DIN EN 58-2012 Bitumen and bituminous binder - Sampling bituminous binders German version EN 58 2012《沥青和沥青粘合剂 沥青粘合剂取样》.pdf

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1、May 2012 Translation by DIN-Sprachendienst.English price group 13No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 91

2、.100.50!$|C6“1893219www.din.deDDIN EN 58Bitumen and bituminous binders Sampling bituminous bindersEnglish translation of DIN EN 58:2012-05Bitumen und bitumenhaltige Bindemittel Probenahme bitumenhaltiger BindemittelEnglische bersetzung von DIN EN 58:2012-05Bitumes et liants bitumineux chantillonnage

3、 des liants bitumineuxTraduction anglaise de DIN EN 58:2012-05SupersedesDIN EN 58:2004-10www.beuth.deDocument comprises pagesIn case of doubt, the German-language original shall be considered authoritative.2905.12 DIN EN 58:2012-05 2 A comma is used as the decimal marker. National foreword This stan

4、dard has been prepared by Technical Committee CEN/TC 336 “Bituminous binders” (Secretariat: AFNOR, France). The responsible German bodies involved in its preparation were the Normenausschuss Materialprfung (Materials Testing Standards Committee) and the Normenausschuss Bauwesen (Building and Civil E

5、ngineering Standards Committee), Joint Committee NA 062-03-32 GA Bitumen; Prfverfahren und Anforde-rungen fr die Bindemittel. Amendments This standard differs from DIN EN 58:2004-10 as follows: a) the standard has been editorially revised; b) a new Subclause 8.1.1 “Necessary drawing off before sampl

6、ing” has been included; c) in the German version, the term “Einwegdose” (“surface sampling can”) has been replaced by “Probe-nahmegef fr Oberflchenproben”. Previous editions DIN 1995: 1929, 1934, 1941-11, 1960x-02 DIN 52001: 1980-12 DIN EN 58: 1986-10, 2004-10 EUROPEAN STANDARD NORME EUROPENNE EUROP

7、ISCHE NORM EN 58 March 2012 ICS 91.100.50 Supersedes EN 58:2004English Version Bitumen and bituminous binders - Sampling bituminous binders Bitumes et liants bitumineux - chantillonnage des liants bitumineux Bitumen und bitumenhaltige Bindemittel - Probenahme bitumenhaltiger Bindemittel This Europea

8、n Standard was approved by CEN on 7 January 2012. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references conce

9、rning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member int

10、o its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Irela

11、nd, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue M

12、arnix 17, B-1000 Brussels 2012 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 58:2012: EEN 58:2012 (E) 2 Contents Page Foreword 31 Scope 42 Terms and definitions .43 Safety precautions .54 Fundamentals of sampling .55 Sample size

13、66 Choice of sampling method 67 Number of samples88 Arrangements, equipment and methods of sampling .99 Further treatment of samples 13Annex A (informative) Example of a form for reporting on the sampling of bituminous binders Unique sample identification . 27DIN EN 58:2012-05 EN 58:2012 (E) 3 Forew

14、ord This document (EN 58:2012) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by

15、September 2012, and conflicting national standards shall be withdrawn at the latest by September 2012. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all suc

16、h patent rights. This document supersedes EN 58:2004. According to the CEN/CENELEC Internal Regulations, the national standards organisations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finla

17、nd, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. DIN EN 58:2012-05 EN 58:2012 (E) 4 1 Scope This European Standard specif

18、ies methods of sampling bituminous binders, to determine the average quality of the material under examination and/or to determine deviations from average quality. 2 Terms and definitions For the purposes of this document, the following terms and definitions apply. 2.1 composite sample sample made u

19、p by the mixing of several spot samples Note 1 to entry: A composite sample is regarded as a representative sample if the spot samples are taken according to a sampling plan which makes it probable that the composition of the composite sample approaches that of the material as closely as possible. 2

