DIN EN ISO 105-E04-2013 Textiles - Tests for colour fastness - Part E04 Colour fastness to perspiration (ISO 105-E04 2013) German version EN ISO 105-E04 2013《纺织品 色牢度试验 第E04部分 耐汗渍色牢.pdf

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1、August 2013 Translation by DIN-Sprachendienst.English price group 8No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS

2、59.080.01!%($U“2050150www.din.deDDIN EN ISO 105-E04Textiles Tests for colour fastness Part E04: Colour fastness to perspiration (ISO 105-E04:2013);English version EN ISO 105-E04:2013,English translation of DIN EN ISO 105-E04:2013-08Textilien Farbechtheitsprfungen Teil E04: Farbechtheit gegen Schwei

3、(ISO 105-E04:2013);Englische Fassung EN ISO 105-E04:2013,Englische bersetzung von DIN EN ISO 105-E04:2013-08Textiles Essais de solidit des coloris Partie E04: Solidit des coloris la sueur (ISO 105-E04:2013);Version anglaise EN ISO 105-E04:2013,Traduction anglaise de DIN EN ISO 105-E04:2013-08Superse

4、desDIN EN ISO 105-E04:2013-06www.beuth.deDocument comprises 12 pagesIn case of doubt, the German-language original shall be considered authoritative.07.13 DIN EN ISO 105-E04:2013-08 2 A comma is used as the decimal marker. National foreword This document (EN ISO 105-E04:2013) has been prepared by Te

5、chnical Committee ISO/TC 38 “Textiles” in collaboration with Technical Committee CEN/TC 248 “Textiles and textile products” (Secretariat: BSI, United Kingdom). The responsible German body involved in its preparation was the Normenausschuss Materialprfung (Materials Testing Standards Committee), Work

6、ing Committee NA 062-05-11 AA Farbechtheit von Textilien Deutsche Echtheitskommission DEK e. V. The DIN Standards corresponding to the International Standards referred to in this document are as follows: ISO 105-A01:1994 DIN EN ISO 105-A01:1995-12 ISO 105-A02 DIN EN 20105-A02 ISO 105-A03 DIN EN 2010

7、5-A03 ISO 105-A04 DIN EN ISO 105-A04 ISO 105-A05 ISO 3696 DIN ISO 3696 Amendments This standard differs from DIN EN ISO 105-E04:2009-07 as follows: a) Clauses 2 and 4 and Table 1 have been revised; b) instrumental assessments have been added in Clauses 2 and 4. Compared with DIN EN ISO 105-E04:2013-

8、06, the following corrections have been made to the German version only and therefore do not affect the English text: a) in Subclause 4.3, the quantities of the chemical substances and the subscripts in the formulas have been supplemented; b) in Subclause 4.4, the quantity of the chemical substance

9、has been supplemented. Previous editions DIN 53957: 1954-01 DIN 54020: 1958-09, 1962-05, 1969-12, 1979-02, 1983-11 DIN EN ISO 105-E04: 1996-08, 2009-07, 2013-06 DIN EN ISO 105-A05 DIN EN ISO 105-E04:2013-08 3 National Annex NA (informative) Bibliography DIN EN 20105-A02, Textiles Tests for colour fa

10、stness Part A02: Grey scale for assessing change in colour DIN EN 20105-A03, Textiles Tests for colour fastness Part A03: Grey scale for assessing staining DIN EN ISO 105-A01:1995-12, Textiles Tests for colour fastness Part A01: General principles of testing DIN EN ISO 105-A04, Textiles Tests for co

11、lour fastness Part A04: Method for the instrumental assessment of the degree of staining of adjacent fabrics DIN EN ISO 105-A05, Textiles Tests for colour fastness Part A05: Instrumental assessment of change in colour for determination of grey scale rating DIN ISO 3696, Water for analytical laborato

12、ry use Specification and test methods DIN EN ISO 105-E04:2013-08 4 This page is intentionally blank EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 105-E04 March 2013 ICS 59.080.01 Supersedes EN ISO 105-E04:2009English Version Textiles - Tests for colour fastness - Part E04: Colour fastness

13、 to perspiration (ISO 105-E04:2013) Textiles - Essais de solidit des coloris - Partie E04: Solidit des coloris la sueur (ISO 105-E04:2013) Textilien - Farbechtheitsprfungen - Teil E04: Farbechtheit gegen Schwei (ISO 105-E04:2013) This European Standard was approved by CEN on 14 January 2013. CEN mem

