DIN EN ISO 7143-2007 Binders for paints and varnishes - Methods of test for characterizing water-based binders (ISO 7143 2007)English version of DIN EN ISO 7143 2007-05《涂料和清漆用粘合剂 水.pdf

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1、May 2007DEUTSCHE NORM English price group 7No part of this standard may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 87.060.20!,xbB“9856331www.d

2、in.deDDIN EN ISO 7143Binders for paints and varnishes Methods of test for characterizing water-based binders (ISO 7143:2007)English version of DIN EN ISO 7143:2007-05Bindemittel fr Beschichtungsstoffe Prfverfahren zur Charakterisierung von wasserverdnnbaren Bindemitteln(ISO 7143:2007)Englische Fassu

3、ng DIN EN ISO 7143:2007-05SupersedesDIN EN ISO 7143:2004-09www.beuth.deDocument comprises 10 pages 08.07DIN EN ISO 7143:2007-05 2 National foreword This standard falls in the domain of Technical Committee CEN/TC 139 “Paints and varnishes” (Secretariat: DIN, Germany). It is identical with Internation

4、al Standard ISO 7143 which was prepared by ISO/TC 35/SC 10 “Test methods for binders for paints and varnishes” (Secretariat: DIN, Germany). The responsible German body involved in its preparation was the Normenausschuss Beschichtungsstoffe und Beschichtungen (Coatings and Coating Materials Standards

5、 Committee), Technical Committee NA 002-00-02 AA Lackrohstoffe. Readers should note that ISO 12000 gives definitions relative to polymer dispersions and lattices, and identifies the test methods applicable to the determination of their properties. ISO 12000 covers both aqueous and non-aqueous polyme

6、r dispersions, and products of synthetic and natural origin, including synthetic rubber lattices. It was prepared by Technical Committee ISO/TC 61 “Plastics” Subcommittee SC 9 “Thermoplastic materials”, in close collaboration with ISO/TC 45 “Rubber and rubber products”. The DIN Standards correspondi

7、ng to the International Standards referred to in the EN are as follows: ISO 976 DIN ISO 976 ISO 2115 DIN ISO 2115 ISO 2811-1 DIN EN ISO 2811-1 ISO 3219 DIN EN ISO 3219 ISO 3251 DIN EN ISO 3251 ISO 4576 DIN EN ISO 4576 ISO 4618 DIN EN ISO 4618 ISO 13741-1 DIN ISO 13741-1 ISO 13741-2 DIN ISO 13741-2 I

8、SO 13885-1 DIN 55672-1 ISO 15528 DIN EN ISO 15528 ISO 15880 DIN EN ISO 15880 ISO 16805 DIN EN ISO 16805 Amendments This standard differs from DIN EN ISO 7143:2004-09 as follows: a) Water-based coating materials have been excluded from the scope because these products are not specified in accordance

9、with this standard. b) The determination of molecular mass has been added to Table 1. c) The normative references have been updated and the text has been editorially revised. Previous editions DIN ISO 7143: 2000-12 DIN EN ISO 7143: 2004-09 DIN EN ISO 7143:2007-05 3 National Annex NA (informative) Bi

10、bliography DIN 55672-1, Gel permeation chromatography (GPC) Part 1: Tetrahydrofuran (THF) as elution solvent DIN EN ISO 2811-1, Paints and varnishes Determination of density Part 1: Pyknometer method DIN EN ISO 3219, Plastics Polymers/resins in the liquid state or as emulsions or dispersions Determi

11、nation of viscosity using a rotational viscometer with defined shear rate DIN EN ISO 3251, Paints, varnishes and plastics Determination of non-volatile matter content DIN EN ISO 4618, Paints and varnishes Terms and definitions DIN EN ISO 15528, Paints, varnishes and raw materials for paints and varn

12、ishes Sampling DIN EN ISO 15880, Paints, varnishes and binders Determination of MEQ value of water-based coating materials and binders DIN EN ISO 16805, Binders for paints and varnishes Determination of glass transition temperature DIN ISO 976, Rubber and plastics Polymer dispersions and rubber lati

13、ces Determination of pH DIN ISO 2115, Plastics Polymer dispersions Determination of white point temperature and minimum film-forming temperature DIN ISO 4576, Plastics Polymer dispersions Determination of sieve residue (gross particle and coagulum content) DIN ISO 13741-1, Plastics/rubber Polymer di

14、spersions and rubber latices (natural and synthetic) Determination of residual monomers and other organic components by capillary-column gas chromatography Part 1: Direct liquid injection method DIN ISO 13741-2, Plastics/rubber Polymer dispersions and rubber latices (natural and synthetic) Determina

15、tion of residual monomers and other organic components by capillary-column gas chromatography Part 2: Headspace method DIN EN ISO 7143:2007-05 4 This page is intentionally blank EUROPEAN STANDARDNORME EUROPENNEEUROPISCHE NORMEN ISO 7143February 2007ICS 87.060.20 Supersedes EN ISO 7143:2004 English V

16、ersionBinders for paints and varnishes - Methods of test forcharacterizing water-based binders (ISO 7143:2007)Liants pour peintures et vernis - Mthodes dessai pourcaractriser les liants base deau (ISO 7143:2007)Bindemittel fr Beschichtungsstoffe - Prfverfahren zurCharakterisierung von wasserverdnnba