20、.2 divided sample sample formed by dividing a spot, composite or representative sample into several similar parts by appropriate means 2.3 flowing material material which flows in a transport pipeline or out of the drainline of a storage container 2.4 laboratory sample sample intended for laboratory

21、 tests 2.5 layer sample upper, middle or lower layer spot sample taken at a specific depth in a stationary material, usually in order to detect segregation in large storage containers 2.6 main stream sample sample taken from the outlet stream of a container, such that the entire cross-section of the

22、 outlet stream is included 2.7 material under examination entire quantity of the bituminous binder of which the properties are to be assessed Note 1 to entry: “Material under examination“ is termed simply “material“ in the body of this document. 2.8 side-stream sample sample taken from the outlet st

23、ream by means of a sampling probe 2.9 spot sample sample, taken in a single operation at a single place and time Note 1 to entry: If it can be assumed that the material is homogeneous, a spot sample is regarded as a representative sample. If the material is not homogeneous, a spot sample is only reg

24、arded as representative of a limited region around the sampling point. DIN EN 58:2012-05 EN 58:2012 (E) 5 2.10 stationary material material in a storage container when all valves are closed and there is no flowing in the container 2.11 surface sample spot sample taken at less than 5 cm below the upp

25、er surface 2.12 test sample sample produced by treatment or subdivision of a laboratory sample during preparation in the laboratory of the sample for individual tests 2.13 vertical straight-through sample sample taken by drawing a sampling device through the total depth of the material under examina

26、tion and thereby including all layers of the material 3 Safety precautions The safety precautions given in this clause represent good practice and shall be applied in all cases where they are not in conflict with local or other regulations which shall be followed. The list of safety precautions give

27、n in this clause is not necessarily exhaustive and they should be considered in conjunction with relevant national safety regulations and/or recognised safety code(s) for the petroleum industry. a) All regulations concerning entry into hazardous areas shall be observed rigorously. b) Equipment shall

28、 be maintained adequately. Regular inspections of equipment should be carried out by a competent person. c) All equipment and access facilities shall be checked to ensure that they are adequate for safe working before commencement of sampling. d) Metallic sampling devices used in flammable atmospher

29、es shall be constructed only from non-ferrous metal(s). e) Cords used as components of sampling devices shall be constructed only from vegetable fibre(s), e.g. manilla or sisal; for emulsions, the cord used shall not absorb water from the emulsion. NOTE Attention is drawn to the situation that, for

30、cords made from man-made fibres, it is possible for an operator to build up a dangerous level of electrostatic charge on his person, if he is not earthed and wearing insulating gloves, and that certain man-made fibres will melt or dissolve in hot bitumen. f) Precautions shall be taken to prevent the

31、 breathing of bitumen vapours during sampling operations. g) For samples taken from the main stream, the sampling device shall be selected such that sampling can be performed without pressure. 4 Fundamentals of sampling 4.1 Correct sampling techniques are a prerequisite if meaningful test results ar

32、e to be obtained. 4.2 The person taking the sample shall be experienced in the methods to be employed. DIN EN 58:2012-05 EN 58:2012 (E) 6 4.3 If the sample is to be subdivided, a suitably large representative sample shall be taken and divided into the required number of divided samples. 4.4 A sampli

33、ng report shall be prepared and signed by the person taking the sample. The sampling report shall include: a) name and address of the manufacturer, b) name and address of the supplier (if different from manufacturer), c) object of sampling (batch number, storage container, pipe identification), d) n

34、ature and type of material sampled, e) date and time of sampling, f) name of the sampler, g) unique identification of the sample(s), h) number and amount of samples, i) sampling method used, j) reference to this European Standard, k) any deviation, by agreement or otherwise, from the procedure descr

35、ibed in the standard, l) any special observations. A prepared form shall be used for the sampling report (for example, see Annex A); a copy of the sampling report shall be placed with each divided sample. Sampling reports shall not be put into sample containers. Because of the variety of materials f