14、bers are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on applicat

15、ion to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Manage

16、ment Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia,

17、 Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 B

18、russels 2013 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 105-E04:2013: EEN ISO 105-E04:2013 (E) Contents Page Foreword 3 1 Scope 4 2 Normative references 4 3 Principle 4 4 Apparatus and materials .5 5 Test specimen 6 6 Proc

19、edure .6 7 Test report 8 2DIN EN ISO 105-E04:2013-08 EN ISO 105-E04:2013 (E) Foreword This document (EN ISO 105-E04:2013) has been prepared by Technical Committee ISO/TC 38 “Textiles” in collaboration with Technical Committee CEN/TC 248 “Textiles and textile products” the secretariat of which is hel

20、d by BSI. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by September 2013, and conflicting national standards shall be withdrawn at the latest by September 2013. Attention is drawn to the possibili

21、ty that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN ISO 105-E04:2009. According to the CEN-CENELEC Internal Regulations, the national standards o

22、rganizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembou

23、rg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. Endorsement notice The text of ISO 105-E04:2013 has been approved by CEN as EN ISO 105-E04:2013 without any modification. 3DIN EN ISO 105-E04:2013-08 1 ScopeThis

24、part of ISO 105 specifies a method for determining the resistance of the colour of textiles of all kinds and in all forms to the action of human perspiration.2 Normative referencesThe following referenced documents are indispensable for the application of this document. For dated references, only th

25、e edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.ISO 105-A01:2010, Textiles Tests for colour fastness Part A01: General principles of testingISO 105-A02, Textiles Tests for colour fastness Part A02: Grey scale for asses

26、sing change in colourISO 105-A03, Textiles Tests for colour fastness Part A03: Grey scale for assessing stainingISO 105-A04, Textiles Tests for colour fastness Part A04: Method for the instrumental assessment of the degree of staining of adjacent fabricsISO 105-A05, Textiles Tests for colour fastnes

27、s Part A05: Instrumental assessment of change in colour for determination of grey scale ratingISO 105-F01, Textiles Tests for colour fastness Part F01: Specification for wool adjacent fabricISO 105-F02, Textiles Tests for colour fastness Part F02: Specification for cotton and viscose adjacent fabric

28、sISO 105-F03, Textiles Tests for colour fastness Part F03: Specification for polyamide adjacent fabricISO 105-F04, Textiles Tests for colour fastness Part F04: Specification for polyester adjacent fabricISO 105-F05, Textiles Tests for colour fastness Part F05: Specification for acrylic adjacent fabr

29、icISO 105-F06, Textiles Tests for colour fastness Part F06: Specification for silk adjacent fabricISO 105-F10, Textiles Tests for colour fastness Part F10: Specification for adjacent fabric: MultifibreISO 3696, Water for analytical laboratory use Specification and test methods3 PrincipleSpecimens of

30、 the textile in contact with adjacent fabrics are treated in two different solutions containing histidine, drained and placed between two plates under a specified pressure in a test device. The specimens and the adjacent fabrics are dried separately. The change in colour of each specimen and the sta

31、ining of the adjacent fabrics are assessed by comparison with the grey scales or instrumentally.EN ISO 105-E04:2013 (E) 4DIN EN ISO 105-E04:2013-08 4 Apparatus and materials4.1 Test devices, each consisting of a frame of stainless steel into which a weight-piece of mass approximately 5 kg and base 6

32、0 mm 115 mm is closely fitted, so that a pressure of (12,5 0,9) kPa can be applied on test specimens measuring (40 2) mm (100 2) mm, placed between glass or acrylic-resin plates measuring approximately 60 mm 115 mm 1,5 mm. The test device shall be constructed so that, if the weight-piece is removed

33、during the test, the pressure remains unchanged.If the dimensions of the composite specimen differ from the size of (40 2) mm (100 2) mm, the weight-piece used shall be such that a nominal pressure of (12,5 0,9) kPa is applied to the specimen.Other devices may be used provided that equivalent result

34、s are obtained.4.2 Oven, maintained at (37 2) C.4.3 Alkaline solution, freshly prepared, using grade 3 water complying with ISO 3696, containing, per litre: 0,5 g of l-histidine monohydrochloride monohydrate (C6H9O2N3HClH2O); 5 g of sodium chloride (NaCl);and either 5 g of disodium hydrogen orthopho

