtschaft und Gartenbau - Anforderungen und Prfverfahren This European Standard was approved by CEN on 13 November 2017. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving t

13、his European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official

14、 versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies of Aus

15、tria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spa

16、in, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels 2018 CEN All rights of exploitation in any form and by any means reserved worl

17、dwide for CEN national Members. Ref. No. EN 17033:2018 EBS EN 17033:2018EN 17033:2018 (E) 2 Contents Page EUROPEAN FOREWORD 4 1 SCOPE . 5 2 NORMATIVE REFERENCES . 5 3 TERMS AND DEFINITIONS . 6 3.1 DEFINITIONS RELATED TO FILMS . 6 3.2 DEFINITIONS RELATED TO BIODEGRADATION AND DISINTEGRATION . 7 3.3 D

18、EFINITIONS RELATED TO TEST SOIL 8 3.4 DEFINITIONS RELATED TO ECOTOXICITY AND CONTROL OF CONSTITUENTS . 9 4 GENERAL REQUIREMENTS 9 5 REQUIREMENTS FOR MATERIALS, TESTING SCHEMES AND EVALUATION CRITERIA FOR BIODEGRADATION AND ECOTOXICITY . 9 5.1 CONTROL OF CONSTITUENTS . 9 5.2 BIODEGRADATION . 10 5.3 E

19、COTOXICITY 11 6 DIMENSIONAL, MECHANICAL AND OPTICAL PROPERTIES OF THE FILMS 14 6.1 REQUIREMENTS 14 6.2 APPEARANCE OF FILMS . 15 6.3 TEST METHODS . 15 7 DELIVERY CHECKING . 17 8 FILM DESIGNATION 17 9 MARKING . 17 9.1 MARKING OF THE FILM (OPTIONAL) 17 9.2 MARKING ON PACKAGING OR LABEL 18 10 TEST REPOR

20、T 18 11 FUNCTIONS AND SERVICE LIFE OF BIODEGRADABLE MULCH FILMS 18 12 CONDITIONS FOR INSTALLATION AND USE OF MULCH FILMS . 18 ANNEX A (NORMATIVE) PREPARATION OF SOILS FOR ECOTOXICITY TESTING 19 A.1 GENERAL 19 A.2 PREPARATION OF THE SOIL 19 A.3 REACTORS 19 A.4 INITIAL TEST ITEM CONCENTRATION 19 A.5 T

21、EST DURATION . 20 ANNEX B (NORMATIVE) DETERMINATION OF ACUTE EFFECTS OF MATERIALS ON THE EMERGENCE AND GROWTH OF HIGHER PLANTS 21 B.1 GENERAL 21 B.2 PROCEDURE 21 BS EN 17033:2018EN 17033:2018 (E) 3 B.3 EVALUATION OF THE RESULTS 22 ANNEX C (NORMATIVE) DETERMINATION OF ACUTE EFFECTS OF MATERIALS ON EA

22、RTHWORMS . 23 C.1 GENERAL . 23 C.2 PROCEDURE 23 C.3 EVALUATION OF THE RESULTS 23 ANNEX D (NORMATIVE) DETERMINATION OF EFFECTS OF MATERIALS ON REPRODUCTION OF EARTHWORMS 24 D.1 GENERAL . 24 D.2 PROCEDURE 24 D.3 EVALUATION OF THE RESULTS 24 ANNEX E (NORMATIVE) DETERMINATION OF NITRIFICATION ACTIVITY O

23、F SOIL MICROORGANISMS . 25 E.1 GENERAL . 25 E.2 PROCEDURE 25 E.3 EVALUATION OF THE RESULTS 25 ANNEX F (NORMATIVE) DETERMINATION OF RELATIVE LIGHT TRANSMISSION 26 F.1 PRINCIPLE . 26 F.2 APPARATUS 26 F.3 PROCEDURE 26 F.4 EXPRESSION OF RESULTS 26 ANNEX G (INFORMATIVE) FUNCTIONS AND SERVICE LIFE OF BIOD