36、or which the same container vehicle or storage tank may be used, account should always be taken of possible contamination by residues, deposits or solvents. For this reason, it is relevant to enter data in the report on the previous history of the container vehicle or storage tank. 5 Sample size Eac

37、h divided sample should consist of at least 0,5 kg material. NOTE The required size of a laboratory sample is dependent upon the nature and extent of the tests to be carried out. 6 Choice of sampling method The sampling method to be used depends upon: a) nature, quantity and temperature of the mater

38、ial under examination, b) number, type and size of the containers or cans from which the sample is to be taken, c) whether the sample is to be taken from a stationary or a flowing material. Arrangements, equipment and methods of sampling are described in Clause 8. DIN EN 58:2012-05 EN 58:2012 (E) 7

39、If samples shall be taken frequently from a large volume liquid material container, sampling appliances such as sampling valves, sampling probes or three-way cocks can conveniently be installed permanently. Otherwise, liquid test materials shall be sampled by immersion techniques, for example, by we

40、ighted sampling cans or bottom closing sampling tubes; materials fluid at low temperature can be sampled from drums or containers of up to 2 m3capacity by means of open sampling tubes. Table 1 gives an informative guideline for sampling devices. Viscous, plastic and semi-solid material shall be samp

41、led using tools of the kind described in 8.4, semi-solid to brittle material by means of hand-operated tools described in 8.5 and granular material or lumps according to 8.5 and 8.6. Sampling from the main stream by disconnecting the pipe linking a container vehicle to a storage tank shall not be ca

42、rried out. DIN EN 58:2012-05 EN 58:2012 (E) 8 Table 1 Sampling methods for material liquid at either high or low temperatures in pipelines, containers or cans Sampling method Sampling from pipelines Sampling from containers of capacity According to subclause Main stream Side stream 800 m3 50 m3 to 8

43、00 m3 2 m3 to 50 m3 2 m3 and cans Sampling using permanently installed equipment sampling probe 8.1.2 - + - - - - from sampling valve 8.1.3 - - + + + - 8.1.4 - + - - - - 3-way valve 8.1.5 + - - - - - Sampling using immersion methods weighted sampling can 8.2.1 - - + + + (+) surface sampling can 8.2.

44、2 - - - - + - bottom closing sampling tube 8.2.3 - - - (+) + + open sampling tube 8.2.4 - - - - - 0 vertical straight-through can 8.2.5 - - - - + + Sampling directly from installations from spraying equipment 8.3 + - - - - - Key + usable (+) limited use 0 only usable for materials fluid at low tempe

45、rature - not applicable 7 Number of samples The number of samples taken shall be dependent upon the size and form of the container and for deliveries in cans and lumps upon the number of those in a delivery; the number of samples to be taken from a container shall be as given for each sampling metho

46、d in Clause 8. For deliveries in cans and lumps, the number of cans or lumps from which samples are to be taken shall conform to Table 2. Initially, one sample from each can or lump shall be tested. If this test shows deviation from the specification, the remaining samples shall be tested. DIN EN 58

47、:2012-05 EN 58:2012 (E) 9 If sampling is intended to check homogeneity (segregation) in stationary liquid material, at least three layer samples (upper layer, middle layer and lower layer) shall be taken. They shall not be mixed to form a composite sample. If, in exceptional circumstances, it is des

48、ired to assess the average quality from layer samples, the geometry of the container shall be taken into account. Table 2 Number of cans or lumps from which samples are to be taken Total number of cans or lumps (n) Number of cans or lumps sampled 2 to 8 2 9 to 27 3 28 to 64 4 65 to 125 5 126 to 216 6 217 to 343 7 344 to 512 8 513 to 729 9 730 to 1 000 10 over 1 000 3n , rounded to the nearest integer above, where n is the total number of cans or lumps 8 Arrangements, equipment and methods of sampling 8.1 Sampling using p