17、ren Bindemitteln(ISO 7143:2007)This European Standard was approved by CEN on 6 February 2007.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date

18、lists and bibliographical references concerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the res

19、ponsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Ice

20、land, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: rue de Sta

21、ssart, 36 B-1050 Brussels 2007 CEN All rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN ISO 7143:2007: EForeword This document (EN ISO 7143:2007) has been prepared by Technical Committee ISO/TC 35 “Paints and varnishes” in collaboration with

22、Technical Committee CEN/TC 139 “Paints and varnishes”, the secretariat of which is held by DIN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by August 2007, and conflicting national standards shal

23、l be withdrawn at the latest by August 2007. This document supersedes EN ISO 7143:2004. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic

24、, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. Endorsement notice The text of ISO 7143:2007 has been appro

25、ved by CEN as EN ISO 7143:2007 without any modifications. 2 EN ISO 7143:2007 (E) 1 Scope This International Standard specifies methods of test for characterizing binders, i.e. aqueous dispersions and solutions of polymers and copolymers, in particular those used as raw materials for water-based coat

26、ing materials. The properties determined will depend on whether a drying or curing system is tested. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the lat

27、est edition of the referenced document (including any amendments) applies. ISO 976, Rubber and plastics Polymer dispersions and rubber latices Determination of pH ISO 2115, Plastics Polymer dispersions Determination of white point temperature and minimum film-forming temperature ISO 2811-1, Paints a

28、nd varnishes Determination of density Part 1: Pyknometer method ISO 3219, Plastics Polymers/resins in the liquid state or as emulsions or dispersions Determination of viscosity using a rotational viscometer with defined shear rate ISO 3251, Paints, varnishes and plastics Determination of non-volatil

29、e-matter content ISO 4576, Plastics Polymer dispersions Determination of sieve residue (gross particle and coagulum content) ISO 11357-2, Plastics Differential scanning calorimetry (DSC) Part 2: Determination of glass transition temperature ISO 11359-2, Plastics Thermomechanical analysis (TMA) Part

30、2: Determination of coefficient of linear thermal expansion and glass transition temperature ISO 13741-1, Plastics/rubber Polymer dispersions and rubber latices (natural and synthetic) Determination of residual monomers and other organic components by capillary-column gas chromatography Part 1: Dire

31、ct liquid injection method ISO 13741-2, Plastics/rubber Polymer dispersions and rubber latices (natural and synthetic) Determination of residual monomers and other organic components by capillary-column gas chromatography Part 2: Headspace method ISO 13885-1, Binders for paints and varnishes Gel per

32、meation chromatography (GPC) Part 1: Tetrahydrofuran (THF) as eluent ISO 15528, Paints, varnishes and raw materials for paints and varnishes Sampling 3 EN ISO 7143:2007 (E) ISO 15880, Paints, varnishes and binders Determination of MEQ value of water-based coating materials and binders ISO 16805, Bin

33、ders for paints and varnishes Determination of glass transition temperature 3 Terms and definitions For the purposes of this document, the following terms and definitions apply. 3.1 polymer dispersion liquid or semi-liquid material, usually milkwhite, containing the polymeric material in a stable co

34、ndition, finely dispersed in a continuous liquid phase, normally water (aqueous dispersion) or an organic liquid (non-aqueous dispersion, NAD) ISO 4618:2006 3.2 water-based binder binder in which the main component of the volatile matter is water 4 Sampling Take a representative sample of the produc

35、t to be tested, as described in ISO 15528. 5 Methods of test The test methods used for a particular binder shall be the subject of agreement between the interested parties, if not otherwise specified. The properties given in Table 1 are considered as characterizing properties of water-based binders,

36、 in particular if they are used as raw materials for paints and varnishes. If reactive groups, e.g. hydroxyl groups, are to be determined, the test shall be carried out as for organic binders, before diluting with water. 6 Test report The test report shall contain at least the following information:

37、 a) a reference to this International Standard (ISO 7143:2007); b) all details necessary for complete identification of the product tested (manufacturer, trade name, batch number, etc.); c) the results of the tests and the test methods used; d) any deviations from the procedures specified; e) the da

38、tes of the tests. 4 EN ISO 7143:2007 (E) Table 1 Characterizing properties and test methods Property Method of test Viscosity ISO 3219 Non-volatile matter ISO 3251 pH-value ISO 976 Sieve residue (gross particle and coagulum content) ISO 4576 Minimum film-forming temperature ISO 2115 Glass transition

39、 temperature ISO 16805 Density ISO 2811-1 Residual monomers ISO 13741-1 and ISO 13741-2 Particle size distribution To be agreed between the interested parties aMEQ value ISO 15880 Molecular mass ISO 13885-1 baThe results of particle size analysis, for example with PCS (photon correlation spectroscop

40、y), strongly depend on the details of the method. The results obtained by different laboratories can therefore be compared only if common reference samples are used. bThe results of GPC (gel permeation chromatography) analysis are relative values and depend on the separation factor, column material,

41、 detector, etc. The data obtained by different laboratories can therefore be compared only if common reference samples are used. 5 EN ISO 7143:2007 (E) Bibliography 1 ISO 4618:2006, Paints and varnishes Terms and definitions 2 ISO 12000, Plastics/rubber Polymer dispersions and rubber latices (natural and synthetic) Definitions and review of test methods 6 EN ISO 7143:2007 (E)