24、EGRADABLE MULCH FILMS . 27 G.1 GENERAL . 27 G.2 FACTORS OF DEGRADATION OF BIODEGRADABLE MULCH FILMS . 27 G.3 MAIN FUNCTIONS OF BIODEGRADABLE MULCH FILMS . 27 G.4 SERVICE LIFE ON SOIL OF BIODEGRADABLE MULCH FILMS 28 ANNEX H (INFORMATIVE) GOOD PRACTICE GUIDANCE FOR USE OF BIODEGRADABLE MULCH FILMS 31

25、H.1 WARNING . 31 H.2 SOIL PREPARATION . 31 H.3 FILM LAYING . 31 H.4 FILM PERFORATION 31 H.5 CULTIVATION TECHNIQUES AND BIODEGRADABLE FILMS 32 H.6 FILM LIFETIME 33 H.7 TREATMENT OF FILMS AT THE END OF CULTIVATION . 33 H.8 STORAGE 33 ANNEX I (INFORMATIVE) QUALITATIVE EVALUATION OF THE DISINTEGRATION I

26、N A SLIDE FRAME TEST . 35 BIBLIOGRAPHY 38 BS EN 17033:2018EN 17033:2018 (E) 4 European foreword This document (EN 17033:2018) has been prepared by Technical Committee CEN/TC249 “Plastics”, the secretariat of which is held by NBN. This European Standard shall be given the status of a national standar

27、d, either by publication of an identical text or by endorsement, at the latest by July 2018, and conflicting national standards shall be withdrawn at the latest by July 2018. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN sha

28、ll not be held responsible for identifying any or all such patent rights. According to the CEN-CENELEC Internal Regulations, the national standards organisations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Den

29、mark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. BS EN

30、 17033:2018EN 17033:2018 (E) 5 1 Scope This document specifies the requirements for biodegradable films, manufactured from thermoplastic materials, to be used for mulch applications in agriculture and horticulture. This document is applicable to films intended to biodegrade in soil without creating

31、any adverse impact on the environment. It also specifies the test methods to assess these requirements as well as requirements for the packaging, identification and marking of films. For information, it defines a classification of biodegradable mulch films according to their service life on soil and

32、 gives a good practice guide for the use of the films. NOTE Films intended to be removed after use and not incorporated in the soil are not in the scope of this standard. They are in the scope of EN 13655 1. 2 Normative references The following documents are referred to in the text in such a way tha

33、t some or all of their content constitutes requirements of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN ISO 472, Plastics - Vocabulary (ISO 472) EN ISO 527-1, Plastics

34、 - Determination of tensile properties - Part 1: General principles (ISO 527-1) EN ISO 527-3, Plastics - Determination of tensile properties - Part 3: Test conditions for films and sheets (ISO 527-3) EN ISO 7765-1:2004, Plastics film and sheeting - Determination of impact resistance by the free-fall

35、ing dart method - Part 1: Staircase methods (ISO 7765-1:1988) EN ISO 11268-1, Soil quality - Effects of pollutants on earthworms - Part 1: Determination of acute toxicity to Eisenia fetida/Eisenia andrei (ISO 11268-1) EN ISO 11268-2, Soil quality - Effects of pollutants on earthworms - Part 2: Deter

36、mination of effects on reproduction of Eisenia fetida/Eisenia andrei (ISO 11268-2) EN ISO 11274, Soil quality - Determination of the water-retention characteristic - Laboratory methods (ISO 11274) EN ISO 12846, Water quality - Determination of mercury - Method using atomic absorption spectrometry (A

37、AS) with and without enrichment (ISO 12846) EN ISO 17294-2, Water quality - Application of inductively coupled plasma mass spectrometry (ICP-MS) - Part 2: Determination of selected elements including uranium isotopes (ISO 17294-2) EN ISO 17556:2012, Plastics - Determination of the ultimate aerobic b