35、sphate dodecahydrate (Na2HPO412H2O)or 2,5 g of disodium hydrogen orthophosphate dihydrate (Na2HPO42H2O).The solution is brought to pH 8 (0,2) with 0,1 mol/l sodium hydroxide solution.4.4 Acid solution, freshly prepared, using grade 3 water complying with ISO 3696, containing, per litre: 0,5 g of l-h

36、istidine monohydrochloride monohydrate (C6H9O2N3HClH2O); 5 g of sodium chloride (NaCl); 2,2 g of sodium dihydrogen orthophosphate dihydrate (NaH2PO42H2O).The solution is brought to pH 5,5 (0,2) with 0,1 mol/l sodium hydroxide solution.4.5 Adjacent fabrics (see ISO 105-A01).Either:4.5.1 A multifibre

37、adjacent fabric complying with ISO 105-F10.or:4.5.2 Two single-fibre adjacent fabrics, complying with the relevant document selected from ISO 105-F01 to F06.One of the adjacent fabrics shall be made of the same kind of fibre as that of the textile to be tested, or that predominating in the case of b

38、lends, the second piece being made of the fibre indicated in Table 1 or, in the case of blends, of the kind of fibre that is second in order of predominance, or as otherwise specified.EN ISO 105-E04:2013 (E) 5DIN EN ISO 105-E04:2013-08 Table 1 Single-fibre adjacent fabricsIf first piece is: Second p

39、iece is to be:cotton woolwool cottonsilk cottonviscose woolpolyamide wool or cottonpolyester wool or cottonacrylic wool or cotton4.5.3 If required, a non-dyeable fabric (for example polypropylene).4.6 Grey scale for assessing change in colour, complying with ISO 105-A02.4.7 Grey scale for assessing

40、staining, complying with ISO 105-A03.4.8 Spectrophotometer or colorimeter for assessing change in colour and staining, complying with ISO 105-A04 and ISO 105-A05.4.9 A set of 11 glass or acrylic resin plates.4.10 Flat-bottomed dish made of inert materials.5 Test specimen5.1 If the textile to be test

41、ed is fabric, eithera) attach a specimen measuring (40 2) mm (100 2) mm to a piece of the multifibre adjacent fabric (4.5.1), also measuring (40 2) mm (100 2) mm, by sewing along one of the shorter sides, with the multifibre fabric next to the face of the specimen; orb) attach a specimen measuring (

42、40 2) mm (100 2) mm between the two single-fibre adjacent fabrics (4.5.2), also measuring (40 2) mm (100 2) mm, by sewing along one of the shorter sides.5.2 Where yarn or loose fibre is to be tested, take a mass of the yarn or loose fibre approximately equal to one half of the combined mass of the a

43、djacent fabrics, and eithera) place it between a (40 2) mm (100 2) mm piece of the multifibre fabric (4.5.1) and a (40 2) mm (100 2) mm piece of the non-dyeable fabric (4.5.3) and sew them along all four sides (see ISO 105-A01:2010, Subclause 10.3, “Preparation of composite specimens”); orb) place i

44、t between a (40 2) mm (100 2) mm piece of each of the two specified single-fibre fabrics (4.5.2) and sew along all four sides.6 Procedure6.1 Lay out the composite specimen smoothly in a flat-bottomed dish and cover with alkaline solution (4.3). Thoroughly wet the composite specimen in this solution

45、at pH 8 (0,2) at an approximate liquor ratio of 50:1, and allow it to remain in the solution at room temperature for 30 min. Press and move it EN ISO 105-E04:2013 (E) 6DIN EN ISO 105-E04:2013-08 from time to time to ensure good and uniform penetration of the liquor. Pour off the solution and wipe th

46、e excess liquor off the specimen between two glass rods.Place the composite specimen between two glass or acrylic-resin plates (see 4.9), under a nominal pressure of (12,5 0,9) kPa, and place in a test device (4.1) which has been preheated to the test temperature.By the same procedure, wet a composi

47、te specimen in the acid solution at pH to 5,5 (0,2) (4.4) and then test it in a separate pre-heated test device.NOTE Up to 10 test specimens, each separated from the next by one plate, can be tested in one test device simultaneously. If less than 10 specimens are prepared, all 11 plates must still b

48、e used to maintain the correct nominal pressure.6.2 Place the test device containing the composite specimen in the oven (4.2) for 4 h at (37 2) C, positioning it so that the test specimens are in either the horizontal position (Figure 1) or the vertical position (Figure 2) depending on the type of device available.Figure 1Figure 26.3 Open out each composite specimen (by break