38、iodegradability of plastic materials in soil by measuring the oxygen demand in a respirometer or the amount of carbon dioxide evolved (ISO 17556:2012) ISO 4591, Plastics Film and sheeting Determination of average thickness of a sample, and average thickness and yield of a roll, by gravimetric techni

39、ques (gravimetric thickness) ISO 4592, Plastics Film and sheeting Determination of length and width BS EN 17033:2018EN 17033:2018 (E) 6 ISO 4593, Plastics Film and sheeting Determination of thickness by mechanical scanning ISO 10390, Soil quality Determination of pH ISO 15685, Soil quality Determina

40、tion of potential nitrification and inhibition of nitrification Rapid test by ammonium oxidation OECD 208, OECD Guidelines for the Testing of Chemicals, Section 2, Effects on Biotic Systems Test No. 208: Terrestrial Plant Test: Seedling Emergence and Seedling Growth Test 3 Terms and definitions For

41、the purposes of this document, the terms and definitions given in EN ISO 472 and the following apply. ISO and IEC maintain terminological databases for use in standardization at the following addresses: IEC Electropedia: available at http:/www.electropedia.org/ ISO Online browsing platform: availabl

42、e at http:/www.iso.org/obp 3.1 Definitions related to films 3.1.1 mulch film film made from thermoplastic material intended to be used in agriculture and horticulture to cover the ground in order to improve growing conditions of crops and depending on the colour to control weeds Note 1 to entry: It

43、is assumed that a transparent mulch film does not allow to control weeds. 3.1.2 material homogenous preparation of biodegradable polymer and additives, as necessary, such as carbon black and colour pigments Note 1 to entry: Additives are usually introduced under the form of masterbatches using as ca

44、rrier resin a biodegradable polymer. 3.1.3 masterbatch well-dispersed mixture of a polymer and high percentages of one or more components (colorants and/or other additives) in known proportions for use in blending in appropriate amounts with the basic polymer in the preparation of a compound SOURCE:

45、 EN ISO 472:2013, definition 2.574 3.1.4 width overall width of a film when lying flat Note 1 to entry: It is expressed in millimetres (mm). BS EN 17033:2018EN 17033:2018 (E) 7 3.1.5 nominal width width of a film, as declared by the manufacturer Note 1 to entry: It is expressed in millimetres (mm).

46、3.1.6 thickness thickness at any point of a film Note 1 to entry: It is expressed in micrometres (m). 3.1.7 nominal thickness thickness of a film, as declared by the manufacturer Note 1 to entry: It is expressed in micrometres (m). 3.1.8 roll length largest dimension of the film corresponding to the

47、 length of the unwinded roll Note 1 to entry: It is expressed in metres (m). 3.1.9 nominal roll length roll length, as declared by the manufacturer Note 1 to entry: It is expressed in metres (m). 3.1.10 longitudinal direction MD direction parallel to the roll length, corresponding to the extrusion d

48、irection 3.1.11 transverse direction TD direction parallel to the width (at a right angle to the roll length) 3.1.12 radiant exposure H time integral of irradiance, measured in joules per square metre (Jm2) Note 1 to entry: measured in joules per square metre (J m2) SOURCE: ISO 9370:2017, definition

49、 3.27 3.2 Definitions related to biodegradation and disintegration 3.2.1 ultimate aerobic biodegradation breakdown of an organic compound by microorganisms in the presence of oxygen into carbon dioxide, water and mineral salts of any other elements present (mineralization) plus new biomass BS EN 17033:2018EN 17033:2018 (E) 8 SOURCE: ISO 17088:2012, 3.10 3.2.2 mineralization decomposition of organic matter or organic substances into carbon dioxide, water and the hydrides, oxides or other mineral salts SOURCE: ISO 11074:2005